Milwaukee MA872 User manual

INSTRUCTION MANUAL
SATISFACTION
GUARANTEED
MA872
Digital Fructose
Refractometer

All rights are reserved. Reproduction in whole or in part is
prohibited without the written consent of the copyright owner,
Milwaukee Instruments Inc., Rocky Mount, NC27804USA.
THANK YOU for choosing Milwaukee Instruments!
This instruction manual will provide you the necessary
information for correct use of the meters.

3
TABLE OF CONTENTS
1. FUNCTIONAL DESCRIPTION.................................................................................4
2. GENERAL DESCRIPTION........................................................................................6
3. SPECIFICATIONS.........................................................................................................7
4. PRINCIPLE OF OPERATION...................................................................................8
5. MEASUREMENT GUIDELINES.............................................................................9
6. CALIBRATION PROCEDURE................................................................................ 10
7. MEASUREMENT PROCEDURE.............................................................................12
8. MAKING A STANDARD % BRIX SOLUTION..................................................13
9. CHANGING TEMPERATURE UNIT.................................................................... 14
10. ERROR MESSAGES............................................................................................... 15
11. BATTERY REPLACEMENT ....................................................................................17
CERTIFICATION.............................................................................................................. 18
RECOMMENDATION.................................................................................................... 18
WARRANTY...................................................................................................................... 18

4MA872 Digital Fructose Refractometer
1. FUNCTIONAL DESCRIPTION
Display
C
F
G
B
A
D
H
E
A. BATTERY STATUS ICON
BLINKS WHEN LOW BATTERY CONDITION DETECTED
B. MEASUREMENT IN PROGRESS TAG
C. SETUP: FACTORY CALIBRATION TAG
D. CAL: CALIBRATION TAG
E. PRIMARY DISPLAY
DISPLAYS MEASUREMENT AND ERROR MESSAGES
F. AUTOMATIC TEMPERATURE COMPENSATION
BLINKS WHEN TEMPERATURE EXCEEDS  °C /  °F
RANGE
G. TEMPERATURE UNITS
H. SECONDARY DISPLAY
DISPLAYS TEMPERATURE MEASUREMENTS;
WHEN BLINKING, TEMPERATURE HAS EXCEEDED OPERATION
RANGE:  °C /  °F

FUNCTIONAL DESCRIPTION 5
Front Panel
MA872
Digital Fructose Refractometer
0 to 85 %Mass
A E F G
B C D
A. LIQUID CRYSTAL DISPLAY LCD
B. READ KEY USER MEASUREMENT
C. ZERO KEY USER CALIBRATION
D. ON/OFF
E. PRIMARY DISPLAY
F. SECONDARY DISPLAY
G. STAINLESS STEEL SAMPLE WELL AND PRISM
Bottom
H
I
H. BATTERY COVER
I. BATTERY COMPARTMENT

6MA872 Digital Fructose Refractometer
2. GENERAL DESCRIPTION
Significance of Use
Thank you for choosing Milwaukee. This instruction manual will
provide you the necessary information for correct use of the meter.
The MA872 is an optical instrument that employs the measurement
of refractive index to determine the % Fructose in aqueous
solutions. The method is both simple and quick. Samples from
expressed, reconstituted or concentrated juice are measured
after a simple user calibration with deionized or distilled water.
Within seconds the instrument measures the refractive index of
the sample and converts it to % by weight concentration units.
The MA872 digital refractometer eliminates the uncertainity
associated with mechanical refractometers and is easily portable
for measurements in the plant.
The measurement technique and temperature compensation
employ methodology recommended in the ICUMSA Methods Book
(Internationally recognized body for Sugar Analysis).
Temperature (in °C or °F) is displayed simultaneously with the
measurement on the large dual level display along with icons for
Low Power and other helpful message codes.
Key features include:
yDual-level LCD
yAutomatic Temperature Compensation (ATC)
yEasy setup and storage
yBattery operation with Low Power indicator (BEPS)
yAutomatically turns o after 3 minutes of non-use.
Remove the instrument from the packing materials and examine
carefully to ensure no damage has occurred during shipping. If
any damage has occurred, notify your Dealer.
Each MA872 instrument is supplied with:
y9 V battery
yInstruction manual
Note: Save all packing material until you are sure that the
instrument functions correctly. A defective instrument must be
returned in its original packing.

SPECIFICATIONS 7
3. SPECIFICATIONS
Range 0 to 85% 0 to 80 °C (32 to 175 °F)
Resolution 0.1% 0.1 °C (0.1 °F)
Accuracy ± 0.2% ± 0.3 °C (± 0.5 °F)
Light Source Yellow LED
Measurement Time Approximately 1.5 seconds
Minimum Sample Volume 100 L (cover prism totally)
Sample Cell SS ring and flint glass prism
Temperature
Compensation
Automatic between 10 and 40 °C
(50 to 104 °F)
Case Material ABS
Enclosure Rating IP 65
Battery Type/Life 1 x 9 volt AA batteries / 5000 readings
Auto-Shut o After 3 minutes of non-use
Dimensions 19.2 x 10.2 x 6.7 cm (7.5 x 4 x 2.6”)
Weight 420 g (14.8 oz.)

8MA872 Digital Fructose Refractometer
4. PRINCIPLE OF OPERATION
The Fructose determination is made by measuring the refractive
index of a solution. Refractive Index is an optical characteristic of
a substance and the number of dissolved particles in it. Refractive
Index is defined as the ratio of the speed of light in empty space
to the speed of light in the substance. A result of this property is
that light will “bend”, or change direction, when it travels through
a substance of dierent refractive index. This is called refraction.
When passing from a material with a higher to lower refractive
index, there is a critical angle at which an incoming beam of
light can no longer refract, but will instead be reflected o the
interface. The critical angle can be used to easily calculate the
refractive index according to the equation:
sin (θcritical) = n2/ n1
Where n2is the refractive index of the lower-density medium; n1is
the refractive index of the higher-density medium.
i
r
n1
n2
= angle of incidence
= angle of refraction
n1 , n2 - refractive index
Refraction Critical Angle Total Internal Reflection
r
i
i critical
i
r
n2
n1
n2
i
i critical
i critical
< >
=
n1
θ
θ
θ
θ
θ θ
θ
θ
θ
θ θ
θ θ
In the MA872, light from an LED passes through a prism in contact
with the sample. An image sensor determines the critical angle
at which the light is no longer refracted through the sample.
TheMA872 automatically applies temperature compensation to
the measurement and converts the refractive index of the sample
to Fructose concentration in units of percent (by weight).

MEASUREMENT GUIDELINES 9
Prism
Lens
L
inear Image Sensor
Sample
Shadow
Led
Sample Well
5. MEASUREMENT GUIDELINES
yHandle instrument carefully. Do not drop.
yDo not immerse instrument under water.
yDo not spray water to any part of instrument except the
“sample well” located over the prism.
yThe instrument is intended to measure sugar solutions. Donot
expose instrument or prism to solvents that will damage it.
This includes most organic solvents and extremely hot or cold
solutions.
yParticulate matter in a sample may scratch the prism. Absorb
sample with a soft tissue and rinse sample well with deionized
or distilled water between samples.
yUse plastic pipettes to transfer all solutions. Do not use
metallic tools such as needles, spoons or tweezers as these
will scratch the prism.

10 MA872 Digital Fructose Refractometer
6. CALIBRATION PROCEDURE
Calibration should be performed daily, before measurements are
made, when the battery has been replaced, or between a long
series of measurements.
1. Press the ON/OFF key, then release. Two instrument test
screens will be displayed briefly; an “all segment” screen
followed by the percentage of remaining battery life. When
LCD displays dashes, the instrument is ready.
2. Using plastic pipettes, fill the sample well with distilled or
deionized water.
Note: If the ZERO sample is subject to intense light such as
sunlight or another strong source, cover the sample well with
your hand or other shade during the calibration.

CALIBRATION PROCEDURE 11
3. Press the ZERO key. If no error messages appear, your unit is
calibrated. (For a description of error messages see "ERROR
MESSAGES" section).
Note: The 0.0 screen will remain until a sample is measured or
the power is turned o.
4. Gently absorb the ZERO water standard with a soft tissue. Use
care not to scratch the prism surface. Wipe o the surface
completely. The instrument is ready for sample measurement.
Note: If instrument is turned o the calibration will not be lost.

12 MA872 Digital Fructose Refractometer
7. MEASUREMENT PROCEDURE
Verify the instrument has been calibrated before taking
measurements.
1. Wipe o prism surface located at the bottom of the sample well.
2. Using plastic pipettes, drip sample onto the prism surface.
Fill the well completely.
Note: If the temperature of the sample diers significantly from
the temperature of the instrument, wait approximately 1 minute
to allow thermal equilibration.
3. Press the READ key. Measurement is displayed in units of % by
weight (w/w).
Note: The last measurement value will be displayed until
the next sample is measured or the instrument is turned o.
Temperature will be continuously updated.
Note: The ATC tag blinks and automatic temperature
compensation is disabled if the temperature exceeds the
10‑40°C / 50‑104 °F range.

MAKING A STANDARD % FRUCTOSE SOLUTION 13
4. Remove sample from the sample well by absorbing with a
soft tissue.
5. Using plastic pipettes, rinse prism and sample well with
distilled or deionized water. Wipe dry. The instrument is ready
for the next sample.
8. MAKING A STANDARD % FRUCTOSE SOLUTION
To make a Fructose Solution, follow the procedure below:
yPlace container (such as a ZERO glass vial or dropper bottle
that has a cover) on an analytical balance.
yTare the balance.
yTo make an X Fructose solution weigh out X grams of high
purity Fructose (CAS #: 57-48-7) directly into the container.
yAdd distilled or deionized water to the container so the total
weight of the solution is 100g.
Note: Solutions above 65% need to be vigorously stirred or shaken
and heated in a water bath to roughly 40 °C (104  °F). Remove
solution from bath when fructose has dissolved. Cool completely
before use. The total quantity can be scaled proportionally for
smaller containers but accuracy may be sacrificed.
Example with 25% Fructose:
%g Fructose g Water Total
25 25.00 75.000 100.000

14 MA872 Digital Fructose Refractometer
9. CHANGING TEMPERATURE UNIT
To change the temperature measurement unit from Celsius to
Fahrenheit (or vice versa), follow this procedure.
1. Press and hold the ON/OFF key continuously for aproximately
15 seconds. The LCD will display the “all segment” screen
followed by a screen with the model number on the primary
display and the version number on the secondary display.
Continue pressing the ON/OFF key.
15 seconds
2. While continuing to hold the ON/OFF key, press the ZERO key.
The temperature unit will change from °C to °F or vice versa.
°C or °F

ERROR MESSAGES 15
10. ERROR MESSAGES
Error Code Description
Err
General failure. Cycle
power to instrument. If
instrument still has error,
contact Milwaukee.
LO Top display
Sample is reading lower
than the 0 % standard
used for meter calibration.
HI Top display Sample exceeds maximum
measurement range.
LO Top display
CAL segment ON
Wrong calibration used
to zero instrument. Use
deionized or distilled
water. Press Zero.
HI Top display
CAL segment ON
Wrong calibration used
to zero instrument. Use
deionized or distilled
water. Press Zero.
t LO Top display
CAL segment ON
Temperature exceeds ATC
low limit (10 °C) during
calibration.
t HI Top display
CAL segment ON
Temperature exceeds ATC
high limit (40 °C) during
calibration.
Air Prism surface insuiciently
covered.
ELt
Too much external light
for measurement. Cover
sample well with hand.
nLt LED light is not detected.
Contact Milwaukee.

16 MA872 Digital Fructose Refractometer
Battery segment
blinking
<5% of battery life is
remaining.
Temperature values
are blinking
0.0°C or 80.0°C
Temperature
measurement out
of sampling range
(0.0 to 80.0°C).
ATC segment
blinking
Outside temperature
compensation range
(10 to 40°C).
SETUP segment
blinking
Factory calibration lost.
Contact Milwaukee.

BATTERY REPLACEMENT 17
11. BATTERY REPLACEMENT
To replace the instrument’s battery, follow these steps:
yTurn the instrument OFF by pressing the ON/OFF key.
yTurn instrument upside down and remove the battery cover
by turning it counterclockwise.
yExtract the battery from its location.
yReplace with fresh 9V battery making certain to observe polarity.
yInsert the back battery cover and fasten it by turning clockwise
to engage.

18 MA872 Digital Fructose Refractometer
MANMA872 09/20
CERTIFICATION
Milwaukee Instruments conform to the CE European Directives.
RoHS
COMPLIANT
Disposal of Electrical & Electronic Equipment. Do not treat this product
as household waste. Hand it over to the appropriate collection point for
the recycling of electrical and electronic equipment.
Disposal of waste batteries. This product contains batteries. Do not
dispose of them with other household waste. Hand them over to the
appropriate collection point for recycling.
Please note: proper product and battery disposal prevents potential
negative consequences for human health and the environment. For
detailed information, contact your local household waste disposal
service or go to www.milwaukeeinstruments.com (US only) or
www.milwaukeeinst.com.
RECOMMENDATION
Before using this product, make sure it is entirely suitable for your specific
application and for the environment in which it is used. Any modification
introduced by the user to the supplied equipment may compromise the
meter’s performance. For your and the meter’s safety do not use or store
the meter in hazardous environment. To avoid damage or burn, do not
perform any measurement in microwave ovens.
WARRANTY
This instrument is warranted against defects in materials and
manufacturing for a period of 2 years from the date of purchase.
Electrodes and Probes are warranted for 6 months. This warranty is
limited to repair or free of charge replacement if the instrument cannot
be repaired. Damage due to accidents, misuse, tampering or lack of
prescribed maintenance is not covered by warranty. If service is required,
contact your local Milwaukee Instruments Technical Service. If the
repair is not covered by the warranty, you will be notified of the charges
incurred. When shipping any meter, make sure it is properly packaged for
complete protection.

Milwaukee Instruments reserves the right to make improvements in design,
construction and appearance of its products without advance notice.

THANK YOU FOR CHOOSING
Sales and Technical Service Contacts:
Milwaukee Electronics Kft.
Alsó-kikötő sor 11C
H-6726 Szeged - HUNGARY
tel: [phone]
fax: [phone]
www.milwaukeeinst.com
e-mail: [e-mail]
Milwaukee Instruments, Inc.
2950 Business Park Drive
Rocky Mount, NC 27804 USA
tel: [phone]
fax: [phone]
www.milwaukeeinstruments.com
e-mail: [e-mail]
MANMA872