Milli-Q IQ Element User manual

User Manual
Milli-Q®IQ Element
®

Table of contents
INTRODUCTION 1
  Systemidentication       1
  Intendeduse        1
Milli-Q®IQElementunitcomponents     2
  Flowschematics        3
QUICK START 5
  Navigatethescreeninterface      5
  Dispensingultrapurewater      6
  Dispensereport        8
MAINTENANCE AND SETTINGS 9
Milli-Q®IQElementunitsettings     9
  Distributiondepressurization      9
  Consumableskitreplacementstandardoperatingprocedure 10
  PurgingairfromtheIPAKQuantaICP®cartridge   16
Icons17
REQUIREMENTS AND SPECIFICATIONS 18
  Systemspecications       18
  Dimensionsandweight       19
  OrderingInformation       20
LEGAL INFORMATION & WARRANTY 21

Introduction 1
Congratulations!
ThankyouforbuyingaMilli-Q®IQ Element unit.
Installationofthisproductshouldbefollowedbyaqualiedservicerepresentativewithaccess
toqualiedinstallationdocumentation.
ThisusermanualisaguideforuseduringthenormaloperationandmaintenanceofaMilli-Q®IQ
Elementunit.Itishighlyrecommendedtofullyreadthismanualandcomprehenditscontents
beforehandlingit.
System identication
System Catalogue number Voltage Frequency
Milli-Q®IQ Element unit ZIQELEMT0 - -
ThesystemiselectricallypoweredandhydraulicallyfedbyaMilli-Q®IQ7003/7005/7010/7015
system-orbyaMilli-Q®IQ7000system-workingthemselveswithinthe100-240Vand50-
60Hzrangesrespectivelyforthevoltageandfrequency.
Manufacturingsite:
MilliporeSAS,67120Molsheim,France
FormoreinformationonyourMilli-Qsystem,pleasecallyourlocalrepresentativeorvisitour
websitewww.emdmillipore.com(NorthAmerica)orwww.merckmillipore.com(RestoftheWorld).
Intended use
MerckKGaA doesnotwarranttheproductfor anyspecicapplication. It isupto the userto
determineifthequalityofthewaterproducedbytheproductmatchestheirexpectations,ts
withnorms/legalrequirementsandtobearresponsibilityresultingfromtheusageofthewater.
The product is not intended to produce: water for injection, water for dialysis, sterile water for
irrigation or injection, bacteriostatic water for injection, sterile puried water in containers, and
sterile water for injection in container or ingestion. The product is not intended to be used in
explosive environments according to ATEX Directive – equipment & protective systems intended
for use in potentially explosive atmospheres. In addition the product is not intended as a Medical
Device, including In-Vitro Devices.
INTRODUCTION

Introduction 2
Milli-Q®IQ Element unit components
1Footpedal 6USBport
2Milli-Q®IQElementunitfrontcover 7IPAKQuantaICP®
3Dispensingtubingsupport 8OptimizerLW™nallter
4Optimizerby-pass 9Milli-Q®IQElementunitproducttubing
5Milli-Q®IQElementunitHMI 10 e-Suretagreader
9
1
2
3
4
7
8
5
10
6

Introduction 3
Flow schematics
Milli-Q® IQ Element unit ow schematic:
1
Connection from the Milli-Q®
IQ 7000 system or the Milli-Q®
7003/7005/7010/7015 system to the
Milli-Q®IQ Element unit
6Milli-Q®IQElementunitproducttubing
2Flowmeter 7Check-valve
3IPAKQuantaICP®8ConnectionfromtheMilli-Q®IQ Element
unittoapotentialQ-POD®
4OptimizerLW™nallter 9Connection from a potential Q-POD®
backtotheMilli-Q®IQ Element unit
52-wayssolenoidvalve 10
ConnectionfromtheMilli-Q®IQ Element
unitbacktotheMilli-Q®IQ7000system
ortheMilli-Q®IQ7003/7005/7010/7015
system
Note:IfnoQ-POD®isinstalled,8isdirectlyconnectedto10and9doesn’texist.
H
G
F
E
D
C
B
A
8
7
6
5
4
3
2
1
H
G
F
E
D
C
B
A
8
7
6
5
4
3
2
1
10
1
2
3
4
6
5
7
8
9
Milli-Q® IQ Element

Introduction 4
Location of the Milli-Q® IQ Element unit on the system ow schematic
Milli-Q®IQElementunitconnectedonaMilli-Q®IQ7000system:
Milli-Q®IQElementunitconnectedonaMilli-Q®IQ7003/7005/7010/7015system:
TheMilli-Q®IQElementunitislocatedonthedistributionsideoftheowschematic.
RegardlessofthesystemtypethatisattachedtotheMilli-Q®IQElementunit,oneQ-POD®can
beconnectedaftertheMilli-Q®IQElementunitfortheproductionoftheultrapurewater.The
Milli-Q®IQElementunitmustbealwayslocatedastherstPODpositionoftheultrapureline.
Milli-Q®IQ Element unit
Milli-Q®IQ Element unit

Quick start 5
QUICK START
Navigate the screen interface
HOME SCREEN
MAIN MENUS
Home
-Waterquality
information
-Dispensingfunctions
-Alerts&Alarms
(whenapplicable)
-Dispensereport
(whenapplicable)
Menu
-Consumables
-Information
-Settings
-Maintenance
-Login
Goto
Consumables
Menu
Goto
Information
Menu
Goto
Settings
Menu
Goto
Maintenance
Menu
Goto
Manageraccess

Quick start 6
Dispensing ultrapure water
Before dispensing
Itisagoodpracticetoalwaysrecirculatewaterbeforedispensing.
Todothis,pressontherecirculationicon ,thisalsorefreshesthewaterqualityparameters:
•Productresistivity
• TOC
•Temperature
When connected to a storage tank, always make sure there is enough water present before
dispensing.Thisinformationisalwaysdisplayedonthemainscreen.
Dispensing ultrapure in free ow mode
Enablesausertodispensemanuallyinafreeowmode.
1.Todispenseultrapurewater,usethefoodpedalswitchconnectedtothebaseoftheMilli-Q®
IQElementunit,asshowninthepicturebelow.
2.Pressonceandquicklyreleasetodispenseinfullow.
3.Pressandholdtostartdispensingindrop-by-drop,keeppressingtoincreasetheowrate
untilfullowisreached.Releaseatthechosenowrate.
4.Pressoneadditionaltimewhenyouwishtostoptheowdispensing.

Quick start 7
Dispensing ultrapure water in volumetric dispensing mode
Enablesausertoautodispenseapre-selectedvolume(20mLto100L).Simplypresstheicon
oftheHomescreentostartavolumetricdispensing.
1- Press the pre-selected volume box to
setthedesiredvolumetodispense.Ifthe
volume is set as you expect, either press
thestart button on the screen or the foot
pedaltoinitiatethedispense.
2-Selecttheunit.
3- Select the desired volume and press
“OK”tovalidate.
4-Eitherpressthestopbuttononthescreenor
thefootpedaltostopthedispense.
Thesystemwillautomaticallystoponcetheinputvolumeisreached.
Note:Thesystemrecordsthelastvolumedispensed.Torepeatavolumetricdispense,clickon
thestarticonorthefootpedal.

Quick start 8
Dispense report
A dispense report is automatically produced after each dispensing operation. A dispensing
operationisconsideredtobealldispenseswithlessthan10secondintervalsbetweenthem.This
canbeinterruptedatanytimebypressingonthedispensereporticonthatbecomesavailable
onthehomescreenassoonasadispenseisinitiated.
1.Consultthereportdata
Clickonthedispensereporticon:
2.Personalize(assignanameorexperimentnumber)
IntheuserIDeld,enterthecontentofyourchoice(max15characters)
3.Export
• ScantheQRcodefromamobiledevicetoinstantlyretrievethereport.
• ClickontheexportbuttontosavethereportonaUSBkey.
4.Automaticarchiving
The dispense report icon on the home screen will automatically disappear after 5 minutes of
inactivity.Eachdispensereport,whetherconsultedornot,isautomaticallyarchivedandcanbe
retrievedanytimebygoinginthehistoryreportsectionavailableintheinformationmenu.
Dispense
report

Maintenance and settings 9
Maintenance & settings
Milli-Q®IQ Element unit settings
ThismenuallowsausertocongureallparametersspecictoMilli-Q®IQElementunitsandPODs.
TheseareuniquetotheMilli-Q®IQElementunit/PODthatisbeingusedtoinputthevalues.
ToduplicateMilli-Q®IQElementunit/PODparameters,theaction(s)shouldberepeatedonallotherPODs.
Milli-Q IQ Element Name
Thiscanbepersonalized.Clickonthetextboxandinputuptoamaximumof8characters.
Screen brightness
Adjusttothepreferredbrightnessfrom1to7usingthearrowsorclickontheboxtoaccessthe
keypadandtype-inthevalue.
Sound volume
EachMilli-Q®IQElementunitcanemitasoundwhenalerts/alarmsaretriggered.Thiscanbeactivated
ordeactivatedusingthesliderbutton.Thesoundcanbeadjustedtothedesiredvolumebyusingthe
arrowsorclickontheboxtoaccessthekeypadandtype-inthevalue.Bydefault,thesoundisdeactivated.
Flowmeter offset
The owmeter has been calibrated in order to achieve volume precision of +/- 5%. In case of an
obviousmistakeoftheowmeterbroughtoutwithanexternalcalibrateddevice,thissettingprovides
thelabmanager(bydefaultpassword:PASS)theabilitytoadjustitbyusinganoffsetfunction.
Adjusttheoffsetbyusingthearrowsorclickontheboxtoaccessthekeypadandtypeinthevalue.
Togainbacktheoriginalcalibrationsetting,setthevaluebackto0.
Distribution depressurization
Having a Milli-Q® IQ Element unit installed
involvedtheuseofthefootpedaltodepressurize
theMilli-Q®IQ7000systemorthedistribution
sideoftheMilli-Q®IQ7003/7005/7010/7015
system.
Thedistributiondepressurizationisavailableby
goingin“MAINTENANCE”,“Depressurization”.
This feature is not necessary during nor-
mal system operation. Please refer to the
Milli-Q® IQ 7000 system or Milli-Q®IQ
7003/7005/7010/7015 system user manuals
formoreinformation.
Pressthe“Exitmaintenance”buttontore-pres-
surizethedistribution.

Maintenance and settings 10
Consumables kit replacement standard operating procedure
1:UnpacktheIPAKQuantaICP®Cartridge.Writetoday’sdateonthesmallstickeratthebottom.
2:RemovetheMilli-Q®IQElementunitfrontcov-
e r.
3:ClickontheMenubuttontoaccessthe
MAINTENANCEsection.
4:Clickon“Installconsumables”.
5: Depending upon the system type that feeds
theMilli-Q®IQElementunit,eitherclickon“IPAK
Meta-IPAKQuanta-IPAKQuantaICP-
Optimizer”or“IPAKQuanta-IPAKQuantaICP-
Optimizer-installation”.
6:DependinguponthesystemtypethatfeedstheMilli-Q®IQElementunit,younowseeeitherof
bothscreensshownbelow.Besuretomeetthepre-requisiteaheadofpressing“Next”.
Important:Inadditiontothe20L(Milli-Q®IQ7003/7005/7010/7015)or30L(Milli-Q®IQ7000)inthetank
requiredtoproceedthewizard,additional20LwillbenecessaryfortheOptimizer™LWnallterrinsing(step
21).IfyourMilli-Q®IQElementunitisfedbyaMilli-Q®IQ7003/7005/7010/7015anda25Lcapacitytank,you
willneedtowaitseveralhoursforthetanktorellinordertonishtheproceduredependingonsystemowrate
capacity.

Maintenance and settings 11
7:ScantheRFIDcard(deliveredintheMilli-Q®IQElementconsumablekit)onthee-Suretagto
registertheinstallationdate,lotnumberandcatalognumberdetails.Youcanalternativelymanually
typeintheinformation.Clickon“Next”tocontinue.
8:Depressurizeusingthefootpedal.Clickon“Next”
tocontinue.
9:ReplacetheIPAKQuanta®.Ifapplicable(Mil-
li-Q®IQ7000),alsoreplacetheIPAKMeta®.
Note:MoredetailsabouttheIPAK
Quanta® and IPAK Meta® in the IQ 7000 or
IQ7003/7005/7010/7015usermanuals.
10:OncetheIPAKQuanta®-andifapplicabletheIPAKMeta®-is/arereplaced,clickon“Next”.

Maintenance and settings 12
11: The end of the dispenser tubing still being
overasink,clickon“Next”. 12:Clickon“Next”.
13: Remove the old Optimizer LW™ nal lter.
Wipethewatergoingoutfromthetubings.
14:InstalltheOptimizer™by-pass.Youwillnor-
mallynditinalittleplasticbagattachedtothe
producttubing.
14bis:Mindthewaytheconettingisoriented
onthephotographbelow.Thenarrowcircleofthe
conemustbeorientedtowardtheby-pass.Same
logicfortheupperconetting.
15:RemovetheoldIPAKQuantaICP®.

Maintenance and settings 13
16:InstallthenewIPAKQuantaICP®.Donotforgettotightenboththeknobstosecurethecar-
tridge.
17:Clickonthe“Startrinsing”button. 18:Usethefootpedaltoproceed.
19:Wait10minutefortherinsingtobecomplete
andthehomescreentobedisplayed.Depressur-
izethedistributionasdescribedpage9.
20:RemovetheOptimizer™by-pass.Keepitina
safelocationforthenextreplacement.

Maintenance and settings 14
21:Removethe OptimizerLW™nal lterfrom
itspackagingbagandfastenboththenutsdeliv-
eredinaseparatebag.
22:InstallthenewOptimizerLW™nallter.Re-
fertostep14bisforthecorrectwayofconnect-
ingboththeconeshapettings.
23:Pressthe “Exit maintenance” button on the
HMI.
24:Fromthehomescreen,performavolumetric
rinsingof20L(refertotheQuickStartchapter).
25: Purge the air out of the IPAK Quanta®ICP
cartridge(refertothededicatedchapter)andout
of the Optimizer LW™ nal lter by temporary
looseningitstheuppernut.
26: Reinstallthe Milli-Q® IQ Element unit front
cover.Congratulations,youareset!

Maintenance and settings 15
Consumables tracability
Theconsumabledataregistrationisincludedinthe“Consumableskitreplacementstandardoperating
procedure”previouslydescribed(step7,page11).Youcanre-registertheconsumableslotnumber
bygoingin“MAINTENANCE”,“Installconsumables”andeither“Optimizer”and/or“IPAKQuantaICP”:
Inboth“Optimizer”and “IPAKQuantaICP”,thecatalognumberisthesame:“IPAKICPK1”. Thelot
numberisthesameforagivenMilli-Q®IQElementconsumablekit.
Example:In“Optimizer”youcanseethefollowingscreen:
YoucaneithermanuallytypeinorfetchthedatabyscanningtheRFIDcardonthee-Suretagreader.
Ifyoumanuallytypeinthedata,replace“XXXXXXXXXXXX”bytheactuallotnumberofthekit.You
canndtheserialnumberwrittenonthelabelofthekitbox.Theexactsamedatahastobetyped
in/scannedin“IPAKQuantaICP”.

Maintenance and settings 16
Purging air from the IPAK Quanta ICP®cartridge
1:Makesureyouarenotinmaintenancemode.
Otherwise, press the “Exit maintenance” button
togobacktothehomescreen.
2:Get a screwdriver with a very thin shaft and
smallhead.Youcanalternativelyuseamechani-
calpencilprovidedthattheleadisretracted.
3:Locatethesmallholeonthetoppartofthe
IPAKQuantaICP®cartridge.
3:GentlyinsertthescrewdriverintotheIPAK
QuantaICP®cartridge.Thiswillopenasmall
ventthatwillexpelanyairintheIPAKQuanta
ICP®cartridge.
Important:BeverycarefulwhenpushingthetipofthescrewdriverintotheventholeoftheIPAK
QuantaICP®cartridge.Theventholeonlyneedstobeopenedaverysmallamount.Weargoggles.

Maintenance and settings 17
Icons
Icon Meaning/Function Icon Meaning/Function
Recirculation Dispensing
Volumetricdispensing Backtomainmenu
Startdispense Stopdispense
1
Alarmwithnumberofactive
alarm(s) Alert
Home Menu
Storagetank Systemmanagerloggedin
MassstorageUSBconnected Ethernet-LANstatusconnected
SliderON SliderOFF
Back Calendarentry
ProductionUnitproducing
water ProductionUnitstandby
ProductionUnitblocked ProductionUnitmaintenance
ProductionUnitMaintenance
exit

18
REQUIREMENTS AND SPECIFICATIONS
System specications
Milli-Q IQ Element water quality
Parameter Value or range
Resistivity 18.2Mohm.cm@25°C
TotalOrganicCarbon(TOC) ≤5ppb
Flowrate upto1.5L/min
Notes :
• ThesespecicationsarevalidforaMilli-QIQElementUnitfedbywaterproducedbyaMilli-Q®
IQ 7003/7005/7010/7015 system or by a Milli-Q® IQ 7000 system with a resistivity at 18.2
Mohm.cmandaTOCbelow5ppb.
• Somespecicationsmayonlybeachievedafterstart-upandonlyifthesystemhasbeenrinsed
correctly.
Communication
EachMilli-Q®IQElementunithasalargeHDcapacitive5”touchscreen(Resolution:800*480)
thatallowscontrolandmonitoringofthesystem.
USB
TheMilli-Q®IQElementunithasabuilt-inUSBportthatoffersthepossibilitytodownloadthe
watersystemusermanual orto exportthesystemdataand/orhistory.TheHost interfaceis
compliantwiththeUSB2.0High-speedstandard.
USBkeysonlyworkwhenformattedFAT32.NTFSformatisnotcompatible.
Ethernet
WhenconnectedthroughanEthernetprotocol,thedisplayinterfacecanbeaccessedremotely
usinginternetwebbrowsers.
Forbestbrowsingperformance,therecommendedbrowserisChrome®.
RFID (casewithembeddedradiofeature)
Useonlythebuilt-inantennasupplied.Unauthorizedmodicationoftheantennaoruseofun-
authorizedaccessoriesmightdamagethesystemandrenderitnon-compliantwiththeEURED
directiveand/orFCCregulations.
EU
WecertifythattheseLabWaterSystemsaredesignedandmanufacturedinapplicationofthe
followingEuropeanCouncildirectives:
DIRECTIVE2014/53/EUOFTHEEUROPEANPARLIAMENTANDOFTHECOUNCILof16April2014
ontheharmonisationofthelawsoftheMemberStatesrelatingtothemakingavailableonthe
marketofradioequipmentandrepealingDirective1999/5/EC.Standardstowhichconformity
isdeclared as applicable are the following. Electromagnetic compatibility and Radiospectrum
Matters(ERM)testsaccordingtostandards:ETSIEN300330.