Labconco RapidVap 73200 Series User manual

RapidVapVertex Evaporator
Models
73200 Series

Copyright © 2017 Labconco Corporation. The information contained in this manual and the
accompanying products are copyrighted and all rights reserved by Labconco Corporation. Labconco
Corporation reserves the right to make periodic design changes without obligation to notify any person or
entity of such change.
Returned or Damaged Goods
Do not return goods without the prior authorization from Labconco. Unauthorized returns will not be
accepted. If your shipment was damaged in transit, you must file a claim directly with the freight carrier.
Labconco Corporation and its dealers are not responsible for shipping damages.
The United States Interstate Commerce Commission rules require that claims be filed with the delivery
carrier within fifteen (15) days of delivery.
Limitation of Liability
The disposal and/or emission of substances used in connection with this equipment may be governed by
various federal, state, or local regulations. All users of this equipment are required to become familiar
with any regulations that apply in the user’s area concerning the dumping of waste materials in or upon
water, land, or air and to comply with such regulations. Labconco Corporation is held harmless with
respect to user’s compliance with such regulations.
Contacting Labconco Corporation
If you have questions that are not addressed in this manual, or if you need technical assistance, contact
Labconco’s Customer Service Department or Labconco’s Product Service Department at 1-800-821-5525
or 1-816-333-8811, between the hours of 7:30 a.m. and 5:30 p.m., Central Standard Time.
Part #7324400, Rev. C
ECO L627
Warranty
Labconco Corporation provides a warranty to the original buyer for the repair or replacement of parts and
reasonable labor as a result of normal and proper use of the equipment with compatible chemicals. Broken
glassware and maintenance items, such as filters, gaskets, light bulbs, finishes and lubrication are not
warranted. Excluded from warranty are products with improper installation, erratic electrical or utility supply,
unauthorized repair and products used with incompatible chemicals.
The warranty for RapidVap®Vertex™ Evaporators will expire one year from date of installation or two years
from date of shipment from Labconco, whichever is sooner. Warranty is non-transferable and only applies to
the owner (organization) of record.
Buyer is exclusively responsible for the set-up, installation, verification, decontamination or calibration of
equipment. This limited warranty covers parts and labor, but not transportation and insurance charges. If the
failure is determined to be covered under this warranty, the dealer or Labconco Corporation will authorize
repair or replacement of all defective parts to restore the unit to operation. Repairs may be completed by 3rd
party service agents approved by Labconco Corporation. Labconco Corporation reserves the rights to limit this
warranty based on a service agent’s travel, working hours, the site’s entry restrictions and unobstructed access
to serviceable components of the product.
Under no circumstances shall Labconco Corporation be liable for indirect, consequential, or special damages
of any kind. This warranty is exclusive and in lieu of all other warranties whether oral, or implied.

T
TA AB BL LE E O OF F C CO ON NT TE EN NT TS S
CHAPTER 1: INTRODUCTION 1
Typographical Conventions 2
CHAPTER 2: PREREQUISITES 3
Electrical Requirements 4
Location and Exhaust Requirements 4
Nitrogen Supply Requirements 4
Space Requirements 4
Tools Required 4
CHAPTER 3: GETTING STARTED 5
Unpacking Your RapidVap Vertex Evaporator 6
RapidVap Vertex Evaporator Components 6
Setting Up Your RapidVap Vertex Evaporator 8
Sample Block 8
Nitrogen Gas Connection 9
Exhaust Port 9
Electrical Connection 10
Chemical Attack on RapidVap Vertex Evaporator Components 10
Solvent Safety Precautions 11
CHAPTER 4: USING YOUR RAPIDVAP VERTEX
EVAPORATOR 13
Planning 14
Loading Glassware into the RapidVap Vertex Evaporator 14
RapidVap Vertex Evaporator Controls 14
Operating the RapidVap Vertex Evaporator Controls 15
Operating the RapidVap Vertex Evaporator 19
Operational Notes 20
Interrupting a Cycle After it has Begun 20
CHAPTER 5: MAINTAINING YOUR RAPIDVAP VERTEX
EVAPORATOR 21

CHAPTER 6: TROUBLESHOOTING 22
APPENDIX A: RAPIDVAP VERTEX EVAPORATOR
COMPONENTS 25
APPENDIX B: RAPIDVAP VERTEX EVAPORATOR
DIMENSIONS 28
APPENDIX C: RAPIDVAP VERTEX EVAPORATOR
SPECIFICATIONS 29
Evaporation Rates 31
APPENDIX D: RAPIDVAP VERTEX EVAPORATOR
ACCESSORIES 32

Product Service 1-800-522-7658
1
C
CH HA AP PT TE ER R 1 1
I
IN NT TR RO OD DU UC CT TI IO ON N
Congratulations on your purchase of a Labconco RapidVap Vertex
Evaporator. Models are available for operation on 115V or 230V. Superior
evaporation rates are achieved by the unique blending of several gentle forces
on the sample. The vials containing the sample are held at an angle to
increase the surface area of the sample thereby increasing the evaporation
rate. A precisely controlled amount of thermal energy can be supplied to the
sample to heat it. Finally, a stream of nitrogen or dry gas is directed
downward onto the surface of the sample. This reduces the partial pressure
directly over the liquid to speed evaporation and helps remove the solvent as
it evaporates. In summary, the RapidVap Vertex Evaporator performance is
maximized by increasing the sample’s surface area, increasing temperature
and directing gas over the sample. The microprocessor provides excellent
regulation of the heater and reproducibility of protocols.

Chapter 1: Introduction
Product Service 1-800-522-7658
2
Typographical Conventions
Recognizing the following typographical conventions will help you
understand and use this manual:
Book, chapter, and section titles are shown in italic type (e.g., Chapter 3:
Getting Started).
Steps required to perform a task are presented in a numbered format.
Comments located in the margins provide suggestions, reminders, and
references.
Critical information is presented in boldface type in paragraphs that are
preceded by the exclamation icon. Failure to comply with the
information following an exclamation icon may result in injury to the user
or permanent damage to your RapidVap Vertex Evaporator.
Important information is presented in capitalized type in paragraphs that
are preceded by the pointer icon. It is imperative that the information
contained in these paragraphs be thoroughly read and understood by the
user.
!


Product Service 1-800-522-7658
3
C
CH HA AP PT TE ER R 2 2
P
PR RE ER RE EQ QU UI IS SI IT TE ES S
Before you install your RapidVap Vertex Evaporator, you need to prepare
your site for installation. Carefully examine the location where you intend to
install your RapidVap Vertex Evaporator. You must be certain that the area is
level and of solid construction. In addition, an exhaust means must be
provided and a source of nitrogen or dry gas must be available. An electrical
source must be located near the installation site.
Carefully read this chapter to learn:
the electrical supply requirements.
the exhaust requirements.
the nitrogen supply requirements.
Refer to Appendix C: RapidVap Vertex Evaporator Specifications for
complete RapidVap Vertex Evaporator electrical and environmental
conditions, specifications and requirements.

Chapter 2: Prerequisites
Product Service 1-800-522-7658
4
Electrical Requirements
A dedicated electrical outlet is required. Minimum requirements for an outlet
is a 15 Amp circuit breaker or fuse for models rated at 115V (60 Hz) or an 8
Amp circuit breaker or fuse is required for 230V (50/60 Hz) models. 115V
models are equipped with a 15 Amp NEMA 5-15P plug. 230V models are
available with a NEMA 6-15P plug for use in the United States, a PS 1363
plug for use in the United Kingdom, a CEE 7/7 plug for use in Europe or a
CHI-10P plug for use in China. It may be necessary to remove the plug and
install a different plug to match the available receptacle if one of these
models does not meet your needs.
Location and Exhaust Requirements
The RapidVap Vertex Evaporator must be located within a fume hood if
hazardous or flammable solvents are used. In all cases, regardless of the
solvent used, it is recommended that the exhaust hose is vented into a fume
hood or other laboratory ventilation device.
Nitrogen Supply Requirements
The 1/4" I.D. hose on the rear of the RapidVap Vertex Evaporator should be
attached to a regulated source of nitrogen or other suitable gas. Pressure
must NOT exceed 80 psi. The nitrogen supply must be capable of 6.5 CFM
flow rate. A suitable barb or compression fitting must be supplied by the
user.
Space Requirements
Refer to Appendix B: RapidVap Vertex Evaporator Dimensions for
dimensional drawings of the RapidVap Vertex Evaporator.
Tools Required
Common hand tools are required to set up the RapidVap Vertex Evaporator.
A screwdriver or 5/16" socket is needed to attach hose clamps. A tubing
cutter or knife is needed to shorten exhaust hoses.
!

Product Service 1-800-522-7658
5
C
CH HA AP PT TE ER R 3 3
G
GE ET TT TI IN NG G S ST TA AR RT TE ED D
Now that the site for your RapidVap Vertex Evaporator is properly prepared,
you are ready to unpack, inspect, install, and test your RapidVap Vertex
Evaporator. Read this chapter to learn how to:
unpack and move your RapidVap Vertex Evaporator.
set up your RapidVap Vertex Evaporator.
connect the nitrogen source to your RapidVap Vertex Evaporator.
connect the electrical supply source to your RapidVap Vertex
Evaporator.
properly exhaust your RapidVap Vertex Evaporator.
solvent safety precautions.
The RapidVap Vertex Evaporator weighs over 35 lbs.
(16 Kg). The carton allows for lifting with a mechanical lift
truck or hand truck.
!

Chapter 3: Getting Started
Product Service 1-800-522-7658
6
Unpacking Your RapidVap Vertex
Evaporator
Carefully unpack your RapidVap Vertex Evaporator and inspect it for damage
that may have occurred in transit. If your RapidVap Vertex Evaporator is
damaged, notify the delivery carrier immediately and retain the entire shipment
intact for inspection by the carrier.
DO NOT RETURN GOODS WITHOUT THE PRIOR
AUTHORIZATION OF LABCONCO. UNAUTHORIZED
RETURNS WILL NOT BE ACCEPTED.
IF YOUR RAPIDVAP VERTEX EVAPORATOR WAS
DAMAGED IN TRANSIT, YOU MUST FILE A CLAIM
DIRECTLY WITH THE FREIGHT CARRIER. LABCONCO
CORPORATION AND ITS DEALERS ARE NOT
RESPONSIBLE FOR SHIPPING DAMAGES.
Do not discard the carton or packing material for your RapidVap Vertex
Evaporator until you have checked all of the components and installed and
tested the RapidVap Vertex Evaporator.
RapidVap Vertex Evaporator
Components
Locate the model of RapidVap Vertex Evaporator you received in the
following table. Verify that the components listed are present and undamaged.
Catalog #
Description
7320020
RapidVap Vertex Evaporator –115V
Plus the Following:
Part #
Component Description
7913100
Exhaust Hose
1966000
Clamp
1334500
Power Cord NEMA 5-15P
7324400
User’s Manual
1533301
Tubing
The United
States
Interstate
Commerce
Commission
rules require
that claims be
filed with the
delivery
carrier within
fifteen (15)
days of
delivery.



Chapter 3: Getting Started
Product Service 1-800-522-7658
7
Catalog #
Description
7320030
RapidVap Vertex Evaporator –230V EU
Plus the Following:
Part #
Component Description
7913100
Exhaust Hose
1966000
Clamp
1336100
Power Cord CEE 7/7
7324400
User’s Manual
1533301
Tubing
Catalog #
Description
7320035
RapidVap Vertex Evaporator –230V UK
Plus the Following:
Part #
Component Description
7913100
Exhaust Hose
1966000
Clamp
1332600
Power Cord PS 1363
7324400
User’s Manual
1533301
Tubing
Catalog #
Description
7320037
RapidVap Vertex Evaporator –230V China
Plus the Following:
Part #
Component Description
7913100
Exhaust Hose
1966000
Clamp
1332700
Power Cord CHI-10P
7324400
User’s Manual
1533301
Tubing
Catalog #
Description
7320040
RapidVap Vertex Evaporator –230V US
Plus the Following:
Part #
Component Description
7913100
Exhaust Hose
1966000
Clamp
1338000
Power Cord NEMA 6-15P
7324400
User’s Manual
1533301
Tubing
Since users’ preference of sample size varies, the sample holding block is not
included with the RapidVap Vertex Evaporator. The correct size block must
be selected and ordered separately. Refer to Appendix D: RapidVap Vertex
Evaporator Accessories for block selection.
If you do not receive one or more of the components listed for your RapidVap
Vertex Evaporator, or if any of the components are damaged, contact
Labconco Corporation immediately for further instructions.

Chapter 3: Getting Started
Product Service 1-800-522-7658
8
Setting Up Your RapidVap Vertex
Evaporator
After you verify the RapidVap Vertex Evaporator components, move your
RapidVap Vertex Evaporator to the location where you want to install it.
Then, follow the steps listed below.
Sample Block
The RapidVap Vertex Evaporator was shipped without the sample block
installed. See Appendix D for available blocks. Vials must be snug in the holes
in the block. Select the appropriate block to fit the vials that will be used.
Make certain that the bottom of the chamber is clean and free of debris. The
sample block slides in on the two guides on the front and MUST rest securely
on the bottom. Make certain that the small .21" dia. temperature sensor hole is
in the upper left hand corner. Placing the block in the chamber improperly will
effect performance. Insert the tubular temperature sensor into the .21" dia. hole
to monitor upper block temperature. The actual sample temperature may be
monitored throughout a run by placing the sensor directly into a sample vial.

Chapter 3: Getting Started
Product Service 1-800-522-7658
9
Nitrogen Gas Connection
Mark the gas supply hose 3/4" (19 mm) from the end and push the hose into
the fitting in the back of the RapidVap Vertex Evaporator. Attach the other
end of the hose to user supplied nitrogen supply.
THE NITROGEN SUPPLY PRESSURE MUST NEVER BE
ALLOWED TO EXCEED 80 PSI (345 KPA).
Exhaust Port
If the RapidVap Vertex Evaporator is not located in a fume hood, attach one
end of the two inch diameter venting hose that is supplied with the RapidVap
Vertex Evaporator to the exhaust port on the rear of the unit. Clamp securely.
Route the other end to a fume hood or other laboratory ventilation device.


Chapter 3: Getting Started
Product Service 1-800-522-7658
10
Electrical Connection
Plug the power cord into the receptacle on the back of the RapidVap Vertex
Evaporator and plug the other end into a suitable wall power receptacle.
Chemical Attack on RapidVap Vertex
Evaporator Components
Your RapidVap Vertex Evaporator is designed to be chemical resistant to most
compounds that are commonly used in the concentration processes that are
performed in it. However, by necessity, the RapidVap Vertex Evaporator is
comprised of a number of different materials, some of which may be attacked
and degraded by certain chemicals. The degree of degradation is obviously
dependent on the concentration and duration of exposure. Some of the major
components of the RapidVap Vertex Evaporator that are susceptible to
degradation are as follows:
C- Moderate Degradation- Questionable Use
D- Severe Degradation-Infrequent use recommended-immediate thorough
cleaning required
Acids
Bases
Solvents
COMPONENT
MATERIAL
Acetic Acid 20%
Boric Acid
Formic Acid
Hydrobromic Acid 20%
Hydrochloric Acid 20%
Nitric Acid 20%
Sulfuric Acid 10%
Trifluoroacetic Acid (TFA)
Ammonium Hydroxide
Potassium Hydroxide
Acetone
Acetonitrile
Chloroform
Dimethyl Formamide
Dimethyl Sulfoxide (DMSO)
Ethanol
Ethyl Acetate
Hexanes
Isoproponal
Methylene Chloride
Toluene
Elbow N2
Polyamid (Nylon)
D
D
D
D
D
D
D
C
D
C
Blower Impeller
Polyamid (Nylon)
D
D
D
D
D
D
D
C
D
C
Blower Housing
Polypropylene
C
C
Exhaust Hose
Polyethylene
C
C
C
C
C
C
C
N2 Supply Hoses
Polyethylene
C
C
C
C
C
C
C
Block Guides
UMHW Polyethylene
C
C
C
C
C
C
C
Window Seal
PVC
D
C
D
D
D
D
D
D
C
D
D
D
D
Lid
Epoxy Coated Alum.
C
D
C
D
Chamber & Block
Aluminum
D
D
D
D
D
D
C
Nozzle N2
Stainless Steel
D
D
D
Exhaust Fitting
Stainless Steel
D
D
D
Ducting
Epoxy Coated Steel
C
D
C
D
Window
Glass

Chapter 3: Getting Started
Product Service 1-800-522-7658
11
Glass lids are suitable for use with all common compounds.
When using compounds in the RapidVap Vertex Evaporator that are hostile to
the materials of construction, it is imperative that the equipment is properly
maintained.
After each run, clean up all residues, spills, and materials that might have
splashed in the chamber using agents suitable for the substance involved.
With prudent maintenance your RapidVap Vertex Evaporator will provide many
years of service. Warranty on the affected parts will be void if maintenance has
obviously been neglected. If you have questions about using specific compounds
in your RapidVap Vertex Evaporator, contact Labconco Technical Service at
1-800-821-5525 or 816-333-8811 or e-mail [email protected].
Safety Precautions
The RapidVap Vertex Evaporator is not classified as “explosion proof.” It has
been designed with safety as a primary consideration and should be used in a
prudent manner using “good laboratory practices.” It has been designed for
use with compounds as described in the United States National Electrical Code
Class I, Group D. The block that holds the sample tubes may be programmed
to run as hot as 100°C, however, the heater element may normally run at
135°C. A thermal fuse limits the heater to a maximum temperature of 152°C.
It is important that the solvents used are compatible with these temperatures.
Do not evaporate solvents that have an autoignition
temperature below 180°C. Do not evaporate solvents that
are classified as Group A, B, or C by the National Electrical
Code. Evaporate only non-flammable or Group D solvents
with autoignition temperatures 180°C or above. Use of
other compounds could cause an explosion.
Solvents used in the RapidVap Vertex Evaporator may be
flammable or hazardous. Use extreme caution and keep
sources of ignition away from the solvents. When using
flammable or hazardous solvents, the RapidVap Vertex
Evaporator should be operated inside a fume hood.
If a sample is spilled in the chamber it must immediately be
cleaned up.
Hazardous materials such as strong acids or bases,
radioactive substances and volatile organics, must be
handled carefully and promptly cleaned up if spilled.
!


Chapter 3: Getting Started
Product Service 1-800-522-7658
12
Several components of the RapidVap Vertex Evaporator
which are located inside the chamber are made of stainless
steel or aluminum which can be attacked by acids. Use of
acids such as trifluoroacetic acid can result in degradation
of the product. Use care when using aggressive liquids
which can damage the RapidVap Vertex Evaporator and
thoroughly clean the RapidVap Vertex Evaporator after
each use. Contact Labconco before evaporating acids.
WARNING: The disposal of substances used in connection
with this equipment may be governed by various Federal,
State or local regulations. All users of this equipment are
urged to become familiar with any regulations that apply in
the user’s area concerning the dumping of waste materials
in or upon water, land or air and to comply with such
regulations.
When lifting this product, use at least two (2) persons and always use safe
lifting practices.
Do NOT use a detachable power cord that is not adequately rated for product.
Always disconnect power from outlet before beginning service operations.
Do not damage internal wiring or other components while service panels are
removed. If internal wiring or components are damaged, do not restore power,
contact Labconco’s Product Service Department immediately.
Wear all required Personnel Protective Equipment (PPE) during service
operations. At a minimum, this includes: eye protection, breathing protection,
skin protection. Do not wear loose fitting clothes that can catch on internal
surfaces. After service, verify safe state of use before using the product.
Contact Labconco’s Product Service Department for questions on
determining safe state of this product.
Verify protective earth ground continuity before using equipment.
No special ventilation requirements.
No hazards exist for: explosion, implosion, or release of toxic or flammable
gases arising from the materials being heated.
No Heat Transfer Media is required for the normal operation of this equipment.
Cleaning solutions that do not contain chlorine-based disinfectants (such as
Bleach or hypochlorites) may be safely used on this equipment.
If there is any doubt about the compatibility of decontamination or
cleaning agents, contact Labconco’s Product Service Department.

Product Service 1-800-522-7658
13
C
CH HA AP PT TE ER R 4 4
U
US SI IN NG G Y YO OU UR R R RA AP PI ID DV VA AP P
V
VE ER RT TE EX X E EV VA AP PO OR RA AT TO OR R
After your RapidVap Vertex Evaporator has been installed as detailed in
Chapter 3: Getting Started, you are ready to begin using your RapidVap
Vertex Evaporator. Read this chapter to learn how to:
set operating parameters.
operate the controls.
properly select and position glassware inside your RapidVap Vertex
Evaporator.
understand the display.
interrupt a cycle after it has begun.
Do not use the RapidVap Vertex Evaporator in a manner
not specified by the manufacturer (refer to Appendix C:
RapidVap Vertex Evaporator Specifications). The electrical
protection properties of the RapidVap Vertex Evaporator
may be impaired if the RapidVap Vertex Evaporator is
used inappropriately.
!

Chapter 4: Using Your RapidVap Vertex Evaporator
Product Service 1-800-522-7658
14
Planning
Thoroughly understand procedures and the equipment operation prior to
beginning work. The unique performance of the RapidVap Vertex
Evaporator is dependent upon the proper balance of heat and nitrogen flow.
If the proper balance is not established, it is possible to damage or lose a
portion of the sample. Therefore, if you are unfamiliar with the RapidVap
Vertex Evaporator or are attempting a new protocol, it may be helpful to
make a trial run that is void of the sample you are attempting to concentrate.
Select the size of the sample tube so it is compatible with the block. Tubes
should not be loose in the block. Blocks are available with holes for various
size tubes.
Loading Glassware Into the RapidVap
Vertex Evaporator
There are 5 control valves that control nitrogen to the 5 horizontal rows of
nozzles. Samples should be positioned in complete rows as much as possible.
This will minimize the number of rows of nozzles and reduce gas consumption.
RapidVap Vertex Evaporator Controls
The control panel for the RapidVap Vertex Evaporator is shown below with a
description about their function.

Chapter 4: Using Your RapidVap Vertex Evaporator
Product Service 1-800-522-7658
15
Nitrogen Control Valves –Used to turn nitrogen flow ON or OFF to the
nozzles above the sample vials. The top valve controls the 10 nozzles on the
top row. The second valve controls the second row of 10 nozzles. The third
valve controls the middle row of 10 nozzles. The fourth valve controls the
fourth row of 10 nozzles. The bottom valve controls the bottom row of 10
nozzles. Push the lever to the right to turn nitrogen flow ON.
Nitrogen Pressure Regulator –Used to adjust the gas pressure and gas flow
rate to the nozzles. To adjust the gas pressure to the nozzles, the gas supply
must be connected. Open all of the control valves that will be used during the
run. Turn the unit ON and press Run, the main gas supply valve will open.
Pull the knob of the Pressure Regulator out and rotate the knob clockwise to
increase pressure, counter clockwise to decrease the pressure. The operating
pressure is displayed on the knob. Once the pressure is set push the regulator
knob in and press Stop.
The pressure can be adjusted at any time during the run. Also note that
opening or closing any of the Nitrogen Control Valves without adjusting the
pressure will change the flow rate at each nozzle.
The flow rate of gas is approximately 1 cfm (28.3 L/min) per row of 10
nozzles when pressure is set at 24 PSI (165 KPA).
Digital Display –The touch screen LCD is used to control run time and
temperature, preheat temperature and other functions as described below.
Operating the RapidVap Vertex Evaporator
Controls
When the power switch on the left hand side is turned ON the opening
display will show:
(In all diagrams, the numbers are just examples and will vary)
Press open area above °C or °F symbol to change the degree display to show
°C or °F. All parameters that are entered will be remembered in the
microprocessor memory and will remain entered until reset.
BLOCK
SAMP
52
51
°C
Run
Pre Heat
Prog

Chapter 4: Using Your RapidVap Vertex Evaporator
Product Service 1-800-522-7658
16
Program:
To enter a new program while in the opening display press “PROG” and the
display will show:
Press “Back” to return to the opening display, press “Run” to start this
program. If the program, temperature or time needs to be changed, press
either “PROG,” “TEMP” or “TIME.” The display will show:
Ten different programs may be stored and then later recalled. Press “PROG”
or “TEMP” or “TIME” and the word will start to flash. Press “Up” or
“Down” to change the value. Another word may be selected and the value
under the word may be changed by pressing “Up” or “Down.” Press either
“Run” to begin the run or press “Back” to return to the opening display.
If “TIME” is set to ON, the program will run continually until turned off by
pressing “STOP” or “PAUSE.”
PROG
TEMP
TIME
1
35
62
Back
Run
PROG
TEMP
TIME
3
67
74
Back
Up Down
Run