Organomation S-EVAP 12060 User manual

Solvent Evaporation System
Model 12060, 12090 & 12008
Digital Time and Control System
INSTRUCTION MANUAL
ORGANOMATION ASSOCIATES INC.
266 RIVER ROAD WEST
BERLIN, MA 01503
U. S. A.
Tel: [phone] Fax: [phone]
S-EVAP-RB
TM

TABLE OF CONTENTS
S-EVAP-RB TM
Introduction
Instrument Items Shipped 4
Instrument Description 7
Glassware sets 5
Installation
Location 8
Bath Setup 8
Instrument Setup 13
Safety Considerations - Read before operation 18
Operation
Instrument Control Identification 17
Planning and Preparation 19
Type Z Purge Intrinsically Safe Bath Option 9
Bath Operation 20
Instrument Operation 25
Optimization 23
Maintenance and Cleaning 26
Trouble Shooting 28
Technical Information
Service and Returns 29
Shipping - Claims for damage or shortage 30
Specifications 31
Wiring Diagrams 32
Contacting Organomation and its Representatives 29
Product designs are subject to change without notice
Printed in U. S. A.
V15.1

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INTRODUCTION
S-EVAP-RB TM
Items Shipped
Carefully check the contents of all cartons received for damage which may have occurred in
transit. Retain all cartons and packaging materials until all components have been checked
against the packing slip, the component list below, and the equipment has been assembled and
tested. Contact Organomation Associates Inc. immediately if any damage or discrepancies are
found.
Your shipment should contain one or more of the instruments and / or glass sets shown below.
Option codes are listed on the next page.
Instruments Only (Glassware Sold Separately)
8 Position S-EVAP, 4.5” deep x 12” Diameter Bath - 250 ML RB Flasks
10 Position S-EVAP, 4.5” deep x 16” Diameter Bath - 250 ML RB Flasks
8 Position S-EVAP, 4.5” deep x 16” Diameter Bath - 500 ML RB Flasks
Flow meter Assembly with Mounting Bracket & Tubing.
0-3500 CCM for condenser water supply.
OA-SYS Water Bath 1100W, Model 12060
OA-HEAT Water Bath 1400W, Models 12090, 12008
Thermometer 0 - 100º Celsius, 6” long, 4.5” deep baths (Optional)
Water Services Tube Assembly includes:
SS water inlet Tube 3/8” (mm) OD, PVC water outlet tube 1/2” (12mm) OD,
and Polypropylene extendable jacket.
Ball Driver, 5/32” x 9” Long.
Manual for all S-EVAP-RB models.
SS Cover disk assembly, includes: Hole covers (5 or 8, subject to Model), collar, and tear
drop handles, 3.0” hole size for 12” diameter and 3.875” hole size for 16” diameter bath.
Cat #
12060
12090
12008
P2121
B2110
B2104
NA1110
- - - -
V11437
- - - -
- - - -
S-EVAP and OA-HEAT are Trademarks of Organomation

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INTRODUCTION
S-EVAP-RB TM
Glassware Sets - Each Set includes the following:
125 ML Glassware Set, includes:
 GP3215 (Quantity 2): Standard flat bottom flask 125 ml, for 24/40 joint
 GP2212: Hopkins condenser 375mm with side arm for individual collection
flask, for 24/40 joint
 GA2273: Glassware clip for 24/40 joint
250 ML Glassware Set, includes:
 GP3216 (Quantity 2): Standard flat bottom flask 250ml, for 24/40 joint
 GP2212: Hopkins condenser 375mm with side arm for individual collection
flask, for 24/40 joint
 GA2273: Glassware clip for 24/40 joint
500 ML Glassware Set, includes:
 GP2214 (Quantity 2): Flat bottom flask 500ml, for 24/40 joint
 GP2212: Hopkins condenser 375mm with side arm for individual collection
flask, for 24/40 joint
 GA2273: Glassware clip for 24/40 joint
Adapter Rings, 3.875 inch
Allow 250 ml flasks to be used in instruments designed to support 500 ml flasks
Adapter Rings, 3.0 inch
Allow 125 ml flasks to be used in instruments designed to support 250ml flasks
Cat #
GS2161
GS2162
GS2163
XA2284
XA2286

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INTRODUCTION
S-EVAP-RB TM
Option Codes and additional items shipped
The following list contains option codes and items which may have been shipped in
conjunction with the standard parts shown on the previous pages. Please check your packing
list and order information carefully to determine if these items are included in your shipment.
Your shipment may contain the following optional items:
Description
Nitrogen manifold option, additional parts include: Gas manifold (5, 8 or 10
position subject to Model) with quick disconnect auto shutoff fittings, gas flow
meter (0-10 LPM), Corrugated tubing (8 or 10 tubes, subject to model) with red
caps, Manifold to flow meter tube, and 1/4” ID x 3/8” OD PVC gas connection line
5 feet long. See specific glass set for additional glass items.
Vacuum manifold (5,8 or 10 position subject to Model) tubing & connectors
OA-SYS water bath has been modified for the Type-Z Purge Intrinsically Safe bath
option. Additional parts include: differential pressure gauge, mounting bracket,
and tubing.
OA-SYS water bath is wired as a 240 Volt unit.
Option
-N
-V
-Z
-2

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INTRODUCTION
S-EVAP-RB TM
Instrument Description
The S-EVAP-RB Solvent Evaporation System is designed for general evaporation and /
or concentration of analytical or environmental samples in a variety of glassware
configurations to meet the needs of specific methods under controlled and reproducible
conditions.
The S-EVAP-RB system features rapid solvent evaporation with solvent vapor recovery.
Solvent recoveries can exceed 96% by volume under ideal conditions. The system may be
used with cold tap water or a recirculating chiller system. The digital controlled water bath
provides even uniform heating without scaulding final samples. The parallel water manifold
system provides even cooling water to each of the condensers. The rotary water manifold
allows unlimited instrument rotation for front loading without condenser tubing wrapping about
the instrument.
Figure 1

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INSTALLATION
S-EVAP-RB TM
Location
The S-EVAP-RB evaporator system should be located on a bench top or in a chemical
fume hood if hazardous or flammable materials and solvents are to be used. The location
should provide the necessary support services for the instrument. These include electrical
power (required for water bath), cold water, and drain. Please review the Specifications
Section for further information.
Bath Setup
1. Position the bath on a stable flat surface such as a lab bench or in a chemical fume hood.
2. Turn the bath rocker switch to the “OFF” position.
3. Turn the heat switch to the center “OFF” position.
4. Plug the bath electrical cord into a 3 wire grounded electrical outlet rated for 110-120
VAC, 50-60 Hz, single phase, 15 amps.
Optional 220 VAC baths are clearly marked and should be plugged into a three wire
grounded electrical outlet rated for 220-240 VAC, 50-60 Hz, single phase, 15 amps.

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INSTALLATION
S-EVAP-RB TM
Bath Setup (Continued)
6. Type-Z Purge Intrinsically Safe Bath option - If you do not have this option, please
proceed to the next section. Procedur es for operating this system may be found
in the Operation Section. Quick start instructions are posted on the front of the bath.
Please refer to Figure 2 below for parts list and installation.
A. Install the Type Z Purge Gauge Assembly to the rear of the bath as shown. The
bracket attaches to the rear of the bath and is held in place by a 6-32 x 1/4” screw
on the shoulder spacer and by a 1/4” bulkhead hex nut on the gas inlet fitting.
B. Connect the small white silicone tube attached to the gauge to the gas inlet fitting
using the compression nut provided.
C. Attach the filter with 5 foot tube to the plastic elbow fitting located at the base of
the bath or control box. Insert the filter into the fitting and tighten the nut.
Connect the tube to a clean gas source.
D. Test the system by turning on the gas flow to the Z Purge System. Adjust the
gas flow until the gauge reads 0.3 inches water pressure.
WARNING - If this unit is located in a hazardous area where volatile fumes are present,
the Z-Purge System must be activated for a minimum of 10 minutes prior
to activation of bath power. Please review the Safety and Operations
sections.
Figure 2
Side mount control box (included on some models) not shown here.

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INSTALLATION
S-EVAP-RB TM
Bath Setup (Continued)
7. Flow meter assembly - Provided with all S-EVAP Systems. If an OA-SYS bath was
purchased without an S-EVAP instrument, proceed to the next section.
A. Units without control box
Attach the flow meter to the bracket mounted on the bath with the two 10/32 x
1/2” screws provided. The meter should be positioned with the scale facing
forward.
B. Units with control box
Attach the flow meter and bracket assembly onto the left rear corner of the
control box with the two 10/32 x 1/2” screws provided. The meter should be
positioned with the scale facing forward.
C: Connect the clear 1/4” ID x 3/8” OD tube to a cold water source (tap or chiller).
Source should be capable of producing 3.5 LPM (1 GPM) and being regulated to
30 psig maximum. If the source is in excess of 30 psig, then Organomation
part # XA0631 Pressure Reducing Regulator will be required.
Figure 3