ThermoFisher Scientific thermoscientific F6000 User manual

LT1249X1 Rev. J August, 2022
Thermo Scientific
Thermolyne Furnace
Premium Large Muffle/
Atmosphere Controlled Ashing
Model Type: F6000
Installation and Operation Manual

© 2022 Thermo Fisher Scientific Inc. All rights reserved.
Thermo Fisher Scientific Inc. provides this document to its customers with a product purchase to use in the
product operation. This document is copyright protected and any reproduction of the whole or any part of this
document is strictly prohibited, except with the written authorization of Thermo Fisher Scientific Inc.
The contents of this document are subject to change without notice. All technical information in this
document is for reference purposes only. System configurations and specifications in this document supersede
all previous information received by the purchaser.
              
                 
                

This document is not part of any sales contract between Thermo Fisher Scientific Inc. and a purchaser. This
document shall in no way govern or modify any Terms and Conditions of Sale, which Terms and Conditions of
Sale shall govern all conflicting information between the two documents.
Release history:


Single Setpoint Models F6010, F6010CN, F6018
Single Setpoint Models with OTP F6020C, F6020C-33, F6020C-33-60, F6020C-60,
F6028C, F6028C-60
8 Segment Programmable Models with
OTP
F6020C-33-60-80, F6020C-33-80, F6020C-60-80,
F6020C-80, F6028C-60-80, F6028C-80
5X 16 Segment Programmable Models
with OTP & RS485 Communication
F6030CM, F6030CM-33, F6030CM-33-60,
F6030CM-60, F6038CM, F6038CM-60
(-60 Models) - Ashing furnace
Type F6000 Furnace
OPERATION MANUAL
AND PARTS LIST
Series 1249
LT1249X1 • Rev J

Thermo Scientific Small Benchtop Muffle 1
C
Chapter 1 Safety Information . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
Alert Signals . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
Important Information . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
Warnings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
Warning . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
Chapter 2 Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
Intended Use . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
General Usage . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
Principles of Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
Chapter 3 General Specification . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
Environmental Conditions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
Chapter 4 Unpacking . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
Chapter 5 Installation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
Site Selection . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16
Electrical Connections . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16
Electrical Conditions in the EU . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
Chapter 6 Operation, All Models . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
Power Switch . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
Cycle Light shown on the display . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
Door Safety Switch . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
Chapter 7 Single Setpoint Models w/OTP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
Eurotherm 3216 Controller Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22
Basic Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22
Buttons and Indicators . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
To change the Setpoint . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
To View the Display Units . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
Controller Parameters . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
Alarms . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24
Sensor Break Protection . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24
Over – Temperature Protection (OTP) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24
Contents

Contents
2Small Benchtop Muffle Thermo Scientific
Tuning . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25
Chapter 8 Single Ramp & Dwell . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27
Functions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28
Program Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29
SetPoint Rate Limit Setup . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30
Running the Program . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30
Holding the Program . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30
Stopping the Program . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30
Clearing the Flashing End . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30
Verifying a Running Program . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31
Chapter 9 8 Segment & 5x16 Segment Programmable Models w/OTP . . . . . . . . . . . 33
Eurotherm 3216 Controller . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34
Operator Interface & HOME Display . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35
Beacon Display and Description . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35
Operator Buttons . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36
Single Set Point Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36
Alternate Set Point Selection (SP2) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37
Set Point Ramp Rate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37
View or Change the Display Units . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 38
Auto Tuning . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39
Parameter List . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 40
Offset Procedure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42
Alarms & Diagnostics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43
Sensor Break & Loop Break Protection . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44
Over-Temperature Protection (OTP) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44
1-Program 8-Segment Controller Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . 46
Soft Start Timer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48
Delayed Switch On Timer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49
5-Program 16-Segment Controller Operation . . . . . . . . . . . . . . . . . . . . . . . . . . 54
Chapter 10 Communication Option . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 61
Adapters - RS 485 to RS 232/USB . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 61
RS 485 Pinout & Connections . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62
Host Computer & Software . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62
3216c/p Controller Paremeters for Communication . . . . . . . . . . . . . . . . . . . . . 62
Troubleshooting Communications . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62
Chapter 11 Installation and Operation of Air Control . . . . . . . . . . . . . . . . . . . . . . . . . 63
Installation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 63
Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 64
Chapter 12 Furnace Loading . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 67
Chapter 13 Preventive Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 69
General Cleaning Instructions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 69

Contents
Thermo Scientific Small Benchtop Muffle 3
Chapter 14 Maintenance and Servicing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 71
To Replace a Heating Element . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72
To Replace a Platinel II Thermocouple . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72
To Replace a Chromel/Alumel Thermocopule . . . . . . . . . . . . . . . . . . . . . . . . . 72
To Replace Solid State Relay: . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 73
To Replace Door Switch . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 73
To Realign Door Strike . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 74
To Replace Controller . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 74
Chapter 15 Troubleshooting . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 75
Chapter 16 Replacement Parts List . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 77
Chapter 17 Ordering Procedures . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 79
Chapter 18 Wiring Diagrams . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 81
Single setpoint control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 82
Single Setpoint Control w/OTP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 83
8 Segment Programmable control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 84
5 X 16 Segment Programmable control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 85
Chapter 19 Regulatory Compliance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 87
Electromagnetic Compatibility . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 87
Additional Regulations & Markings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 88
WEEE Compliance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 91
Product Safety . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 87

Contents
4Small Benchtop Muffle Thermo Scientific

Thermo Scientific Premium Large Muffle 5
1
Safety Information
Contents
• “Alert Signals” on page 6
• “Important Information” on page 6
• “Warnings” on page 6
• “Warning” on page 7

1 Safety Information
Alert Signals
6Premium Large Muffle Thermo Scientific
Alert Signals
Important Information
Your Thermo Scientific Thermolyne F30400 Model Furnace has been designed with function,
reliability and safety in mind. It is your responsibility to install it in conformance with local electrical
codes. For safe operation, please pay attention to the alert signals throughout the manual.
This manual contains important operating and safety information.
You must carefully read and understand the contents of this manual prior to the use of this furnace.
If the equipment is used in a manner not specified by the manufacturer, protection provided by the
equipment may be impaired.
Warnings
To avoid electrical shock, this furnace must:
1. Use a properly grounded electrical outlet of correct voltage and current handling capacity.
2. Be disconnected from the power supply prior to maintenance and servicing.
3. Have the door switch operating properly.
To avoid burns, this furnace must:
Caution: Hot Surface - Avoid Contact. To avoid burns, do not touch the exterior or interior surfaces of
this furnace during use or for a period of time after use.
To avoid personal injury:
1. Do not use in the presence of flammable or combustible materials; fire or explosion may result.
This device contains components which may ignite such material.
2. Refer servicing to qualified personnel.
Warnings alert you to a possibility of personal injury.
Cautions alert you to a possibility of damage to the equipment.
Notes alert you to pertinent facts and conditions.
Hot surfaces alert you to a possibility of personal injury if you come in contact with a
surface during use or for a period of time after use.

1 Safety Information
Warning
Thermo Scientific Premium Large Muffle 7
3. Always wear safety glasses or a safety shield and high temperature gloves when loading or
unloading the furnace. Long sleeved, fire retardant clothing and a fire retardant apron is also
recommended.
Warning
This warning is presented for compliance with California Proposition 65 and other regulatory agencies
and only applies to the insulation in this product. This product contains refractory ceramic, refractory
ceramic fiber or fiberglass insulation, which can produce respirable dust or fibers during disassembly.
Dust or fibers can cause irritation and can aggravate pre-existing respiratory diseases. Refractory
ceramic and refractory ceramic fibers (after reaching 1000°C) contain crystalline silica, which can cause
lung damage (silicosis). The International Agency for Research on Cancer (IARC) has classified
refractory ceramic fiber and fiberglass as possibly carcinogenic (Group 2B), and crystalline silica as
carcinogenic to humans (Group 1).
The insulating materials can be located in the door, the hearth collar, in the chamber of the product or
under the hot plate top. Tests performed by the manufacturer indicate that there is no risk of exposure
to dust or respirable fibers resulting from operation of this product under normal conditions. However,
there may be a risk of exposure to respirable dust or fibers when repairing or maintaining the insulating
materials, or when otherwise disturbing them in a manner which causes release of dust or fibers. By
using proper handling procedures and protective equipment you can work safely with these insulating
materials and minimize any exposure. Refer to the appropriate Material Safety Data Sheets (MSDS) for
information regarding proper handling and recommended protective equipment. For additional
MSDS copies, or additional information concerning the handling of refractory ceramic products,
please contact the Customer Service Department at 1-800-438-4851.

1 Safety Information
Warning
8Premium Large Muffle Thermo Scientific

Thermo Scientific Premium Large Muffle 9
2
Introduction
Contents
• “Intended Use” on page 10
• “General Usage” on page 10
• “Principles of Operation” on page 10

2 Introduction
Intended Use
10 Premium Large Muffle Thermo Scientific
Intended Use
The Type F6000 furnaces are general purpose laboratory and heat treating furnaces. For optimum
element life, we recommend observing these temperature ranges: from 100°C (212°F) to 1093°C
(2000°F) continuous use or from 1093°C (2000°F) to 1200°C (2192°F) for intermittent use. (-60)
Ashing models continuous temperature range is 100°C (212°F) to 975°C (1787°F). Continuous use is
operating the furnace for more than 3 hours and intermittent use is operating the furnace for less than
3 hours.
All furnaces consist of:
1. a vented heating chamber;
2. a temperature controller; and
3. a door safety switch for operator safety.
General Usage
Do not use this product for anything other than its intended usage.
Principles of Operation
The furnace chamber is heated by electric resistance elements and is insulated with ceramic fiber
insulation. The controller is located under the furnace chamber and is well insulated from the heat
generated in the furnace chamber. A door safety switch removes power to the heating elements
whenever the furnace door is opened. The temperature is controlled by one of three types of
controllers. The (-60) models operate the same as the other models except at a lower temperature and
can inject gas into the chamber.
Do not exceed operating temperatures shown in ““General Specification” on page 9.”
Exceeding these limits will result in severely reduced element life.

Thermo Scientific Premium Large Muffle 11
3
General Specification
For F6000 Furnace
Models
F6020C
F6020C-33
F6020C-33-60
F6020C-33-60-
80
F6020C-33-80
F6020C-60
F6020C-60-80
F6020C-80
F6030CM
F6030CM-33-6
0
F6030CM-60
F6028C
F6028C-60
F6028C-60-80
F6038CM
F6038CM-60
F6010
F6010CN
F6018
 

  19.25(48.9) 19.25(48.9) 19.25(48.9) 19.25(48.9)
 21 (53.3) 21 (53.3) 21 (53.3) 21 (53.3)
 20 (50.8) 20 (50.8) 20 (50.8) 20 (50.8)
  12.75 (32.4) 12.75 (32.4) 12.75 (32.4) 12.75 (32.4)
 6.75 (17.1) 6.75 (17.1) 6.75 (17.1) 6.75 (17.1)
 10 (25.4) 10 (25.4) 10 (25.4) 10 (25.4)
   96 (43.5) 96 (43.5) 96 (43.5) 96 (43.5)
  220-240 208 220-240 208
  18.3 19.2 12.9 11.2

3 General Specification
Environmental Conditions
12 Premium Large Muffle Thermo Scientific
Environmental Conditions
 4400 4000 3095 2325
 50/60 50/60 50/60 50/60
 1111


212-2192°F
(100-1200°C)
212-2192°F
(100-1200°C)
212-2192°F
(100-1200°C)
212-2192°F
(100-1200°C)
*212-1787°F
(*100-975°C)
*212-1787°F
(*100-975°C)
Models
The maximum ramp rates for this furnace for heat up are: 12°C (22°F) per min. from
25°C-537°C (75°F-1000°F), 10°C (18°F) per min. from 537°C-1093°C
(1000°F-2000°F).
*(-60) coal-ashing furnaces.
 17°C to 27°C; 20% to 80% relative humidity, non-condensing. Installation Category II (over
voltage) in accordance with IEC 664. Pollution degree 2 in accordance with IEC 664.
  2,000 meters.
 -25°C to 65°C; 10% to 85% relative humidity.
  240VAC +/- 10%
°F (°C)

Thermo Scientific Premium Large Muffle 13
4
Unpacking
1. Visually check for any physical damage to the shipping container.
2. Inspect the equipment surfaces that are adjacent to any damaged area.
3. Open the furnace door and remove the packing material from inside the furnace chamber.
4. Vacuum the chamber prior to use to remove the insulation dust due to shipment.
5. Retain the original packaging material if reshipment is foreseen or required.
(-60) models are supplied with two stainless steel trays, handle and porcelain pegs.
The Type 6000 furnaces do not come with a power cord because current
requirements are too great to be handled by ordinary power cords and standard wall
supply. (F6010 and F6018 are supplied with cord and plug).

4 Unpacking
14 Premium Large Muffle Thermo Scientific

Thermo Scientific Premium Large Muffle 15
5
Installation
Contents
• “Site Selection” on page 16
• “Electrical Connections” on page 16
• “Electrical Conditions in the EU” on page 17

5 Installation
Site Selection
16 Premium Large Muffle Thermo Scientific
Site Selection
Install furnace on a sturdy surface and allow space for ventilation.
Electrical Connections
1. The electrical ratings are located on the specification plate on the back of the furnace. Consult
customer service if your electrical service is different than those listed on the specification plate. Be
sure the front power switch is in the OFF position before connecting the furnace to your electrical
supply. Your 6000 furnace may be wired either directly through a conduit system or by using a
power cord and plug which conforms to the National Electrical Codes and electrical code
requirements of your area. The terminal block to be used in wiring is located on the lower rear of
the furnace.
Be sure ambient temperature does not exceed 40°C (104°F). Ambient above this level
may result in damage to the controller.
Allow at least six inches of space between the furnace, at least 40 inches above the
furnace and any combustible surface. This permits the heat from the furnace case to
escape so as not to create a possible fire hazard.
To avoid electrical shock, this furnace must be installed by a competent, qualified
electrician who ensures compatibility among furnace specifications, power source and
grounding code requirements. (Disregard Step 2 if you have Model F6010 or
F6018).
For supply connections, use 10 AWG or larger wires suitable for at least 90°C. Failure
to observe this caution could result in damage to furnace.
Do not use in the presence of flammable or combustible materials; fire or explosion
may result. This device contains components which may ignite such material..
Caution: Hot Surface. Avoid Contact.
To avoid burns, this furnace must not be touched on the exterior or interior surfaces
during use or for a period of time after use.
Please observe the alert signals on the left hand side of this page before operating your
furnace.
Models F6010, F6010-33, F6018

5 Installation
Electrical Conditions in the EU
Thermo Scientific Premium Large Muffle 17
Electrical Conditions in the EU
Electrical Conditions for operating the furnaces in the EU:
The furnaces are intended for use at a network supply with a maximum system impedance of
Zmax= 0.0229 ohm at the point of connection, according to EN 61000-3-11 clause 6.2.2. The user
has to ensure that the device is operated on a network supply that meets these requirements. If
necessary, the system impedance can be confirmed by the energy supplier.