PerkinElmer DSC 6000 Assembly Instructions

DSC 6000
Installation and Hardware
Guide
THERMAL ANALYSIS

Release History
Part Number Release Publication Date
09931393 C January 2018
Any comments about the documentation for this product should be addressed to:
User Assistance
PerkinElmer, Inc.
710 Bridgeport Avenue
Shelton, Connecticut 06484-4794
U.S.A.
Or contact: http://www.perkinelmer.com/contactus/
Notices
The information contained in this help file is subject to change without notice.
Except as specifically set forth in its terms and conditions of sale, PerkinElmer makes no
warranty of any kind with regard to this help file, including, but not limited to, the implied
warranties of merchantability and fitness for a particular purpose.
PerkinElmer shall not be liable for errors contained herein for incidental consequential damages in
connection with furnishing, performance or use of this material.
Copyright Information
This help file contains proprietary information that is protected by copyright.
All rights are reserved. No part of this file may be reproduced in any form whatsoever or translated into
any language without the prior, written permission of PerkinElmer, Inc.
Copyright © 2018 PerkinElmer, Inc.
Trademarks
Registered names, trademarks, etc. used in this help file, even when not specifically marked as such,
are protected by law.
PerkinElmer is a registered trademark of PerkinElmer, Inc.
Pyris is a trademark of PerkinElmer, Inc.
Microsoft and Windows are registered trademarks of Microsoft Corporation in the United States and
other countries.

Contents
Introduction...............................................................................................5
Pyris Installation ............................................................................................... 6
Safety and Regulatory Information...........................................................7
Symbols Used in Online Help ............................................................................. 8
Notes, Cautions and Warnings..................................................................... 8
Symbols Used on the Instruments.....................................................................11
Electrical Warnings...........................................................................................12
General Warning..............................................................................................14
Electromagnetic Compatibility (EMC).................................................................15
Europe......................................................................................................15
South Korea..............................................................................................15
United States (FCC)...................................................................................15
Electrical Safety ...............................................................................................16
Pollution Degree 2.....................................................................................16
WEEE Instructions for PerkinElmer Products ......................................................17
Prepare the Laboratory............................................................................19
Prepare the Laboratory.....................................................................................20
Electrical Requirements..............................................................................20
Environmental Requirements......................................................................20
Purge Gas and Pneumatic Supply ...............................................................21
Space Requirements..................................................................................21
Install Multiple Analyzers ........................................................................23
Install Multiple Analyzers ..................................................................................24
Install a DSC 6000 ...................................................................................27
Safety Precautions for the DSC 6000.................................................................28
Decontamination and Cleaning..........................................................................31
Decontamination .......................................................................................31
Cleaning the Instrument ............................................................................31
General Laboratory Safety..........................................................................31
DSC 6000 Warning Labels.................................................................................32
Warning Labels on the Upper Ring Around the Furnace................................32
Warning Labels on the Back of the DSC 6000..............................................34
Install a DSC 6000 ...........................................................................................36
Unpacking the DSC 6000..................................................................................37
Unpacking the DSC 6000............................................................................37
Unpacking the CryoFill LN2 Dewar..............................................................38
Set Up the DSC 6000 System Components.........................................................39
Select the Correct Voltage for the DSC 6000 ...............................................39
Connect the Purge Gas Supply to the DSC 6000 ..........................................41
Connect the Purge Gas and System Purge Gas Lines to the DSC 6000 ..........42
Connect the Cooling Device to the DSC 6000...............................................42
Connect the DSC 6000 System Components ......................................................48
Configure the DSC 6000 ...................................................................................49
Starting the Pyris Manager.........................................................................50
Calibrate the DSC 6000.....................................................................................51
DSC 6000 Hardware.................................................................................55
DSC 6000 ........................................................................................................56
Furnace and Sensor Design........................................................................56
Cooling .....................................................................................................57
Calibration of the DSC 6000..............................................................................58
Temperature Calibration ............................................................................58
Perform Indium and Zinc Runs...................................................................59

Perform a Peak Area with Onset Calculation ...............................................59
Performing a Temperature Calibration........................................................60
Heat Flow Calibration ................................................................................60
Operating Variables and Sample Handling.........................................................62
Temperature Range ..................................................................................62
Scanning Rate...........................................................................................62
Subambient Operation of the DSC 6000............................................................63
DSC 6000 Maintenance....................................................................................64
DSC 6000 Part Numbers...................................................................................65
Miscellaneous Part Numbers ......................................................................66
AS 8000 Autosampler...............................................................................67
AS 8000 Autosampler.......................................................................................68
Safety Precautions for the AS 8000...................................................................70
How the AS 8000 Autosampler Works...............................................................71
Autosampler Work Cycle............................................................................71
Reduced Time Cycle..................................................................................73
AS 8000 Autosampler Gripper Alignment...........................................................74
AS 8000 Sample Handling ................................................................................75
Sample Preparation...................................................................................75
Sample Pans.............................................................................................75
Sample Loading ........................................................................................75
Running a Play List with the AS 8000................................................................78
Troubleshooting ..............................................................................................82
Error Messages from the DSC 6000............................................................85
AS 8000 Autosampler Maintenance...................................................................86
Cleaning and Decontamination...................................................................86
Install a Reference Pan in a DSC 4000, DSC 6000, Pyris 6 DSC or Jade DSC
with AS 8000 Autosampler ...............................................................................87

Introduction

6 . DSC 6000 Installation and Hardware Guide
Pyris Installation
NOTE: If you are going to install multiple analyzers, or just want to install a universal serial
bus, see Install Multiple Analyzers before you begin to install an analyzer.
This user’s guide gives information on the installation of your PerkinElmer Thermal Analysis
System, and details about the operation and maintenance of the hardware. This information
can also be found in the Pyris Installation and Hardware Help provided with your Pyris
software.
Information on the operation of the Pyris software can be found in the software Help.
In general, the installation procedure consists of the following steps:
•Prepare the laboratory
•Unpack the thermal analysis system
•Set up the required system components (for example, purge gases, cooling supply, and
analyzer-specific items)
•Connect the system components
•Configure the analyzer
•Calibrate the analyzer

Safety and Regulatory
Information

8 . DSC 6000 Installation and Hardware Guide
Symbols Used in Online Help
Bold text refers to text that is displayed on the screen.
UPPERCASE text, for example ENTER or ALT, refers to keys on the computer keyboard. '+' is
used to show that you have to press two keys at the same time, for example, ALT+F.
All eight-digit numbers are PerkinElmer part numbers unless stated otherwise.
Notes, Cautions and Warnings
Three terms, in the following standard formats, are also used to highlight special
circumstances and warnings.
NOTE: Anote indicates additional, significant information that is provided with some
procedures.

Safety and Regulatory Information . 9
CAUTION
We use the term CAUTION to inform you about situations that could
result in serious damage to the instrument or other equipment. Details
about these circumstances are in a box like this one.
Caution (Achtung)
Bedeutet, daß die genannte Anleitung genau befolgt werden muß, um
einen Geräteschaden zu vermeiden.
Caution (Bemærk)
Dette betyder, at den nævnte vejledning skal overholdes nøje for at
undgå en beskadigelse af apparatet.
Caution (Advertencia)
Utilizamos el término CAUTION (ADVERTENCIA) para advertir sobre
situaciones que pueden provocar averías graves en este equipo o en
otros. En los recuadros como éste se proporciona información sobre
este tipo de circunstancias.
Caution (Attention)
Nous utilisons le terme CAUTION (ATTENTION) pour signaler les
situations susceptibles de provoquer de graves détériorations de
l'instrument ou d'autre matériel. Les détails sur ces circonstances
figurent dans un encadré semblable à celui-ci.
Caution (Attenzione)
Con il termine CAUTION (ATTENZIONE) vengono segnalate
situazioni che potrebbero arrecare gravi danni allo strumento o ad
altra apparecchiatura. Troverete informazioni su tali circostanze in un
riquadro come questo.
Caution (Opgelet)
Betekent dat de genoemde handleiding nauwkeurig moet worden
opgevolgd, om beschadiging van het instrument te voorkomen.
Caution (Atenção)
Significa que a instrução referida tem de ser respeitada para evitar a
danificação do aparelho.

10 . DSC 6000 Installation and Hardware Guide
WARNING
We use the term WARNING to inform you about situations that could
result in personal injury to yourself or other persons. Details about
these circumstances are in a box like this one.
Warning (Warnung)
Bedeutet, daß es bei Nichtbeachten der genannten Anweisung zu einer
Verletzung des Benutzers kommen kann.
Warning (Advarsel)
Betyder, at brugeren kan blive kvæstet, hvis anvisningen ikke
overholdes.
Warning (Peligro)
Utilizamos el término WARNING (PELIGRO) para informarle sobre
situaciones que pueden provocar daños personales a usted o a otras
personas. En los recuadros como éste se proporciona información sobre
este tipo de circunstancias.
Warning (Danger)
Nous utilisons la formule WARNING (DANGER) pour avertir des
situations pouvant occasionner des dommages corporels à l'utilisateur
ou à d'autres personnes. Les détails sur ces circonstances sont données
dans un encadré semblable à celui-ci.
Warning (Pericolo)
Con il termine WARNING (PERICOLO) vengono segnalate situazioni
che potrebbero provocare incidenti alle persone. Troverete
informazioni su tali circostanze in un riquadro come questo.
Warning (Waarschuwing)
Betekent dat, wanneer de genoemde aanwijzing niet in acht wordt
genomen, dit kan leiden tot verwondingen van de gebruiker.
Warning (Aviso)
Significa que a não observância da instrução referida poderá causar um
ferimento ao usuário.

Safety and Regulatory Information . 11
Symbols Used on the Instruments
Caution, hot surface.
Attention surface chaude.
Caution, risk of electric shock.
Attention, risque d'électrocution.
Caution
Documentation must be consulted to determine
the nature of the potential hazard and any actions which have to be
taken.
Attention
La documentation doit être consultée pour déterminer
La nature du risque potentiel et des actions qui doit être pris.
Caution – Cold surface
Attention, Surface froide
The following additional graphic symbols used on the instrument:
Indicates alternating current
Indicates the primary protective grounding terminal
Indicates the
off
position of the main power switch
Indicates the
on
position of the main power switch

12 . DSC 6000 Installation and Hardware Guide
Electrical Warnings
WARNING
AVERTISSEMENT
Connect the instrument to an AC line power outlet that has a
protective ground connection. To ensure satisfactory and safe
operation of the instrument, it is essential that the protective ground
conductor (the green/yellow lead) of the line power cord is
connected to true electrical ground. Any interruption of the protective
ground conductor, inside or outside the instrument, or disconnection
of the protective ground terminal may impair the protection provided
by the instrument.
Connectez l'instrument à une prise de courant de ligne AC qui a une
connexion de terre de protection. Pour assurer un fonctionnement
satisfaisant et sécurisé de l'instrument, il est essentiel que le
conducteur de terre de protection (le fil vert / jaune) du cordon
d'alimentation de la ligne soit connecté à une vraie terre électrique.
Toute interruption du conducteur de terre de protection, à l'intérieur
ou à l'extérieur de l'instrument, ou la déconnexion de la borne de
terre de protection peut nuire à la protection fournie par l'instrument.
WARNING
AVERTISSEMENT
Do not operate the instrument with any covers or parts removed.
Ne pas utiliser l'instrument avec des couvertures ou des pièces
retirees.
WARNING
AVERTISSEMENT
Do not attempt to make adjustments, replacements, or repairs to
this instrument except as described in this help file. Only a
PerkinElmer service representative should be permitted to service
the instrument.
N'essayez pas de faire des ajustements, des remplacements ou des
réparations à cet instrument, sauf comme décrit dans ce fichier
d'aide. Seul un représentant du service PerkinElmer devrait être
autorisé à servir l'instrument.

Safety and Regulatory Information . 13
WARNING
AVERTISSEMENT
Use only fuses with the required current rating and of the specified
type for replacement.
N'utilisez que des fusibles avec la note de courant requise et du type
spécifié pour le remplacement.

14 . DSC 6000 Installation and Hardware Guide
General Warning
The CryoFill system of PerkinElmer’s Differential Scanning Calorimeter emits a small amount of
nitrogen during normal operations. If your laboratory is not properly ventilated, the level of
oxygen in the laboratory may fall below the normal range. Please follow the applicable
laboratory ventilation standards to ensure that an appropriate oxygen level is maintained.
WARNING
AVERTISSEMENT
Do not operate the Differential Scanning Calorimeter in an enclosed
environment without adequate ventilation.
Ne faites pas fonctionner le Calorimètre à balayage différentiel dans
un environnement fermé sans ventilation adéquate.

Safety and Regulatory Information . 15
Electromagnetic Compatibility (EMC)
Europe
All information concerning EMC standards is in the Declaration of Conformity, and these
standards may change as the European Union adds new requirements.
PerkinElmer instruments have been designed and manufactured, having regard to the state
of the art, to ensure that:
•the electromagnetic disturbance generated does not exceed the level above which
radio and telecommunications equipment or other equipment cannot operate as
intended;
•it has a level of immunity to the electromagnetic disturbance to be expected in its
intended use which allows it to operate without unacceptable degradation of its
intended use.
South Korea
This device complies with MSIP (Ministry 0f Science, ICT, and Future Planning) EMC
Registration requirements. This instrument is registered as a Class B instrument for
residential and/or buiness use.
B급기기 (가정용 방송통신기자재)
이기기는 가정용(B급) 전자파적합기기로서 주
로가정에서 사용하는 것을 목적으로 하며, 모든
지역에서 사용할 수있습니다.
United States (FCC)
This equipment has been tested and found to comply with the limits for a Class B
digital device, pursuant to part 15 of the FCC Rules. These limits are designed to provide
reasonable protection against harmful interference when the equipment is operated in a
commercial environment. This equipment generates, uses, and can radiate radio frequency
energy and, if not installed and used in accordance with the instruction manual, may cause
harmful interference to radio communications. Operation of this equipment in a residential
environment may cause harmful interference in which the user will be required to correct the
interference at their own expense.
NOTE: Changes or modifications not expressly approved by PerkinElmer could cause the
instrument to violate FCC (U.S. Federal Communications Commission) emission
regulations, and because of this violation could void the user’s authority to operate
this equipment.

16 . DSC 6000 Installation and Hardware Guide
Electrical Safety
This analyzer conforms to IEC publication 61010-1 (“Safety requirements for electrical
equipment for measurement, control and laboratory use”) as it applies to IEC Class 1
(earthed) appliances, and therefore meets the requirements of the Low Voltage Directive
2006/95/EC.
Pollution Degree 2
This product will operate safely in environments that contain nonconductive foreign matter
up to Pollution Degree 2 in EN/IEC 61010-1.
Normally only non-conductive POLLUTION occurs. Occasionally, however, a temporary
conductivity caused by condensation must be expected.

Safety and Regulatory Information . 17
WEEE Instructions for PerkinElmer Products
or
A label with a crossed-out wheeled bin symbol and a rectangular bar indicates that the
product is covered by the Waste Electrical and Electronic Equipment (WEEE) Directive and is
not to be disposed of as unsorted municipal waste. Any products marked with this symbol
must be collected separately, according to the regulatory guidelines in your area.
The objectives of this program are to preserve, protect and improve the quality of the
environment, protect human health, and utilize natural resources prudently. Requirements
for waste collection, reuse, recycling, and recovery programs vary by regulatory authority at
your location. Contact your local responsible body (for example, your laboratory manager) or
authorized representative for information regarding applicable disposal regulations. Contact
PerkinElmer at the web site listed below for information specific to PerkinElmer products.
Web address:
www.perkinelmer.com/WEEE
For Customer Care telephone numbers select “Contact us” on the web page.
Products from other manufacturers may also form a part of your PerkinElmer system. These
other producers are directly responsible for the collection and processing of their own waste
products under the terms of the WEEE Directive. Please contact these producers directly
before discarding any of their products.
Consult the PerkinElmer web site (above) for producer names and web addresses.

18 . DSC 6000 Installation and Hardware Guide

Prepare the Laboratory

20 . DSC 6000 Installation and Hardware Guide
Prepare the Laboratory
The following sections describe requirements for your Thermal Analysis System. Make sure
your laboratory meets all of the requirements before you try to install the system. You should
step through the topics in the order presented below.
Before starting installation, please read the Safety and Regulatory Information.
•Electrical Requirements
•Environmental Requirements
•Purge Gas and Pneumatic Supply Requirements
•Space Requirements
Electrical Requirements
Power Source
An independent power source should be provided for the system, including the computer.
The power source should not be associated with heavy-duty equipment such as large motors,
or with possible sources of high-frequency interference such as photocopying systems,
discharge lamps, or radio transmitters. The power supply should be fused at a maximum of
20 A (120 V systems) or 16 A (200–240 V systems).
Line Voltage
PerkinElmer analyzers and their associated instruments are designed to operate within a line
voltage range of 10% of the nameplate voltage or other such voltage selected at installation
to suit the particular country or region. (The range for 240 V systems is +6%, –10%.) The
supply must be smooth, clean, earthed and free of transient voltages over 40 V.
The frequency range is ±1% for 50 Hz and 60 Hz systems.
Instrument Maximum Power Requirements
Refer to the Safety Precautions for the instrument.
Environmental Requirements
You must provide the following laboratory conditions for your Thermal Analysis System:
•A clean area, free from vibration and strong magnetic fields.
•An adequate and stable power source for all system components.
•The area must have a relative humidity of 20–75% (without condensation).
•For optimum performance, the temperature of the area should be between 10 °C and
35 °C (50 °F and 95 °F).
•The instrument will operate safely between 5 °C and 40 °C.
•Place the system components in an area that is not in direct sunlight or direct contact
with heating and cooling ducts or units.