Kinematica POLYTRON SYSTEM PT 1300 D User manual

Instruction Manual for
POLYTRON®System PT 1300 D
Voltage
90 –260 V, 50/60 Hz
Make sure the power supply is correct and corresponds with the
technical data plate on the instrument
This is a quality product of:
Luzernerstrasse 147a Tel.: [phone]
CH-6014 Lucerne Fax: [phone]
Switzerland E-mail:[email protected]

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INDEX: PAGE:
1INTRODUCTION......................................................................................................................................... 3
1.1 OPERATING INSTRUCTIONS................................................................................................................ 3
1.2 ORGANISATIONAL MATTERS .............................................................................................................. 5
1.3 WARNING NOTICES............................................................................................................................... 6
2SAFETY ...................................................................................................................................................... 6
2.1 SUMMARY............................................................................................................................................... 7
2.2 SAFETY CONCEPT................................................................................................................................. 7
2.3 RESIDUAL DANGERS .......................................................................................................................... 10
2.4 WARNINGS............................................................................................................................................ 11
3USE ........................................................................................................................................................... 13
3.1 DESCRIPTION ........................................................................................................................................... 13
3.2 POLYTRON-AGGREGATES ................................................................................................................... 13
3.3 OPTION STAND ST-P00/200..................................................................................................................... 15
3.4 TECHNICAL SPECIFICATIONS.................................................................................................................. 16
4INSTALLATION........................................................................................................................................ 17
4.1 UNPACK................................................................................................................................................ 17
4.2 COUPLING/DECOUPLING OF THE HOMOGENIZING AGGREGATE................................................ 17
4.3 WORKING WITH THE PT 1300 D.......................................................................................................... 18
5MAINTENACE .......................................................................................................................................... 22
5.1 MAINTENACE OF THE SUPPLY AND CONTROL UNIT...................................................................... 22
5.2 MAINTENACE OF THE CONTROL AND OPERATING MODULE ....................................................... 22
5.3 MAINTENACE OF THE POLYTRON-AGGREGATES............................................................................ 22
5.4 DISASSEMBLY INSTRUCTIONS ......................................................................................................... 23
5.5 ASSEMBLY INSTRUCTIONS......................................................................................................................... 23
6TROUBLE SHOOTING............................................................................................................................. 24
7general accessories................................................................................................................................ 25
8Guarantee................................................................................................................................................. 25
1Appendix..................................................................................................Fehler! Textmarke nicht definiert.
1.1 LEGEND TO THE DRAWING OF PT1300D AND ST-P00/200...................FEHLER!TEXTMARKE NICHT DEFINIERT.
1.2 LEGEND TO THE DRAWINGS OF PT-DA05/2EC.., 07/2EC.., 12/2EC.., 12/2 .. ECFEHLER!TEXTMARKE NICHT
DEFINIERT.
2Appendix: control with rs-232-interface ............................................................................................... 31
2.1 SYSTEM DESCRIPTION........................................................................FEHLER!TEXTMARKE NICHT DEFINIERT.
2.2 HOST INTERFACE ..............................................................................FEHLER!TEXTMARKE NICHT DEFINIERT.
2.3 COMMUNICATING RULES.....................................................................FEHLER!TEXTMARKE NICHT DEFINIERT.
2.4 DIFFERENCE BETWEEN SET RPM AND CURRENT RPM (*).......................FEHLER!TEXTMARKE NICHT DEFINIERT.
2.5 ERROR TREATMENT............................................................................FEHLER!TEXTMARKE NICHT DEFINIERT.
2.6 COMMAND SAMPLES ..........................................................................FEHLER!TEXTMARKE NICHT DEFINIERT.
3Appendix: control with MODBUS-interface..........................................Fehler! Textmarke nicht definiert.
3.1 IMPLEMENTATION ..................................................................................................................................... 34

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1 INTRODUCTION
This chapter gives information on the structure of this document. It will assist you in
making use of it and show how to find the required information quickly.
1.1 OPERATING INSTRUCTIONS
PLEASE READ THESE OPERATING INSTRUCTIONS BEFORE SWITCHING ON OR
OPERATING THE EQUIPMENT. THEY DESCRIBE THE USE OF THE POLYTRON
PT 1300 D, ITS INSTALLATION AND MAINTENANCE AND THE APPROPRIATE
REPLACEMENT PARTS AND ACCESSORIES. THEY WILL HELP YOU AVOID
ERRONEOUS USE AND SUBSEQUENT DAMAGE. ALTHOUGH POLYTRONUNITS
ARE DESIGNED FOR EASE OF SERVICE, THIS DOES NOT RELEASE YOU FROM
THE OBLIGATION TO INSPECT YOUR EQUIPMENT CAREFULLY AND TO CLEAN IT
THOROUGHLY.
KINEMATICA AG is a specialist manufacturer of machines and equipment for dispersion
and mixing technology.
An important objective of these operating instructions is to fully inform you, the user, about
the correct and safe use of our equipment.
In order to achieve this, it is essential that you should carefully study chapter 2, “Safety”,
and follow the instructions in this book.

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1.1.1 RANGE OF VALIDITY
The information in these operating instructions relates to the POLYTRON®identified as
follows:
Manufacturer: KINEMATICA AG, CH-6014 Luzern
Brand name: POLYTRON®
Product name: POLYTRON®PT 1300 D & POLYTRON®PT 1300 D RS232
Artikelnummer
Bezeichnung
11010030
PT 1300 D, MODBUS (with EU-Plug)
11010031
PT 1300 D, MODBUS (with CH-Plug)
11010039
PT 1300 D, MODBUS (with UK-Plug)
11010032
PT 1300 D, MODBUS (with EU-Plug, customer-specific)
Dispersing Aggregates (choice)
11030004
PT-DA 03/2EC-E050
11030012
PT-DA 05/2EC-E085
11030009
PT-DA 05/2EC-E068
11030031
PT-DA 07/2EC-E107
11030024
PT-DA 07/2EC-E092
11030030
PT-DA 07/2SYN-E082
11030062
PT-DA 12/2EC-E123
11030042
PT-DA 12/2EC-E157
11030266
PT-DA 12/2MEC-E157
11030060
PT-DA 12/2WEC-E157
Stands
11040012
ST-P01/200 –Hinge Stand
11040011
ST-P12/600 –Metal plate Stand specifically for the PT1300D
11040013
ST-P15/320 –Plate Stand
ATTENTION:
The new Unit is not exchangeable with the old one. The new unit has a new
designed supply module.

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1.1.2 TARGET AUDIENCE
These operating instructions are intended for all authorised users of our
machines/equipment. We distinguish different user roles, taking account of the different
demands placed on the user by the activity to be carried out.
You will find the definitions of user roles with the demands on the user in chapter 2,
“Safety”. You can fulfil one or more of these roles, provided that you meet the
corresponding demands.
1.2 ORGANISATIONAL MATTERS
If you are unable to find the answer to any question in the operating instructions, please
contact the equipment manufacturer directly.
1.2.1 LOCATION OF THE OPERATING INSTRUCTIONS
The operating instructions can only be of use to you if you always have them at hand.
They should therefore always be kept at the place where the equipment is used.
1.2.2 MANUFACTURER CONTACT ADDRESS
KINEMATICA AG
Luzernerstrasse 147a
CH-6014 Lucerne
TEL: [phone]
FAX: [phone]
e-mail: [email protected]

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1.3 WARNING NOTICES
Please be aware of the meaning of the following warning signs:
SAFETY INSTRUCTIONS MUST BE OBSERVED TO
ENSURE SAFE OPERATION.
THIS SYMBOL INDICATES HIGH VOLTAGE, WITH
RISK TO HEALTH AND ENVIRONMENT.
CAUTION!
BEWARE OF HOT SURFACE.
CAUTION!
DEVICE NOT DESIGNED FOR USE IN
EXPLOSION DANGER ENVIRONMENT.
2 SAFETY
This chapter is directed at all users of KINEMATICA laboratory equipment. It includes
information on safe and optimum use.

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2.1 SUMMARY
Any incorrect use of the installed equipment can be dangerous. Inadequately trained users
can cause material damage and personal injury. This chapter informs you about the safety
concept and the requirements for safe and optimum use of the equipment.
All those authorised to operate, service and repair the equipment are required to study
chapter 2, “Safety”.
2.2 SAFETY CONCEPT
The safety concept sets down the entitlement to use the equipment and the responsibilities
of the individual users.
The machines and equipment are designed and constructed according to the state of the
art and the recognised safety rules.
2.2.1 INTENDED USE OF THE EQUIPMENT
The equipment is designed and constructed for the following use:
Dispersion and homogenisation of pumpable fluid products in accordance with the
technical specifications (see point 3.2) and compatibility with the materials coming
into contact with the products.
If you use the equipment for any purpose other than those listed, the manufacturer cannot
be held liable for any resulting damage.
2.2.2 IMPROPER USE
Any use other than the “intended use” without the written approval of the manufacturer or
any operation outside the technical limits of use is improper use.
2.2.3 USER ROLES
To guarantee safety, we place requirements on the users of the equipment that must be
met without fail. Only persons meeting the requirements are authorised to work with the
equipment.
We describe all those who work with the equipment as users. Since the requirements of
these users are very much dependent on their activity, we distinguish the following user
roles.

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Contract partner:
The manufacturer can impose legal obligations on the contract partner when the
equipment is purchased. The contract partner is obliged to ensure that the equipment is
properly used.
Operating company:
The operating company ensures that the equipment is properly used and authorises
persons who are entitled to work with the equipment in any one of the defined user roles.
They are under the obligation to instruct the users.
Note:
Contract partner and operating company can be the same person.
Service technician:
The service technician is an employee of the operating company and looks after the
equipment in special operating mode(s). He is a specialist with mechanical, electrical and
electronic professional training. The service technician undertakes commissioning,
decommissioning service and repair of the equipment. He must be appropriately trained to
be able to carry out the service work required.
Operator:
The operator turns the equipment on and off. In the event of an alarm signal he informs the
service technician.

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2.2.4 DANGER AREA
System/equipment
The system danger area includes the whole system/equipment including the connecting
lead and controls.
Proximity danger area
This refers to all areas within a defined distance of the equipment.
User danger area
This danger area includes all persons working with the equipment.
2.2.5 AREAS OF RESPONSIBILITY
In order that the system/equipment can be used safely and without risk, the users in
various roles bear the responsibility for particular danger areas.
Contract partner:
The contract partner bears the responsibility for the “proximity danger area”.
Operating company:
The operating company bears the responsibility for the “user danger area”. Only those
users may be authorised to operate the system/equipment who fulfil all requirements of the
user roles concerned. In doing so, attention must be paid to the following points:
It is to be ensured that all users of the system/equipment have fully read and
understood chapter 2, “Safety” and act accordingly in a safety-conscious manner.
It is to be ensured that no unauthorised person carries out work with the
system/equipment.
It is to be ensured that users are informed of the possible risks and dangers
connected with the system/equipment.
It is to be ensured that those being trained or engaged in general training are under
the permanent supervision of a trained and authorised person.
Service technician:
The service technician bears the responsibility for the “system/equipment danger area”. He
ensures that the system/equipment is at all times free from technical faults, safe and
functions correctly.

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2.2.6 GENERAL SAFETY RULES
Observe the following general safety rules:
follow these operating instructions,
in addition, observe the legal obligations and requirements for accident prevention
and environmental protection of the country in which you operate the equipment,
do not make any modifications to the equipment without the written authorisation of
the manufacturer,
only original replacement parts may be used for repairs,
before any service work on the equipment, it must be ensured that the electrical
supply is switched off,
after any service, maintenance or repair work has been carried out on the
system/equipment, it must be given a test run by the service technician.
depending on the place at which it is installed, circumstances may require that
hearing protection is worn when remaining in the vicinity of the equipment for long
periods.
2.3 RESIDUAL DANGERS
When the system/equipment is used in accordance with rules and regulations, residual
dangers are minimal.
Residual danger
Countermeasures
Tripping over feed or
return lines
These should be laid appropriately.
Breakage of glass
containers
Wear protective clothing
(goggles etc.).
Spitting of the product
Hearing loss due to loud
noise.
According to the application
ear protection must be used.
Tilting of the device
Use stable, non-slip base
IN EVERY CASE THE ELECTRICAL INSTALLATION HAS
TO BE DONE BY TECHNICIAN!

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2.4 WARNINGS
Ensure that the rated voltage of the equipment matches the supply.
Before changing any dispersing aggregate, the line cord has to be
plugged out
IT IS IMPORTANT THAT THE MAINS SUPPLY WHERE THE DEVICE
IS PLUGGED IN COMPLIES WITH THE INFORMATION ON THE
TYPE LABEL AND THE INTERNATIONAL STANDARDS FOR POWER
SUPPLIES. IF NOT, SUCCESSFUL OPERATION CANNOT BE
GUARANTEED
In the event that hazardous chemicals or materials that endanger health
can influence the surroundings or use of the equipment, appropriate
countermeasures must be taken.
At long term use the aggregate and the coupling may get hot –danger
of skin burn.
The equipment may not be operated in explosive areas
It is not allowed to work with fluids, which are highly inflammable.
It is not allowed to mix materials which can cause strong exothermal
reactions
WARNINGS: TO BE CONTINUED ON NEXT PAGE

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WARNINGS: CONTINUED
THE DEVICE MAY ONLY BE OPENED BY AUTHORISED
KINEMATICA SERVICE STATIONS.
Ensure that enough free space is available at the backside of device, so
that effective airflow and cooling is assured. Insufficient cooling may
lead to a decrease of power output.
The device has to be placed in a manner that dirt or fluids cannot
penetrate through the ventilation slots at backside of the drive.
Before changing any dispersing aggregate, the line cord has to be
plugged out
POLYTRONdispersion aggregates may not be operated dry –the
lower sleeve bearing is cooled and lubricated by the medium being
processed. Running dry will destroy the sleeve bearing.
The dispersing aggregates should be cleaned after every operation.
Never pull the coupling during operation –the aggregate could fall out
of the coupling.
Never place the handheld horizontally or vertically with engaged
aggregate. By non-use of the handheld always provided in the recess at
the base station. Fluid is running in the motor and the life of the engine
is greatly reduced.
The handheld of version 2 is not interchangeable with the new base
station.
The handheld of version 3 is not interchangeable with the old base
station.
When the line cord is plugged, never touch the saw teeth of the
aggregate –danger of injuries due to rotating shafts and blades
KINEMATICA AG products comply with all the usual CE directives,
carry the CE marking and are delivered with a corresponding
declaration of conformity.

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3 USE
POLYTRONPT 1300 D handheld units are specially designed for the dispersing,
homogenizing, suspending, emulsifying, decomposing and mixing of organic and inorganic
sample material in small quantities.
3.1 DESCRIPTION
The POLYTRONPT 1300 D consists of a microprocessor-controlled supply and control
module and a high-performance low-voltage drive with a control and operating module
including an LED display as well as a selection of three different homogenizing
aggregates. A hinged stand, a plate stand and a metal plate stand are also available as an
option.
For a ready-to-use system you need:
Control module (Handheld)
Supply module (Base station)
A dispersing aggregate
A mains connection according to the type label
3.2 POLYTRON

-AGGREGATES
Dispersing units (choice)
PT-DA
03/2EC-E50
PT-DA
05/2EC-E68
PT-DA
05/2EC-E85
PT-DA
07/2SYN-E082
PT-DA
07/2EC-E092
Shaft length, mm
50
68
85
82
92
Stator/Rotor
Ø, mm
2.2/3.5
5.5/3
5.5/3
7.8/5
7.8/5
Processing
volume
approx.
0.05 –2 ml
Ca.
0.1 –3 ml
Ca.
0.1 –3 ml
Ca.
0.5 –10 ml
Ca.
0.5 –10 ml
Notes
-
-
-
Synthetik
Temperature
up to about 90 °C processing temperature
Pressure
not pressurised
Materials
stainless steel 1.4435 (316L) and PTFE compound
Cleaning
can be sterilised by all the usual methods, e.g. autoclave
Product
requirements
The product to be dispersed must be pumpable and fluid and must not
contain any solid particles that might destroy the attachment.

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Dispersing units (choice)
PT-DA
07/2EC-E107
PT-DA
12/2EC-E123
PT-DA
12/2EC-E157
PT-DA
12/2MEC-E157
PT-DA
12/2WEC-E157
Shaft length, mm
107
123
123
123
123
Stator/Rotor Ø,
mm
7.8/5
12/9
12/9
12/9
12/9
Processing
volume
Ca.
0.5 –10 ml
Ca.
3 –250 ml
Ca.
3 –250 ml
Ca.
3 –250 ml
Ca.
3 –250 ml
Notes
-
-
-
Knife Rotor
W-Geometry
Temperature
up to about 90 °C processing temperature
Pressure
not pressurised
Materials
stainless steel 1.4435 (316L) and PTFE compound
Cleaning
can be sterilised by all the usual methods, e.g. autoclave
Product
requirements
The product to be dispersed must be pumpable and fluid and must not
contain any solid particles that might destroy the attachment.
3.3 STAND ST-P01/200
POLYTRONPT 1300 D handhelds can be supplemented with the joint stand ST-
P01/200. The stand consists of the following components:
Baseplate
Pivotable articulated arm with the possibility of right, left, up, down movement
Motor mounting with adjustable pitch up to approx. 15°
The stand should allow for a higher degree of flexibility at the workplace. The drive only
needs to be plugged into the provided socket.
Make sure that the dive cable is attached to the cable holder
on the arm so that it can not enter into the working area.
Make sure that the mounting screw on the rear side of the
stand has been tightened firmly so that the stand arm cannot
move away during operation. (see the installation drawing
enclosed)
See under Appendix, Chapter 10

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3.4 STAND ST-P12/600
POLYTRONP T 1300 D handheld units can be used with the optinal plate stand ST-
P00/200. The stand consists of the following components:
Baseplate
Stand column with a maximum stroke of about 550mmMotor mounting with
drive holder with the option of left, right, up and down movement
The stand should allow for a higher degree of flexibility at the workplace. The drive only
needs to be plugged into the provided socket.
As an option, the following components are available:
Cross sleeve complete for the attachment of a vessel holder
Vessel holder
An adjustment ring for precise positioning of the handset
Make sure that the mounting screw on the rear side of the
stand has been tightened firmly so that the stand arm cannot
move away during operation. (see the installation drawing
enclosed)
See under Appendix, Chapter 10
3.5 STAND ST-P15/320
POLYTRONPT 1300 D handheld units can be used with the optinal plate stand ST-
P15/320. The stand consists of the following components:
Baseplate with stand
Drive holder with the possibility of moving up and down
Ability to provide the base station to the base plate
The stand should allow for a higher degree of flexibility at the workplace. The drive only
needs to be plugged into the provided socket.

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Make sure that the mounting screw on the rear side of the
stand has been tightened firmly so that the stand arm cannot
move away during operation. (see the installation drawing
enclosed)
3.6 TECHNICAL SPECIFICATIONS
POLYTRONPT 1300 D
motor type
Brushless DC-motor, electronically commuted
supply voltage
90-260VAC
fuse
2.5 A T (Passive)
supply frequency
50/60 Hz
input power
100 W
output power
50 W
max. speed
2'000 to ca. 30'000 rpm infinitely adjustable
direction of rotation
clockwise, seen from above
ambient temperature
0 –40°C
relative humidity
Max. rel. 95%
standards
EMV: certified by IEC/EN 61000-6-1 / 61000-6-3 / 61326-1
Safety: certified by IEC/EN 61010-2-51 & 61010-1
protection type
IP 20
max. period of continuous
operation
100%
Noise emission
70 dB (A) with full rotational speed with aggregate
PT-DA12/2EC-E157 in H2O
ON/OFF Switch
separate at control- and operating module
Current consumption
max. 0.5 A at 230 V
max. 1 A at 100-120 V
Interface
Standard MODBUS, Optional RS 232
weight (drive only)
control module 1033 g / operating module 568 g

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4 INSTALLATION
4.1 UNPACK
Open the dispatch box and check that the contents agrees with the delivery note.
CHECK ALL PARTS FOR POSSIBLE TRANSPORT
DAMAGE. INFORM US OR YOUR DEALER IMMEDIATELY
ABOUT ANY DISAGREEMENT OR FAULT. IF POSSIBLE
SEND US DIGITAL PHOTOS BY EMAIL TO
[e-mail]
4.2 COUPLING/DECOUPLING OF THE HOMOGENIZING AGGREGATE
All POLYTRONPT 1300 D handheld units are equipped with quick-coupling.
Dispersing aggregates with diameters of 3, 5, 7 and 12 mm are available for the
PT 1300 D drive unit. All aggregates are connected to the drive in exactly the same
manner.
For assembly, while at a standstill, the coupling ring is pushed in the direction of the drive
and the coupling part of the aggregate is pushed completely into that of the drive. The
coupling ring snaps forwards again if the connection has been made properly (see the
enclosed assembly sketch).
BEFORE STARTING WORK, MAKE SURE THAT THE
AGGREGATE IS CONNECTED PROPERLY WITH THE
DRIVE. AN INCORRECT CONNECTION CAN DAMAGE THE
COUPLING PARTS OF THE DRIVE OR THE
HOMOGENIZING VESSEL.

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To remove the aggregate from the drive, push the retaining ring of the coupling upward
and/or in the direction of the drive. At the same time, the aggregate is to be carefully pulled
downward in the axial direction so that the homogenizing aggregate is not tilted in the
coupling housing (see the enclosed assembly sketch).
WITH PUSHING UP OF THE COUPLING RING, THE
AGGREGATE CAN UNINTENTIONALLY FALL OUT OF THE
COUPLING. FOR THIS REASON, ALWAYS HOLD IT WITH
ONE HAND.
THE SAW-TEETH OF THE STATOR ARE GROUND TO BE
SHARP. THERE IS THE DANGER OF INJURY WITH
IMPROPER HANDLING.
4.3 WORKING WITH THE PT 1300 D
Connect your corresponding homogenising aggregate.
Along with the drive unit, you also have the control in your hand. Firstly check for a
proper connection of the supply and control module and the drive unit, then switch
on the main switch on the supply and control module (green light).
When you turn on, the display shows the selected firmware version for example
C01
POLYTRON-DISPERSING AGGREGATES MAY NOT BE
USED IN THE DRY STATE –THE LOWER SLIDE BEARING
ARE COOLED AND LUBRICATED BY THE LIQUID PHASE
OF THE PROCESSES MEDIUM.
Guide the connected aggregate into the medium to be processed. The optimal
submersion depth of the aggregate is approx. 2/3 below the liquid surface and 1/3
above the vessel bottom. By submerging at an angle of approx. 15°, the degree of
effectiveness can additionally be improved.

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THE MAXIMUM SUBMERSION DEPTH IS BENEATH THE
UPPER SCAVENGING HOLE OF THE STATOR TUBE.
Switch on the control and operating module by using the ON/OFF switch. The unit
now runs at the lowest rotational speed of 2000 rpm. Once the ON / OFF button is
pressed the fan runs. This is required so that the motor is cooled in a continuous
operation.
WHEN THE LINE CORD IS PLUGED, NEVER TOUCH THE
SAW TEETH OF THE AGGREGATE –DANGER OF
INJURIESDUE TO ROTATING SHAFTS AND BLADES
After done work the handheld is turned off with the ON / OFF button. The unit stops
and the display shown OFF. The fan runs about 1 minute, then it stops
automatically.

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4.4 FUNCTIONAL DESCRIPTION OF THE KEY
With the ON/OFF switch, turn on the control and operating module as
soon as the main switch has been turned on at the supply and control
module.
The rotational speed will be 2’000 rpm if the PT 1300 D has
meanwhile been switched off by means of the main switch, otherwise
the control and operating module uses the last set rotational speed.
With the ON/OFF switch, turn the control and operating module off
again. The fan runs about 1 minute and then it stops automatically.
If the control and operating module has not bees used for a longer
period of time, you should additionally switch off the main switch on
the basis station.
With the UP key, you can increase the rotational speed of the control
and operating module in 100 rpm steps.
The speed range is from 2’000 to 30’000 rpm.
The rotational speed increases quicker when you press the switch.
With the DOWN switch, you can decrease the rotational speed of the
control and operating module in 100 rpm steps.
The speed range is from 2’000 to 30’000 rpm.
The rotational speed decreases quicker when you press the switch.
By continually pressing the MEMO switch (approx. 1 sec.), you can
store the current rotational speed. Storage of the rotational speed is
confirmed by flashing (3 times) of the display.
A stored rotational speed can be loaded by shortly pressing the
MEMO switch (approx. 1 sec.)
The maximum rotational speed depends on the size of the dispersing
aggregate, the type of product and viscosity. With deviations from the
programmed rotational speed, e.g. by means of a strong rise in
viscosity, the digital display flashes, which means that the preset
rotational speed will not be reached any longer. With overloading of
the drive, it is switched off by means of a thermal fuse.
ON/OFF
UP
DOWN
MEMO