Agilent Technologies 8000 Series User manual

Agilent Technologies
Agilent 8000
Dissolution Sampling
Station
Operator’s Manual

8000 Operator’s Manual
Notices
© Agilent Technologies, Inc. 2014
No part of this manual may be reproduced
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laws.
Manual Part Number
70-9060
Edition
Rev C, May 2014
Agilent Technologies, Inc.
3501 Stevens Creek Blvd.
Santa Clara, CA 95052 USA
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Safety Notices
CAUTION
A CAUTION notice denotes a
hazard. It calls attention to an
operating procedure, practice, or
the like that, if not correctly per-
formed or adhered to, could result
in damage to the product or loss
of important data. Do not proceed
beyond a CAUTION notice until
the indicated conditions are fully
understood and met.
WARNING
A WARNING notice denotes a
hazard. It calls attention to an
operating procedure, practice,
or the like that, if not correctly
performed or adhered to, could
result in personal injury or
death. Do not proceed beyond a
WARNING notice until the
indicated conditions are fully
understood and met.

8000 Operator’s Manual 3
Contents
Figures 7
Tab les 9
1Safety 11
Electrical Hazards 12
Warning 13
Caution 13
Note 13
Information Symbols 14
2 Introduction 15
8000 with Peristaltic Pump 17
Conventions Used in this Manual 17
Serial Number Format 18
3 Setting Up the 8000 19
Unpacking of 8000 and Components 20
Unpacking Your 8000 21
Unpacking / Setup of 8000 & Peristaltic Pump 22
Unpacking / Setup of 8000 & Syringe Pump 26
Unpacking / Setup of 8000, Syringe Pump, and Filter
Changer 29
Setup of 8000 and Components 34
Installing 8000 Full Flow Filters 34
Power and Network Connections 34
Installing the Sample Tray 36

48000 Operator’s Manual
Contents
Installing the Media Rinse Reservoir 36
Installing and Connecting the Autocalibration Block
(Peristaltic Pump only) 37
Installing the RM Module 38
Loading Filters (Filter Changer only) 40
Changing Filter Types (Filter Changer Only) 40
Hidden Key Functions 41
4 Operating the 8000 45
Operating the 8000 with Apparatus 1 / 2 46
8000 Keypad Options 46
8000 Menu Options - Apparatus 1 / 2 48
Creating a Sample Program 61
Starting a 8000 Program 66
Operating the 8000 with Apparatus 3 / 7 72
8000 Keypad Options 72
8000 with Apparatus 3 / 7 - Menu Options 74
Creating a Sample Program 86
Starting a Program 91
Manual Sample 95
Volumetric Calibration (Peristaltic Pump only) 97
Automatic Calibration 97
Manual Calibration 99
Checking the Calibration - Volume Accuracy 101
Daisy Chaining 102
Printer Operation and Communications 103
5 Maintenance and Troubleshooting 105
Preventive Maintenance 106
Clean System with Peristaltic Pump 106
Clean System Function with Syringe Pump 111

Contents
8000 Operator’s Manual 5
Syringe and Seal Replacement 112
Cleaning the Syringes 113
System Cleaning Procedure with Syringe Pump and Filter
Changer (optional) 115
Cleaning the Filter Changer Drip Tray 117
Cleaning the Media Replacement Pump 117
Report Center Impact Printer 119
Installing the Cartridge Ribbon 119
Replacing a Paper Roll 120
Toggling Your Printer Online 121
Printer Self Test 121
Printer Configuration 122
Obtaining Warranty and Other Services 123
Index 125

68000 Operator’s Manual
Contents
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8000 Operator’s Manual 7
Figures
Figure 1. Agilent 8000 Dissolution Sampling Station 21
Figure 2. Peristaltic Pump 22
Figure 3. Cable Connections for 8000, Peristaltic Pump, and VK
7000 / 7010 24
Figure 4. Resident Probe 25
Figure 5. 806 Syringe Pump 26
Figure 6. Cable Connections for 8000, Syringe Pump, and VK
7000 / 7010 27
Figure 7. Y Cable 5075-0446 and Adapter 5075-0852 28
Figure 8. 808 Filter Changer 30
Figure 9. Cable Connections for 8000, Syringe Pump, Filter
Changer, and VK 7000 / 7010 31
Figure 10. Y Cable 5075-0446 and Adapter 5075-0852 32
Figure 11. Resident Probe Housing and Sample Cannula 33
Figure 12. Internal Media Replacement Module 38
Figure 13. External Media Replacement Module 39
Figure 14. 8000 Keypad 46
Figure 15. 8000 Keypad 72
Figure 16. The Cleaning Process 108

88000 Operator’s Manual
Figures
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8000 Operator’s Manual 9
Tables
Table 1. Hidden Key Functions 41
Table 2. Front Panel Options (Apparatus 1 / 2) 47
Table 3. Main Menu Options (Apparatus 1 / 2) 49
Table 4. Set Clock and Alarms Options (Apparatus 1 / 2) 51
Table 5. Disso Parameters Options (Apparatus 1 / 2) 53
Table 6. Set Syringe Pump Parameters (Apparatus 1 / 2) 55
Table 7. Disso Control/Monitor Options (Apparatus 1 / 2) 57
Table 8. Manual Operations Options (Apparatus 1 / 2) 58
Table 9. Operate Syringe/Filter Changer Options (Apparatus 1 /
2) 59
Table 10. Program Variables Options (Apparatus 1 / 2) 62
Table 11. Select Start Mode Options (Apparatus 1 / 2) 68
Table 12. Disso Options (Apparatus 1 / 2) 69
Table 13. Select Disso Program Start Mode Options (Apparatus
1 / 2) 71
Table 14. Front Panel Options (Apparatus 3 / 7) 73
Table 15. Main Menu Options (Apparatus 3 / 7) 75
Table 16. Set Clock and Alarms Options 77
Table 17. Set App 3/7 Parameters Options (Apparatus 3 /
7) 79
Table 18. Set Syringe Pump Parameters Options (Apparatus 3 /
7) 81
Table 19. App 3/7 Control/Monitor Options 83
Table 20. Manual Operations (Apparatus 3 / 7) 84
Table 21. Operate Syringe/Filter Changer Options 85
Table 22. Program Variables Options (Apparatus 3 / 7) 88
Table 23. Select Start Mode Options (Apparatus 3 / 7) 93
Table 24. App 3/7 Options 94

10 8000 Operator’s Manual
Tables
Table 25. Manual Sampling Options 95
Table 26. Volume Accuracy Parameter Options 101
Table 27. Print Selections Options 104
Table 28. Program Auto Clean Variables 110
Table 29. Disso Parameters. 115
Table 30. Program Variables 116