Anton Paar ViscoQC 300 Series Original instructions

Measure
what is measurable
and make measurable
that which is not.
Galileo Galilei (1564-1642)
Instruction Manual and Safety Information
ViscoQC 300
Rotational Viscometer
(Original Instruction)
Software Version: 1.00.xx

Instruction Manual and Safety Information
ViscoQC 300
Rotational Viscometer
(Original Instruction)
Software Version: 1.00.xx

Disclaimer
This document may contain errors and omissions. If you discover any such errors or if you would like to see
more information in this document, please contact us at our address below. Anton Paar assumes no liability
for any errors or omissions in this document.
Changes, copyright, trademarks etc.
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as such. They are the property of their respective owner.
Further information
Published and printed by Anton Paar GmbH, Austria
Copyright © 2018 Anton Paar GmbH, Graz, Austria
Address of the instrument producer: Anton Paar GmbH
Anton-Paar-Str. 20
A-8054 Graz / Austria – Europe
Tel: [phone]
Fax: [phone]
E-Mail: [email protected]
Web: www.anton-paar.com
Date: December 2018
Document number: C78IB007EN-B

Contents
C78IB007EN-B 5
Contents
1 Safety Instructions................................................................................................................................. 6
1.1 General Safety Instructions............................................................................................................... 6
1.2 Special Safety Instructions................................................................................................................ 7
1.3 Safety Signs on the Instrument......................................................................................................... 7
1.4 Conventions for Safety Messages.................................................................................................... 7
1.5 Remaining Risks............................................................................................................................... 7
2 ViscoQC 300 - An Overview................................................................................................................... 8
2.1 Intended Use of the Instrument......................................................................................................... 8
2.2 Functional Components.................................................................................................................... 9
3 Checking the Supplied Parts ............................................................................................................... 10
4 Installing and Switching On the Instrument....................................................................................... 11
4.1 Installation Requirements ............................................................................................................... 11
4.2 Installation....................................................................................................................................... 11
5 Operating the Instrument..................................................................................................................... 16
5.1 Log on/off and User Management .................................................................................................. 16
5.2 The Display..................................................................................................................................... 17
5.3 Spindle, Spindle Guard, DIN Adapter............................................................................................. 19
6 Adjusting and Calibrating .................................................................................................................... 19
6.1 Calibrating....................................................................................................................................... 19
6.2 Adjusting......................................................................................................................................... 20
7 Measuring Settings, Methods and Modes ..........................................................................................22
7.1 Measuring Speeds – the Speed List............................................................................................... 22
7.2 Measurement Methods................................................................................................................... 22
7.3 Measurement Modes...................................................................................................................... 24
7.4 Spindles and Measuring Systems................................................................................................... 25
7.5 Instrument Setup............................................................................................................................. 26
8 Performing Measurement..................................................................................................................... 28
8.1 Preparation and Sample Filling....................................................................................................... 28
8.2 Measurement Procedure ................................................................................................................ 29
8.3 Measured Data ............................................................................................................................... 30
9 Cleaning................................................................................................................................................. 31
9.1 Standard Cleaning.......................................................................................................................... 31
9.2 Wetted Parts................................................................................................................................... 32
10 Maintenance Work .............................................................................................................................. 32
10.1 Software Maintenance.................................................................................................................. 32
10.2 Adjusting the Head Retention....................................................................................................... 33
10.3 Storing and Transporting the Instrument ...................................................................................... 33
Appendix A: Technical Data ................................................................................................................... 34
Appendix B: Spindle Overview............................................................................................................... 35
Appendix C: Menu Tree........................................................................................................................... 36
Appendix D: Trouble shooting ............................................................................................................... 39

1 Safety Instructions
6C78IB007EN-B
1 Safety Instructions
• Read this instruction manual before using
ViscoQC 300.
• Follow all hints and instructions contained in this
instruction manual to ensure the correct use and
safe functioning of ViscoQC 300.
• The manual is a part of the product. Keep this
manual for the complete working life of the prod-
uct and make sure it is easily accessible to all
people involved with the product. If you receive
any additions or revisions to this manual from
Anton Paar GmbH, these must be treated as
part of the manual.
1.1 General Safety Instructions
Liability
• This instruction manual does not claim to
address all safety issues associated with the
use of the instrument and samples. It is your
responsibility to establish health and safety
practices and determine the applicability of reg-
ulatory limitations.
• Anton Paar GmbH only warrants the proper
functioning of ViscoQC 300 if no adjustments
have been made to the mechanics, electronics,
and firmware.
• Only use ViscoQC 300 for the purpose
described in this instruction manual. Anton Paar
GmbH is not liable for damages caused by
incorrect use of ViscoQC 300.
Installation and use
• ViscoQC 300 is not an explosion-proof instru-
ment and therefore must not be operated in
areas with risk of explosion.
• The installation procedure should only be car-
ried out by authorized personnel who are famil-
iar with the installation instructions.
• Do not use any accessories or spare parts other
than those supplied or approved by Anton Paar
GmbH (see section 3).
• Make sure all operators are trained to use the
instrument safely and correctly before starting
any applicable operations.
• In case of damage or malfunction, do not con-
tinue operating ViscoQC 300. Do not operate
the instrument under conditions which could
result in damage to goods and/or injuries and
loss of life.
• Check ViscoQC 300 for chemical resistance to
the samples and cleaning agents.
Maintenance and service
• The results delivered by ViscoQC 300 not only
depend on the correct functioning of the instru-
ment, but also on various other factors. We
therefore recommend you have the results
checked (e.g. plausibility tested) by skilled per-
sonnel before consequential actions are taken
based on the results.
• Service and repair procedures may only be car-
ried out by authorized personnel or by Anton
Paar GmbH.
Disposal
• Concerning the disposal of ViscoQC 300,
observe the legal requirements in your country.
Returns
• For repairs send the cleaned ViscoQC 300 to
your Anton Paar representative. Only return the
instrument together with the filled out RMA
(Return MaterialAuthorization) and the form
"Safety Declaration for Instrument Repairs".
Please download the Safety Declaration form
from our website www.anton-paar.com.
• Do not return instruments which are contami-
nated by radioactive materials, infectious agents
or other harmful substances that cause health
hazards.
Precautions for highly flammable samples and
cleaning agents
• Observe and adhere to your national safety reg-
ulations for handling the measured samples
(e.g. use of safety goggles, gloves, respiratory
protection etc.).
• Only store the minimum required amount of
sample, cleaning agents and other inflammable
materials near ViscoQC 300.
• Do not spill sample/cleaning agents or leave
theircontainersuncovered. Immediately remove
spilled sample/cleaning agents.
• Make sure that the setup location is sufficiently
ventilated. The environment of ViscoQC 300

1 Safety Instructions
C78IB007EN-B 7
must be kept free of inflammable gases and
vapors.
• Connect ViscoQC 300 to the mains via a safety
switch located at a safe distance from the instru-
ment. In an emergency, turn off the power using
this switch instead of the power switch on
ViscoQC 300.
• Supply a fire extinguisher.
• Ensure the sufficient supervision of
ViscoQC 300 during operation.
1.2 Special Safety Instructions
• Do not use ViscoQC 300 to measure fluids of
the IIC group according to EN 60079-14, such
as e.g. carbon disulfide or acetylene.
• Move the head up an down using the hand
wheel on the head.
• To move or lift ViscoQC 300, grasp the rod of
the stand with one hand and the foot of the
stand with the other hand. Do not take
ViscoQC 300 by the measuring head, nor by the
spindle guard.
• Carry ViscoQC 300 in front of you and keep it
close to your body.
• Disconnect spindles or measuring systems by
pulling them sideways. This reduces strain on
and wear of the internal low-friction bearing.
1.3 Safety Signs on the Instrument
No safety sign on ViscoQC 300.
Optional equipment – Stainless steel bath cover for
600 mL beaker (use with optional bath thermostat):
1 Warning Hot Surface
Fig. 1: Safety sign on optional stainless steel bath cover
1.4 Conventions for Safety Messages
The following conventions for safety messages are
used in this manual:
1.5 Remaining Risks
Droppingtheinstrumentmightcauseinjuriestoyour
feet.
Knocking over the ViscoQC 300 might cause dam-
age to other lab equipment due to the instrument’s
weight. If measuring hazardous samples, take care
not to knock over the sample vessel. The spillage of
hazardous samples represents a serious health
risk.
1
WARNING
Risk of injury, health risk
If measuring at high temperatures, the bath
cover and bath liquid are hot. Keep clear of the
bath tank. Wait until the bath liquid has reached
an uncritical temperature before you handle any
parts. Use suitable protective equipment.
Adhere to all safety instructions in the bath’s
documentation.
DANGER
Description of risk.
Danger indicates a hazardous situation which, if
not avoided, will result in death or serious injury.
WARNING
Description of risk.
Warning indicates a hazardous situation which, if
not avoided, could result in death or serious
injury.
CAUTION
Description of risk.
Caution indicates a hazardous situation which, if
not avoided, could result in minor or moderate
injury.
NOTICE
Description of risk.
Notice indicates a situation which, if not avoided,
could result in damage to property.

2 ViscoQC 300 - An Overview
8C78IB007EN-B
2 ViscoQC 300 - An Overview
ViscoQC 300 is a rotational viscometer that deter-
mines the dynamic (apparent) viscosity as multiple
points. The instrument serves for quality control of
liquid samples such as solvents up to semi-solid
substances such as lotions.It returns instant results
on a built-in color screen. Measured data are stored
in the data memory and can be printed or exported
as .csv or .pdf format. LIMS Bridge Software allows
the data transfer for implementation in LIMS.
The Toolmaster™ system automatically recognizes
connected measuring systems (spindles and cylin-
dersystems).APt100temperaturesensor allows to
monitor the temperature of the measured sample.
A magnetic coupling serves as connection for spin-
dles or measuring systems. This reduces the risk to
bend or damage parts.
Optional software packages for additional functions:
• V-Curve: online graph of real time measurement
data, programmability of up to 50 steps, mathe-
matical models and yield stress determination
with vane spindles (see also p. 18)
• V-Comply: joint with pharma qualification pack-
age for perfect traceability and to fulfill regula-
tions of FDA 21 CFR part 11
If ViscoQC 300 has been ordered together with a
software package, you need not activate it upon de-
livery. If upgrading existing devices, you get an un-
lock code. The first 8 characters of the code are the
serial number of the ViscoQC 300. See "Activate
Software Packages", p. 38.
Fig. 2: Rotational viscometers: ViscoQC 300
2.1 Intended Use of the Instrument
ViscoQC 300 is an instrument for determination of
dynamic viscosity. It can measure a wide range of
viscous and viscoelastic samples within the speci-
fied measuring range. There are three different
models available for different viscosity measuring
ranges (L – low, R – regular, and H – high). These
ranges depend on the torque range of the model.
See appendix A.
CAUTION
Risk of injury, health risk
Using chemically or biologically hazardous
chemicals as samples or cleaning liquids is a
health risk. Measuring at high (> 40 °C) or low
temperatures (< 0 °C) is a health risk.
The above risks could cause serious injuries
unless special precautions are taken.
Consult the material safety data sheets of the
sample substances and cleaning liquids.
Operate the ViscoQC 300 in a fume hood and
make sure to use suitable protective equipment.
Wear protective gloves
Wear protective gloves when handling
samples and cleaning liquids.
Wear safety goggles
Wear safety goggles when handling
samples and cleaning liquids.
Use protective clothing
Use protective clothing when handling
samples and cleaning liquids.

2 ViscoQC 300 - An Overview
C78IB007EN-B 9
2.2 Functional Components
1 ViscoQC 300 measuring head
2 Measuring head retention
3 Hand wheel – move the measuring head up or down
4 Rod of stand
5 Foot of stand
6 Leveling screws – level the ViscoQC
7 Spindle coupling (magnetic)
8 Touch screen
Fig. 3: ViscoQC 300 – front view
Turn the hand wheel (3) to move the measuring
head up or down. If you are in front of ViscoQC, turn
the hand wheel towards you to lower the head; turn
the hand wheel away from you to lift the head.
1 ViscoQC 300 measuring head
2 Power switch
3 Power inlet
4 Interface for Pt100 temperature sensor
5 USB interface (3x) – to connect optional 2D bar code
reader, external keyboard, or USB printer for data
export to USB device. Also for firmware update from
storage device.
6 PC interface (for V-Collect Software)
7 CAN interface for optional accessories
8 Mount for spindle guard or measuring cup on the
measuring flange
9 Type plate with serial number
10 Ethernet interface – for connection to a network
printer or LIMS bridge software
Fig. 4: ViscoQC 300 – rear view
NOTICE
Risk of damage to the instrument
• Do not test a sample if you do not know which
cleaning liquid removes this sample. Make
sure the wetted parts of ViscoQC 300 are
chemically resistant to any tested sample or
cleaning liquid.
• Do not test any samples which harden or
solidify during the time they are in contact
with parts of ViscoQC 300.
• Do not test any samples that are specified in
section 1.2.
1
2
3
4
8
5
6
7
1
5
6
4
2
9
8
3
7
361 mm
444 mm
281 mm
10

3 Checking the Supplied Parts
10 C78IB007EN-B
3 Checking the Supplied Parts
ViscoQC 300 was tested and packed carefully be-
fore shipment. However, damage may occur during
transport.
1. Keep the packaging material (box, foam piece,
transport protection) for possible returns and
further questions from the transport and insur-
ance company.
2. Check the delivery for completeness by compar-
ing the supplied parts to those noted in table 1.
TIP: Concentric cylinder systems, the double-gap
system and other accessories have to be ordered
separately and are not included in the below table.
Check these parts using the delivery note.
3. If a part is missing, contact your Anton Paar rep-
resentative.
4. If a part is damaged, contact the transport com-
pany and yourAnton Paar representative.
Table 1: Supplied Parts
Symbol Pcs. Article Description Mat. No.
1ViscoQC 300 - L a
or
ViscoQC 300 - R a
or
ViscoQC 300 - H a
(with transport protection for magnetic coupling – see
arrow)
105023
105024
105025
1Viscometer stand (see above picture) 189184
1Set L-spindles – supplied with ViscoQC 300 - L:
consisting of 4 spindles L1 to L4
or
Set RH-spindles – supplied with ViscoQC 300 - R / H:
consisting of 6 spindles RH2 to RH7
190845
190846
1Set of torque range stickers L / R / H
Find this set on the front page of this instruction manual.
189804
1Power supply unit with connection cable to ViscoQC
(comes in a cardboard box – a reminder to remove the
ViscoQC transport protection covers the box)
186547