Olympus BIX III User manual

International edition
10-015490-01EN — Rev. 2
June 2020
BTX III
X-Ray Diffraction Analyzer
User’s Manual
This instruction manual contains essential information on how to use this Olympus product safely and effectively.
Before using this product, thoroughly review this instruction manual. Use the product as instructed.
Keep this instruction manual in a safe, accessible location.

Olympus Scientific Solutions Americas, 48 Woerd Avenue, Waltham, MA 02453, USA
Copyright © 2020 by Olympus. All rights reserved. No part of this publication may be
reproduced, translated, or distributed without the express written permission of Olympus.
This document was prepared with particular attention to usage to ensure the accuracy of the
information contained therein, and corresponds to the version of the product manufactured
prior to the date appearing on the title page. There could, however, be some differences
between the manual and the product if the product was modified thereafter.
The information contained in this document is subject to change without notice.
International edition
Part number: 10-015490-01EN
Rev. 2
June 2020
Printed in the United States of America
SwiftMin is a registered trademark of the MinEx CRC. All brands are trademarks or
registered trademarks of their respective owners and third party entities.

Table of Contents iii
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Table of Contents
List of Abbreviations ...................................................................................... vii
Labels and Symbols ........................................................................................... 1
Important Information — Please Read Before Use ..................................... 5
Intended Use .......................................................................................................................... 5
Instruction Manual ................................................................................................................ 5
Instrument Compatibility ..................................................................................................... 6
Repair and Modification ....................................................................................................... 6
Safety Symbols ....................................................................................................................... 7
Safety Signal Words .............................................................................................................. 7
Note Signal Words ................................................................................................................ 8
Safety ....................................................................................................................................... 9
Warnings ................................................................................................................................. 9
Richtlinien für den Strahlenschutz im deutschsprachigen Raum ................................ 11
Deutschland ........................................................................................................... 11
Österreich ............................................................................................................... 11
Schweiz ................................................................................................................. 12
Equipment Disposal ............................................................................................................ 12
CE (European Community) ............................................................................................... 13
WEEE Directive .................................................................................................................... 13
China RoHS .......................................................................................................................... 13
Korea Communications Commission (KCC) ................................................................... 14
KCC (South Korea Community) ....................................................................................... 14
EMC Directive Compliance ................................................................................................ 15
FCC (USA) Compliance ...................................................................................................... 15
ICES-001 (Canada) Compliance ........................................................................................ 16
Packing and Return Shipping ............................................................................................ 16
Open Source Software ......................................................................................................... 17
Warranty Information ......................................................................................................... 17

Table of Contentsiv
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Technical Support ................................................................................................................ 18
Introduction ...................................................................................................... 19
1. Analyzer Overview .................................................................................... 21
1.1 Packing List ................................................................................................................ 21
1.2 Front/Top Panel ......................................................................................................... 23
1.2.1 Power Key Switch .......................................................................................... 24
1.2.2 Keypad ............................................................................................................. 24
1.2.3 Stop/Emergency Shutoff Button .................................................................. 25
1.2.4 LED Indicators ................................................................................................ 25
1.2.5 Sample Chamber ............................................................................................ 26
1.2.6 Display ............................................................................................................. 26
1.3 Rear Panel ................................................................................................................... 26
2. Safety Information ..................................................................................... 29
2.1 Radiation Safety Information .................................................................................. 29
2.2 Safety Interlocks ........................................................................................................ 30
2.3 Radiation Dose Measurements ............................................................................... 33
3. Set Up and Operation ................................................................................ 35
3.1 Connecting AC Power to the BTX III ..................................................................... 35
3.2 Turning On or Off the BTX III ................................................................................. 37
3.3 Preparing a Sample for Analysis ............................................................................ 38
3.4 Loading a Sample ...................................................................................................... 39
3.5 Testing a Sample ........................................................................................................ 45
3.6 Unloading a Sample ................................................................................................. 48
4. Local Area Network Communication .................................................... 49
4.1 Checking the Network Configuration ................................................................... 50
4.2 Connecting to your LAN through the Ethernet Connector ................................ 51
4.3 Broadcasting a WLAN through a Wireless LAN Dongle ................................... 52
4.4 Connecting your PC to the WLAN ......................................................................... 53
5. SwiftMin® Software User Interface ....................................................... 57
5.1 Opening and Closing the SwiftMin® Software User Interface .......................... 57
5.2 SwiftMin® User Access Levels ................................................................................ 58
5.2.1 Default Access ................................................................................................. 58
5.2.2 Manager Access .............................................................................................. 59
5.3 Using the SwiftMin® Software ............................................................................... 60
5.3.1 Screen Tabs ...................................................................................................... 61

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5.3.2 Default Access Workflow ............................................................................. 61
5.3.3 Manager Access Workflow ........................................................................... 64
5.3.3.1 Mineral Config Tab ............................................................................. 65
5.3.3.2 Mode Setup Tab ................................................................................... 68
5.3.4 Changing the User Interface Language ...................................................... 73
Appendix A: Specifications ........................................................................... 75
Appendix B: About Powder XRD Testing ................................................... 77
Appendix C: Data Analysis ............................................................................ 79
List of Figures ................................................................................................... 89
List of Tables ..................................................................................................... 91
Index ................................................................................................................... 93

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10-015490-01EN, Rev. 2, June 2020
List of Abbreviations vii
List of Abbreviations
ALARA as low as reasonably achievable
AMCSD American Mineralogist Crystal Structure Database
BAG Bundesamt für Gesundheit (Schweiz)
CCD charge-coupled device
DHCP dynamic host configuration protocol
EFUP environment-friendly use period
FWHM full width at half maximum
HVPS high-voltage power supply
LAN local area network
OSS open source software
PXRD powder X-ray diffraction
RIR reference intensity ratio
RöV Röntgenverordnung (Deutschland)
StrSchG Strahlenschutzgesetz (Österreich)
SUVA Schweizerische Unfallversicherungsanstalt
WLAN wireless local area network
XRD X-ray diffraction

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List of Abbreviationsviii

10-015490-01EN, Rev. 2, June 2020
Labels and Symbols 1
Labels and Symbols
Safety-related labels and symbols are attached to the BTX III X-ray diffraction
analyzer (see Figure i-1 on page 1). If any of the labels or symbols are missing or
illegible, please contact Olympus.
Figure i-1 X-ray warning labels
The rating label is attached to the BTX III analyzer. The label symbols are described in
Table 1 on page 2.

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Labels and Symbols2
Table 1 Content of the rating label
Item Description
This device complies with Part 15 of the FCC Rules.
Operation is subject to the following two conditions: (1) this
device may not cause harmful interference, and (2) this
device must accept any interference received, including
interference that may cause undesired operation.
The CE marking is a declaration that this product conforms
to all the applicable directives of the European Community.
See the Declaration of Conformity for details. Contact your
Olympus representative for more information.
The WEEE symbol indicates that the product must not be
disposed of as unsorted municipal waste, but should be
collected separately.
The regulatory compliance mark (RCM) label indicates that
the product complies with all applicable standards, and has
been registered with the Australian Communications and
Media Authority (ACMA) for placement on the Australian
market.

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Labels and Symbols 3
The KCC marking is a declaration that this product conforms
to all the applicable standards of South Korea. Contact your
Olympus representative for more information. The MSIP
code for the BTX III is the following: R-R-OYN-BTX III.
The China RoHS mark indicates the product’s Environment-
Friendly Use Period (EFUP). The EFUP is defined as the
number of years for which listed controlled substances will
not leak or chemically deteriorate while in the product. The
EFUP for the BTX III has been determined to be 15 years.
Note: The Environment-Friendly Use Period (EFUP) is not
meant to be interpreted as the period assuring functionality
and product performance.
The direct current symbol.
SERIAL NUMBER The serial number is in the following format: BTX-XXX
where: XXX represents a three-digit number
Table 1 Content of the rating label (continued)

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Labels and Symbols4

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Important Information — Please Read Before Use 5
Important Information — Please Read Before Use
Intended Use
The BTX III X-ray diffraction analyzer is designed primarily for analyzing a variety of
powder sample types.
Do not use the BTX III analyzer for any purpose other than its intended use. It must
never be used to inspect or examine human or animal body parts.
Instruction Manual
This instruction manual contains essential information on how to use this Olympus
product safely and effectively. Before using this product, thoroughly review this
instruction manual. Use the product as instructed.
Keep this instruction manual in a safe, accessible location.
WARNING

10-015490-01EN, Rev. 2, June 2020
Important Information — Please Read Before Use6
Some of the details of components and/or software images in this manual may differ
from your instrument’s components or software display. However, the principles
remain the same.
Instrument Compatibility
The BTX III XRD analyzer is primarily a self-contained unit. However, it does have a
series of I/O ports that can be used to connect compatible peripherals and connect it to
a PC. The unit derives its required DC input power from the BTX III analyzer’s AC
adaptor.
Always use equipment and accessories that meet Olympus specifications. Using
incompatible equipment could cause equipment malfunction and/or damage, or
human injury.
Repair and Modification
The BTX III XRD analyzer does not contain any user-serviceable parts, apart from one
exception: the measurement window. If the measurement window is damaged, the
window assembly should be replaced as soon as possible. This User’s Manual
contains more details on this procedure.
In order to prevent human injury and/or equipment damage, do not disassemble,
modify, or attempt to repair the instrument.
IMPORTANT
CAUTION
CAUTION

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Important Information — Please Read Before Use 7
Safety Symbols
The following safety symbols might appear on the instrument and in the instruction
manual:
General warning symbol
This symbol is used to alert the user to potential hazards. All safety messages that
follow this symbol shall be obeyed to avoid possible harm or material damage.
Radiation warning symbol
This symbol is used to alert the user to the presence of potentially harmful
ionizing radiation generated within the XRD analyzer. All safety messages that
follow this symbol shall be obeyed to avoid possible harm.
Shock hazard caution symbol
This symbol is used to alert the user to potential electric shock hazards. All safety
messages that follow this symbol shall be obeyed to avoid possible harm.
Safety Signal Words
The following safety signal words might appear in the documentation of the
instrument:
The DANGER signal word indicates an imminently hazardous situation. It calls
attention to a procedure, practice, or the like that if not correctly performed or
adhered to will result in death or serious personal injury. Do not proceed beyond a
DANGER signal word until the indicated conditions are fully understood and met.
DANGER

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Important Information — Please Read Before Use8
The WARNING signal word indicates a potentially hazardous situation. It calls
attention to a procedure, practice, or the like that if not correctly performed or
adhered to could result in death or serious personal injury. Do not proceed beyond a
WARNING signal word until the indicated conditions are fully understood and met.
The CAUTION signal word indicates a potentially hazardous situation. It calls
attention to a procedure, practice, or the like that if not correctly performed or
adhered to may result in minor or moderate personal injury, material damage,
particularly to the product, destruction of part or all of the product, or loss of data. Do
not proceed beyond a CAUTION signal word until the indicated conditions are fully
understood and met.
Note Signal Words
The following note signal words could appear in the documentation of the
instrument:
The IMPORTANT signal word calls attention to a note that provides information that
is important or essential to the completion of a task.
The NOTE signal word calls attention to an operating procedure, practice, or the like,
that requires special attention. A note also denotes related parenthetical information
that is useful, but not imperative.
The TIP signal word calls attention to a type of note that helps you apply the
techniques and procedures described in the manual to your specific needs, or that
provides hints on how to effectively use the capabilities of the product.
WARNING
CAUTION
IMPORTANT
NOTE
TIP

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Important Information — Please Read Before Use 9
Safety
Before turning on the instrument, verify that the correct safety precautions have been
taken (see the following warnings). In addition, note the external markings on the
instrument, which are described under “Safety Symbols.”
Warnings
General Warnings
• Carefully read the instructions contained in this instruction manual prior to
turning on the instrument.
• Keep this instruction manual in a safe place for further reference.
• Follow the installation and operation procedures.
• It is imperative to respect the safety warnings on the instrument and in this
instruction manual.
• If the equipment is used in a manner not specified by the manufacturer, the
protection provided by the equipment could be impaired.
• Do not install substitute parts or perform any unauthorized modification to the
instrument.
• Service instructions, when applicable, are for trained service personnel. To avoid
the risk of electric shock, do not perform any work on the instrument unless
qualified to do so. For any problem or question regarding this instrument, contact
Olympus or an authorized Olympus representative.
Radiation Safety Warning
Do not open the system, disassemble, or modify any internal components. These
actions could result in serious damage to the system and a health hazard to the
operator.
WARNING
WARNING

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Important Information — Please Read Before Use10
Electrical Warnings
• Before operating this instrument using mains electricity, you must connect the
protective earth terminal of the instrument to the protective conductor (mains) of
the power cord. The mains plug shall only be inserted into a socket outlet
provided with a protective earth contact. Never negate the protective action by
using an extension cord (power cable) without a protective conductor
(grounding).
• If there is any possibility that the ground protection could be impaired, you must
make the instrument inoperative and secure it against any unintended operation.
• The instrument must only be connected to a power source corresponding to the
type indicated on the rating label.
If an unauthorized power supply cord is used to power the instrument, Olympus
cannot guarantee the electrical safety of the equipment.
High Voltage
The BTX III XRD analyzer uses a 30 kV high-voltage power supply (HVPS) for X-ray
generation. The permanent connection between the HVPS and the X-ray tube is sealed
and shielded in such a way that no high voltage connector could accidentally get loose
or disconnected inside the system. There is no high voltage risk to the user when
using the BTX III analyzer under normal conditions. Should you notice substantial
damage to the outside of the system, or suspect any internal damage after excessive
shock, DO NOT turn on the system, return it to the factory for full inspection and
potential repairs.
• X-ray tubes and detectors in this instrument contain beryllium metal in the form
of coated foil. In its as-supplied state, the beryllium poses no harm to the user.
WARNING
CAUTION
WARNING
CAUTION

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Important Information — Please Read Before Use 11
However, if a detector or tube is damaged, contact with small particles is possible
if the instrument is breached (for example, a window is broken or during window
replacement). Intact skin is sufficient protection against this situation and
washing with soap and water will effectively remove any beryllium
contamination. If granulated beryllium embeds in an open wound, seek medical
attention.
• Instruments with a damaged detector or tube must be returned to your local
distributor or the manufacturer. Care should be taken to limit the release of
beryllium from the instrument.
Richtlinien für den Strahlenschutz im deutschsprachigen Raum
Deutschland
Der Betrieb eines tragbaren Röntgenfluoreszenzanalysators ist in jedem Fall genehmi-
gungspflichtig (§ 3 RöV).
Sorgen Sie dafür, dass in Ihrem Betrieb mindestens ein Strahlenschutzbeauftragter
mit Fachkunde R2 nach der deutschen Röntgenverordnung verfügbar ist. Darüber hi-
naus sollten Sie die Bediener regelmäßig schulen lassen. Eine jährliche Unterweisung
der Bediener ist vom Strahlenschutzbeauftragten durchzuführen.
Es ist i. d. R. ein Betriebsbuch (Nachweis der Betriebszeiten, Wartungsarbeiten und
Störfälle) zu führen. Eine betriebliche Strahlenschutzanweisung ist zu erstellen und
mit der deutschsprachigen Bedienungsanleitung den Gerätebedienern jederzeit zu-
gänglich zu machen.
Das Strahlenschutztechnische Gutachten für das jeweilige Instrument wird bei Aus-
lieferung des Gerätes von einem behördlich zugelassenen Sachverständigen erstellt
und sollte jederzeit einsehbar sein. Spätestens nach 5 Jahren muss dieses Gutachten
erneuert werden.
Die Genehmigungsbehörde kann weitere Maßnahmen zur Arbeitssicherheit festle-
gen.
Österreich
Der Betrieb eines tragbaren Röntgenfluoreszenzanalysators ist genehmigungspflich-
tig.

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Important Information — Please Read Before Use12
Es ist ein Strahlenschutzbeauftragter und die entsprechende Anzahl von weiteren,
mit der Wahrnehmung des Strahlenschutzes betrauten Personen, zu nominieren. Der
Strahlenschutzbeauftragte ist der Behörde bekannt zu geben. Der Strahlenschutzbe-
auftragte und die weiteren Personen haben eine entsprechende Ausbildung gemäß
der allgemeinen österreichischen Strahlenschutzverordnung nachzuweisen.
Das Bedienpersonal (sofern nicht selber strahlenschutzbeauftragt) ist gemäß § 16 All-
gemeine Strahlenschutzverordnung mindestens einmal jährlich vom Strahlenschutz-
beauftragten gemäß § 29 StrSchG zu unterweisen. Dies muss dokumentiert werden.
Eine deutschsprachige Bedienungsanleitung sowie Handlungs- und Arbeitsanwei-
sungen sind dem Bedienpersonal jederzeit zur Verfügung zu stellen.
Es wird empfohlen jeden Bediener mit einem amtlichen Dosimeter auszurüsten.
Schweiz
Der Betrieb von Röntgenfluoreszenzanalysatoren ist der BAG anzuzeigen (Bewilli-
gungsverfahren).
Für den Einsatz von tragbaren Röntgengeräten ist für jeden Betrieb ein für den Strah-
lenschutz verantwortlicher Mitarbeiter zu benennen, der eine dem Schweizer Strah-
lenschutzgesetz genügende Ausbildung bei der SUVA (eintägiger Kursus) erfolgreich
absolviert hat.
Die Bedienungsanleitung sowie weitere eventuell von den Behörden geforderte Un-
terlagen wie Arbeitsanweisungen und Anweisung im Falle von Störungen müssen
den Bedienern zugänglich gemacht werden.
Tragbare RFA-Geräte mit offenem Strahlengang müssen im Zwei-Hand-Modus be-
dient werden.
Equipment Disposal
Before disposing of the BTX III, check your local laws, rules, and regulations, and
follow them accordingly.