Varian GC 3800 Manual

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PARTS
LIST
DOC: 03-925914-01/02
DESC: Micro - TCD Installation
PAGE:
REV
1 of 3 1
TOOLS
PREPARED BY: Sax Makthepharack REVISED BY: CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN
-
03 - 10 - 00
Michael Slaughter
MENU
CHG
HISTORY
INSTALLATION OF MICRO-TCD
STATION #3, ASSEMBLY PROCEDURES
ADAPTER (SEE NEXT PAGE)
TEE (SEE NEXT PAGE)

PARTS
LIST
DOC: 03-925914-01/02
DESC: Micro - TCD Installation
PAGE:
REV
2 of 3 1
TOOLS
PREPARED BY: Sax Makthepharack REVISED BY: CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN
-
03 - 10 - 00
Michael Slaughter
MENU
CHG
HISTORY
EFC CARRIER
INJECTOR (REF.)
SEE DETAIL “A”
ANALYTICAL COLUMN (CP-7758)
REFERENCE COLUMN (CP-735732) SEE DETAIL “B”
03-925910-01
BALANCE ADAPTOR
SEE DETAIL “B”
SCHEMATIC OF MICRO-TCD WITH ADAPTOR REFERENCE
DETAIL “A” DETAIL “B”
INJECTOR (REF.)
CLICK HERE FOR
MICRO-TCD ASSEMBLY
16-000589-00
TEE
28-694581-00
FERRULE
03-949551-00
NUT
CP-470100
FERRULE, Ø0.32 COLUMN
CP-085887
NUT
(03-925916-01)
MICRO-TCD REF. SIDE, ADAPTOR FACTORY
MICRO-TCD CELL (REF.)
SCHEMATIC OF MICRO-TCD WITH INJECTOR REFERENCE

PARTS
LIST
DOC: 03-925914-01/02
DESC: Micro - TCD Installation
PAGE:
REV
3 of 3 1
TOOLS
PREPARED BY: Sax Makthepharack REVISED BY: CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN
-
03 - 10 - 00
Michael Slaughter
MENU
CHG
HISTORY
INSTALLATION OF MICRO-TCD:
1. ENSURE GC OVEN INSULATION IS CAREFULLY WRAPPED UNDER AND
AROUND, THE MICRO-TCD TO PREVENT COLUMN OVEN CONDITIONS
COUPLING WITH DETECTOR.
2. FEED HEATER AND PROBE TO LOCATION ON PWA’S
- HEATER TO ZONE ON POWER PWA.
- PROBE TO ZONE ON MAIN PWA.
3. INSTALL MICRO-TCD PWA BOARD (03-925904-01) AND SECURE. ROUTE FLAT,
RIBBON CABLE FROM MICRO-TCD ALONGSIDE PNEUMATICS BULKHEAD AND
AROUND TO MICRO-TCD PWA BOARD. SECURE WITH CABLE CLAMP. 03-925904-01
MICRO-TCD PWA
HEATER CONNECTOR ZONE
PROBE CONNECTOR ZONE
03-925914-11/12
MICRO-TCD SUB-ASSEMBLY

PARTS
LIST
DOC: 03-925914-01/02
DESC: Micro - TCD Installation
PAGE:
REV
4 of 3 1
TOOLS
PREPARED BY: Sax Makthepharack REVISED BY: CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN
-
03 - 10 - 00
Michael Slaughter
MENU
CHG
HISTORY

PARTS
LIST
DOC: 03-925862-00
DESC:
PAGE:
REV
1 of 2
3800GC W/DEFC Leak Test Procedure 1
TOOLS
PREPARED BY: Sax Makthepharack REVISED BY: CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN
-
06 - 09 - 98
Michael Slaughter
MENU
CHG
HISTORY
INJECTOR EFC LEAK TEST PROCEDURE
1. Install ETS software Version 1.6.2 or newer. (be sure to discharge yourself before touching ROM pwa.)
2. Set the DIP Switches on the main board as shown:
3. Turn on power and connect Carrier Gas inlet tube.
4. Make sure jumpers on EFC board are in the correct position.
5. Cap off all unused gas inlet fittings and the Injector column out fitting.
6. Press MENU key.
7. Check com board if installed (under AOC cont.) pg.2.
8. Check Detector Electrometer pwa’s, (3) are they present?.
9. Check EFC’s, (5) are they present? Are they good?
10. If EFC’s are present and good, press Enter Key and set to Pressure DAC 5.00 and Flow DAC to 3.00.(Left blue toggle key below display 3
times to pressure up instrument).
11. After completing items 1 thru 10, turn on Carrier Gas.
12. When the pressure is stable, turn OFF Carrier Gas and press LEAKSTOP Key. (blue key below display)
13. The leak test procedure will run for 5 minutes then stop and display the leak value for the 5 min. period. (< .30 + .10 for each EFC installed is
the acceptance criteria, (if the test fails, retest and measure the flow at the EFC Vent tube. If a leak is detected and is less than .10 ml/min.
subtract the amount from your total leak value. If that value is less than the spec (above), the instrument passed the test. If over, the
instrument Fail and the leak must be found and corrected. Retest as above until a pass condition is reached.
14. Record the resulting value of the leak test on the QC Record Sheet.
15. Press Menu Key, go to TEMPERATURE MENU (4) check and press Enter.
16. Set all Temp zones to NOT USED and press Enter. (use decrease key)
17. Go to Pg.2 of 3, check Vent Doors for unrestricted opening and closing. (toggle ON enter, OFF enter)
18. If any Cryo is installed, go to pg. 3. Select the proper external event then activate to assure opening and closing. (blue Time Off/On key
under display)
19. Go back to pg. 1 and Enable those zones used. Observe temperature go to 50 deg. and hold stable.
20. Press CONTACTOR key.
21. If Fan is running, go back to pg. 2 and turn off Fan.
22. Go to EFC Control (5) enter, select flow key and measure each Inj/Det. for some amount of flow.
23. Go to Main Menu, select EFC Control, press enter, go to EFC location (front, middle, rear) then go to pg. 6. In lower right corner of display
see EFC type, is it correct? (type 1,3,4,5, etc.) Turn Instrument Off, replace ROM board and restart instrument. Initial Display should
appear.

PARTS
LIST
DOC: 03-925862-00
DESC:
PAGE:
REV
2 of 2
3800GC W/DEFC Leak Test Procedure 1
TOOLS
PREPARED BY: Sax Makthepharack REVISED BY: CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN
-
06 - 09 - 98
Michael Slaughter
MENU
CHG
HISTORY
DETECTOR EFC LEAK TEST PROCEDURE
1. Connect Helium to makeup line for FID, TSD, ECD and TCD. Connect Helium to H2 line for PFPD and TCD(H2).
2. Cap off all other gas inlets
3. Make sure DEFC position jumpers in correct position.
4. Cap all other inlets (Top and bottom of Detector)
5. Plug in customer software.
6. Turn on the power
7. Press ∞to go to local mode.
8. From the “Instrument Setup” menu, Enter the IEFC type(s) in the appropriate positions in the “Heated Zones” screen
9. Save and Exit
10. When the GC is done initializing (~2 minutes), Press ∞to go to local mode.
11. Press “Detector” button to get to the Detector Menu
12. For each detector:
* Pick Detector
* Go to the “adjustments” screen, page 2
* Turn on the gas
* Within 2 minutes, the flowrate of the Helium channel (1) should go to 0. In the case of PFPD, channel 2 is used. In the case of
TCD(H2), Channel 1 is used.
* If flowrate does not go to 0, fix leaks and retest. (.1 is acceptable for PFPD with manufacture engineer approval).
* Turn off gas and GC

PARTS
LIST
DOC: 03-925709-01
DESC: Assy, Column Oven Cryogenics, (CO2)
PAGE:
REV
1 of 3 1
CHG
HISTORY TOOLS
PREPARED BY: Sax Makthepharack REVISED BY: CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN
-
04 - 05 - 00
Michael Slaughter
MENU
ASSY, COLUMN OVEN CRYOGENICS, (CO2)
3800GC SUB-ASSEMBLIES STATION, ASSEMBLY PROCEDURES

PARTS
LIST
DOC: 03-925709-01
DESC: Assy, Column Oven Cryogenics, (CO2)
PAGE:
REV
2 of 3 1
CHG
HISTORY TOOLS
PREPARED BY: Sax Makthepharack REVISED BY: CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN
-
04 - 05 - 00
Michael Slaughter
MENU
NOTES:
1.
03-925567-01
3800 CO2 VALVE FACTORY INSTALL
COLUMN OVEN CRYOGENICS EXPLODED VIEW
28-694205-00
1/8IN ADAPTER
28-609966-00
ADAP, COMP., 1/8 X 1/8 SST
12-222060-04, 2 PLCS
SCREW, 10-32 X 1/4 PAN, SS
03-925261-01
BRACKET, CRYO VALVE
03-925497-01
CO2 OUTLET TUBE
FLOW DIRECTIOIN
60°(REF.)
INSTALL TEFLON TAPE ON FITTING THREADS AS REQUIRE AND
FRONT VIEW (REF.)
1
1
2
CO2 OUTLET TUBE (REF.)
3800 CO2 VALVE
FACTORY INSTALL
CRYO VALVE BRACKET (REF.)
1-1/2 - 2 TURNS IN THE DIRECTION OF THREADS.
SURE TUBING TOWARD THE FAN SHAFT INSIDE THE OVEN
WHEN INSTALLING THE CO2 OUTLET TUBE (03-925497-01) MAKE2.

PARTS
LIST
DOC: 03-925709-01
DESC: Assy, Column Oven Cryogenics, (CO2)
PAGE:
REV
3 of 3 1
CHG
HISTORY TOOLS
PREPARED BY: Sax Makthepharack REVISED BY: CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN
-
04 - 05 - 00
Michael Slaughter
MENU
COLUMN OVEN
CRYOGENICS ASSEMBLY (REF.)
22-799995-00
BUSHING, STRAIN REL.
12-901163-00, 2 PLCS
SCREW, 8-32 X 3/8 SEM
03-925489-01
ASSY, CABLE, CRYO EXTENSION
9
1
7
NOTE:
CONNECT CRYOU EXTENSIO
WIRES PIN TO (J-47) ON PWA
(J-47)
CONNECTOR (REF.)

PARTS
LIST
DOC: 03-925709-01
DESC: Assy, Column Oven Cryogenics, (CO2)
PAGE:
REV
4 of 3 1
CHG
HISTORY TOOLS
PREPARED BY: Sax Makthepharack REVISED BY: CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN
-
04 - 05 - 00
Michael Slaughter
MENU

PARTS
LIST
DOC: 03-925708-01
DESC: Assy, Column Oven Cryogenics
PAGE:
REV
1 of 4 1
CHG
HISTORY TOOLS
PREPARED BY: Sax Makthepharack REVISED BY: CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN
-
04 - 25 - 00
Micheal Slaughter
MENU
ASSY, COLUMN OVEN CRYOGENICS (LN2 VERSION)
3800GC STATION #3, ASSEMBLY PROCEDURES

PARTS
LIST
DOC: 03-925708-01
DESC: Assy, Column Oven Cryogenics
PAGE:
REV
2 of 4 1
CHG
HISTORY TOOLS
PREPARED BY: Sax Makthepharack REVISED BY: CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN
-
04 - 25 - 00
Micheal Slaughter
MENU
03-925557-01
3800 LN2 VALVE
03-925261-01
BRACKET, CRYO VALVE
28-691979-00
1/4 T X 1/8 P BR MALE CONN.
28-695130-00
B-4-TA-1-2 ADAPTER, COMPRESSION 1/4 TUBE
03-925378-01
LIQUID NITROGEN OUTLET TUBE
03-925489-01
ASSY, CABLE, CRYO EXTENSION
14-312010-00, 2 PLCS
WASHER, EXT LOCK, #10
OUTLET SIDE
INLET SIDE
NOTES:
1
12-222010-06, 2 PLCS
10-24 X 3/8 PH PAN
INSTALL TEFLON PIPE TAPE (88-189669-00) FITTING THREADS PRIOR TO INSTALLATION.
2 WHEN INSTALLING LIQUID NITROGEN OUTLET TUBE (03-925378-01) INTO THE 1/4 T X 1/8 P
BR MALE CONNECTOR (28-691979-00), MAKE SURE HOLES ON THE END OF OUTLET TUBE
IS UPWARD PRIOR TO TIGHTENING. SEE DETAIL “A”.
2
1OUTLET TUBING (REF.)
SEE NOTE #2
FOR REFERENCE ONLY
REFER TO NEXT PAGE FOR CONFIGURATION

PARTS
LIST
DOC: 03-925708-01
DESC: Assy, Column Oven Cryogenics
PAGE:
REV
3 of 4 1
CHG
HISTORY TOOLS
PREPARED BY: Sax Makthepharack REVISED BY: CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN
-
04 - 25 - 00
Micheal Slaughter
MENU
LN2 OVEN CRYO
NO OVEN CRYO
BULK ISSUE ITEMS (03-925515-XX)
3 INJECTORS 2 INJECTORS 1 INJECTOR NO INJECTOR
57-000235-00
PRESSURE RELIEF VALVE 1
28-695036-00
SWAGELOK #B-4-TA-7-4
28-691946-00
TEE, UNION 1/4” TUBE BRASS 1
03-925651-01
TUBE, 1/4” CROSS, TEE, CONNECTOR
03-925654-01
DEFLECTOR, AIR FLOW

PARTS
LIST
DOC: 03-925708-01
DESC: Assy, Column Oven Cryogenics
PAGE:
REV
4 of 4 1
CHG
HISTORY TOOLS
PREPARED BY: Sax Makthepharack REVISED BY: CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN
-
04 - 25 - 00
Micheal Slaughter
MENU
VALVE ARRANGEMENT (REF.)
23-230938-00
COVER, SQUARE
88-494510-00, 5” LG
PIPE INSULATION 3/8” ID .42” 12-901163-00, 2 PLCS
SCREW, 8-32 X 3/8, SEM

PARTS
LIST
DOC: 03-925632,633,634&635-XX
Assy, 1177 Manual and Type 5 EFC Installation
PAGE:
REV
1 of 4 1
CHG
HISTORY TOOLS
PREPARED BY: Sax Makthepharack REVISED BY: CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN
-
12 - 03 - 99
Steve Swihart
MENU
DESC:
ASSY, 1177 MANUAL AND TYPE 5 EFC INSTALLATION
3800GC STATION #3, ASSEMBLY PROCEDURES

PARTS
LIST
DOC: 03-925632,633,634&635-XX
Assy, 1177 Manual and Type 5 EFC Installation
PAGE:
REV
2 of 4 1
CHG
HISTORY TOOLS
PREPARED BY: Sax Makthepharack REVISED BY: CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN
-
12 - 03 - 99
Steve Swihart
MENU
DESC:
03-925469-01
BRACKET, SPLIT VLV. MTG.
27-239921-00
GAGE PRESSURE, 0-60 PSI
28-694302-00
ADAPTER 1/8” UNION
BRS. COMP. FTG.
03-918853-03
PEEK TUBING, GREEN
27-180135-00
KOJIMA FLOW CONTL.
03-918959-02
PENCIL FILTER
03-925467-01
SOLENOID VALVE 3- WAY
03-918174-00
BACK PRESSURE REGULATOR
03-918853-03
PEEK TUBING, GREEN
03-918853-03
PEEK TUBING, GREEN
28-158923-00
TYGON TUBING, CLEAR.
FROM INJECTOR
VENT
28-691944-00
TEE, 1/16” BRASS
03-918853-03
PEEK TUBING, GREEN
12-222008-04
SCREW, 8-32,X 1/4” LG PH,
SST 2EA
03-918853-07
PEEK TUBING, NATURAL
03-918853-03
PEEK TUBING, GREEN
CLICK HERE TO SEE SOLENOID CONNECTION TO J42 ON POWER BD.
03-917157-00
WASHER , VITON FERRLE 3EA
03-917084-00
NUT, VITON FERRULE 3EA
03-917142-00
VITON FERRLE 3EA
03-917157-00
WASHER , VITON
FERRLE 2EA
03-917142-00
VITON FERRLE 2EA
SEE ADJ.
NOTE/ DETAIL
03-917084-00
NUT, VITON FERRULE 2EA
03-917157-00
WASHER , VITON FERRLE 2EA
03-917142-00
VITON FERRLE 2EA
03-917084-00
NUT, VITON FERRULE
3EA
03-917157-00
WASHER , VITON FERRLE
3EA
03-917142-00
VITON FERRLE 3EA
12-901132-00
SCREW 8-32 X 3/8” LG EXT STL. 2EA
03-918853-03
PEEK TUBING, GREEN
03-917128-00
NUT, 1/6 NPS-”O” RING
“CARRIER GAS IN”
03-917157-00
WASHER , VITON FERRLE
03-917084-00
NUT, VITON FERRULE
03-917142-00
VITON FERRLE
28-849067-00
10-32 ADAPTER HOSE
03-918853-07
PEEK TUBING 1/8” NAT.
03-918853-07
PEEK TUBING 1/8” NAT.
28-849067-01
BESWICK FITTING
NOTE: DETAIL OF SOLENOID VALVE
12-901162-00
SCREW (2 PL)

PARTS
LIST
DOC: 03-925632,633,634&635-XX
Assy, 1177 Manual and Type 5 EFC Installation
PAGE:
REV
3 of 4 1
CHG
HISTORY TOOLS
PREPARED BY: Sax Makthepharack REVISED BY: CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN
-
12 - 03 - 99
Steve Swihart
MENU
DESC:
03-925996-XX
1177 INJECTOR, EFC
03-925110-01
EFC TYPE 1
12-901163-00
SCREW, 8-32 X 3/8” EXT.
4 ON EFC, 2 INJ., 6 TOTAL
03-925374-01
TEMPERATURE PROBE
03-925987-01
120V HTR. CART., 100V
03-925987-02
220V HTR. CART., 100V
03-925987-03
101V HTR.CART., 100V
03-918532-01
VAR SEPTUM PURGE
NOTE:
1 BE SURE INJ. IS IN ONE OF THE (4) A/S LOCATIONS. SEE INJ. COVER
FOR ALIGNMENT.
1

PARTS
LIST
DOC: 03-925632,633,634&635-XX
Assy, 1177 Manual and Type 5 EFC Installation
PAGE:
REV
4 of 4 1
CHG
HISTORY TOOLS
PREPARED BY: Sax Makthepharack REVISED BY: CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN
-
12 - 03 - 99
Steve Swihart
MENU
DESC:
1177 INJECTOR EFC TYPE 5
CLICK HERE OR ON PICTURE
TO SEE S/A EXPLOSION CLICK HERE OR ON PICTURE
TO SEE S/A EXPLOSION
INJ
FRONT DET.
FRONT INJ
MIDDLE DET.
MIDDLE INJ
REAR DET. REAR
INJECTOR
SPLIT VENT
SPARE
SPARE
INJECTOR SIDE MANIFOLD PLUMBING
G.C. FRONT
G.C. BACK
VENT THRU
PNEU. PANEL
SPLIT
VENT
PRESSURE
SENSE (TO 1177)
CARRIER IN FROM
CROSS FITTING
CARRIER
OUT
CARRIER IN - FROM EFC
CARRIER IN
(GREEN)
(GREEN COLORED MARKER)
SPLIT VENT
SEPTUM PURGE
TO SPORT VALVE
(NO COLORED MARKER)

PARTS
LIST
DOC: 03-925630&631-XX
DESC: Assy, 1177 EFC Injector Installation
PAGE:
REV
1 of 4 1
CHG
HISTORY TOOLS
PREPARED BY: Sax Makthepharack REVISED BY: CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN
-
12 - 1 - 99
Steve Swihart
MENU
ASSY, 1177 EFC INJECTOR INSTALLATION
3800GC STATION #3, ASSEMBLY PROCEDURES