Radleys Reactor-Ready Pilot User manual

Instructions
Reactor-Ready Pilot™
Lab Reactor
Patent Pending
Your Local istributor
Radleys, Shire Hill, Saffron Walden, Essex, CB11 3AZ. United Kingdom.
Tel: [phone] Fax: [phone]
Email: [e-mail] Web: www.radleys.com
July 2018 Issue 6

Page 1
Reactor-Ready Pilot - Lab Reactor
ndex
Page 1 ndex
Page 2 1. ntroduction
2. Warranty
Page 3 3. Safety nformation
4. mportant WARN NGS
Page 4 5. Reactor-Ready Pilot and Accessories
Page 5 5. Reactor-Ready Pilot and Accessories - Continued
Page 6 5. Reactor-Ready Pilot and Accessories - Continued
Page 7 6. Component and Vessel Guide
Page 8 6. Component and Vessel Guide - Continued
Page 9 6. Component and Vessel Guide - Continued
Page 10 7. Quick Start Guide
Page 11 7. Quick Start Guide - Continued
Page 12 7. Quick Start Guide - Continued
Page 13 8. Set-Up and Operation
8.1 Optimising thermal performance
8.2 Operating temperature range
Page 14 8. Set-Up and Operation - Continued
8.3 Setting up the base
Page 15 8. Set-Up and Operation - Continued
8.3 Setting up the base
8.4 Assembling the Manifolds
Page 16 8. Set-Up and Operation - Continued
8.5 Assembling the Manifolds on the right hand rod
Page 17 8. Set-Up and Operation - Continued
8.6 Locating the support platform
8.7 Assembling the brace rods
& Leveling the Framework
Page 18 8. Set-Up and Operation - Continued
8.8 Assembling the stirrer support
8.9 Preparing the reaction vessel
Page 19 8. Set-Up and Operation - Continued
8.9 Preparing the reaction vessel
8.10 Assembling the vessel lid, stirrer guide and probe
Page 20 8. Set-Up and Operation - Continued
8.10 Assembling the vessel lid, stirrer guide and probe
8.11 Attaching the thermofluid hoses
Page 21 8. Set-Up and Operation - Continued
8.12 Attaching the overhead stirrer
Page 22 8. Set-Up and Operation - Continued
8.13 Choosing your thermoregulator (circulator)
8.14 Choosing your thermofluid
8.15 Connecting the thermoregulator
Page 23 8. Set-Up and Operation - Continued
8.14 Connecting the thermoregulator - Continued
8.15 If adapters and isolating valves are not to be used
8.16 If adapters and isolating valves are to be used
8.17 Charging Reactor-Ready with thermofluid
Page 24 8. Set-Up and Operation - Continued
8.18 Static
Page 25 8. Set-Up and Operation - Continued
8.19 raining thermofluid from Reactor-Ready Pilot
8.20 isconnecting the thermoregulator
Page 26 8. Set-Up and Operation - Continued
8.21 Hose Tidies
9. Accessories
9.1 Universal Boss
9.2 Rod Extender
9.3 rip Trays
Page 27 9.4 Reflux ividers
9.5 Accessory Glassware
Page 28 10. Jacketed Glass Reaction Vessels
10.1 Materials of Construction
10.2 Vacuum & Pressure
10.3 Safe elta T (ΔT)
10.4 Temperature Range
10.5 The use of self-sealing couplings - not recommended
10.6 Vessel Sidearms
Page 29 10. Jacketed Glass Reaction Vessels - Continued
10.7 Vacuum Jacketed Vessels
10.8 V4 Zero ead Space Stopcock (V4 Z S)
Page 30 10. Jacketed Glass Reaction Vessels - Continued
10.9 Minimising weeping at low or high temperatures
10.10 Replacement Pistons & O-Rings
Page 31 11. General Specifications
Page 32 11. General Specifications - Continued
12. Routine Maintenance
Page 33 Huber Thermoregulator Performance
Page 34
WARRANTY - EMAIL BACK

Reactor-Ready Pilot - Lab Reactor
Thank you for purchasing Reactor-Ready Pilot.
Please read this nstruction Manual thoroughly before operating the unit.
1. ntroduction
Reactor-Ready Pilot is designed as a universal reactor work station that can be used for different vessel sizes and different projects.
Reactor-Ready Pilot is ideal for process development, scale-up, pilot and kilo labs. The beauty of Reactor-Ready Pilot is that one reactor
work station can replace many, saving you money and fumehood space.
Features include
• Rapid vessel exchange with quick-release vessel clamp and wide bore hose couplings.
• Range of single and vacuum jacketed vessels from 5 litres to 20 litres.
• Vessels manufactured at 1.25 to 1 ratio (internal height to diameter) to mimic plant scale reactors.
• N200 vessel flange.
• Accepts all leading brands of overhead stirrer and allows easy, tool-free adjustment.
• Compact stainless steel framework accepts all vessel sizes.
• Self-aligning stirrer coupling engages without the need for tools.
• Temperature range: -70ºC to +230ºC. (Chemraz O-Rings are recommended for use above +150˚C)
• Innovative hose manifolds allow easy thermofluid drain down.
• Wide range of accessory glassware including condensers, dropping funnels etc.
• Optional software allows you to log & control 3rd party devices.
• Operating Pressure Range 10mbar to 1.5 bar (absolute).
2. Warranty
Reactor-Ready Pilot includes one year full parts and labour warranty from date of original purchase.
Warranty will only be valid if a completed Warranty Email Back is returned within 1 month of date of purchase (see last
page). In the event of product failure please contact your local distributor.
Please do not return any goods without prior agreement.
Page 2

3. Safety nformation
The following symbols are intended to assist the user in the safe and efficient operation of Reactor-Ready Pilot.
4. mportant WARN NGS
Please read these instructions completely before using the Reactor-Ready Pilot system.
• Always read the instructions of any third party equipment, such as overhead stirrers and thermoregulators thoroughly to ensure you are not
contravening any safety recommendations or manufacturers warranty when used in conjunction with Reactor-Ready Pilot.
• Always ensure that the Reactor-Ready Pilot vessel is clamped and supported correctly, using the purpose built framework and clamp. Under
no circumstances should the system be operated without this framework.
• The maximum operating stirring speed for PTFE stirrer guides in general is 500rpm for continuous operation and 800rpm for short periods,
but for the large vessel volumes in Reactor-Ready Pilot, slower speeds should be used.
• It is the responsibility of the user to ensure correct set up and continued maintenance of the stand, clamps and framework.
• Always ensure that Reactor-Ready Pilot is located on a level surface.
• Operate only in a fumehood with protective safety sash.
• Risk of burns from hot or extreme cold surfaces during and after heating/cooling, therefore take care not to touch the Reactor-Ready Pilot
unit, or any of the auxiliary modules.
• Reactor-Ready Pilot unit will remain hot for some considerable time after the heating source has been switched off. A temperature probe or
temperature sensitive label can be used to indicate when components are too hot to touch.
• Before starting your reaction, ensure that all fittings to the thermoregulator are fully tightened, not leaking and that the manifold drain and
vent valves are closed.
• Reactor-Ready Pilot metal components are resistant to the majority of solvents and splash-resistant to dilute acids and alkalis at room
temperature.
• Always wipe away any chemical spills immediately and avoid exposure to strong vapours such as HCl etc, as continued exposure to
chemical vapours or liquids will cause corrosion to metal and/or plastic components.
• Reactor-Ready Pilot can be used with a recirculating fluid at a temperature of up to 230˚C, or down to -70°C without damage to the unit.
Careful inspection of all fluid connections to Reactor-Ready Pilot should be regularly performed when operating at these temperatures.
• Ensure all wires and cables connecting auxiliary equipment are secured such that they cannot come into contact with Reactor-Ready Pilot
surfaces, or moving parts.
• Flowing liquids can create a build up of static, leading to risk of sparks and explosion. Care must be taken to properly bond and ground
components of Reactor-Ready Pilot to meet local safety requirements.
• Reactor-Ready Pilot should only be operated by trained and competent personnel. As with all chemistries, a full risk assessment should be
performed prior to starting and care should be taken to monitor reactions at all stages. uring operation Reactor-Ready Pilot should not be
left unattended unless in a supervised area.
Page 3
Warning
Applies when there is a possibility
of personal injury.
mportant Note
Alerts the user to important facts.
!
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Reactor-Ready Pilot - Lab Reactor

Page 4
Reactor-Ready Pilot - Lab Reactor
5. Reactor-Ready Pilot and Accessories
How to order Reactor-Ready Pilot
1. Select the Reactor-Ready Pilot Core: RR210000.
2. Choose the lid you require.
3. Choose the Vessel Kit or Kits required by selecting the vessel volume & style.
4. Select the overhead stirrer required.
5. If thermoregulator, hoses, hose adapters, thermofluid and accessory glassware are
needed, select from the accessory list opposite.
6. If automation is required, add the Control Software and ata Hub.
Reactor-Ready Pilot Core System
RR210000 Reactor-Ready Pilot Core System includes:
• Base frame, support rods, vessel clamp, I-beam
& stirrer support bosses.
• Vessel to manifold insulated hoses with quick-release
connections.
• Lower inlet manifold with drain.
• Upper outlet manifold with vent.
• PTFE Stirrer guide & Stainless steel stirrer drive coupling.
• One aluminium vessel support collar.
• FEP flange O-Ring and PTFE centering collar.
Important: Hoses to connect the Reactor-Ready ilot framework to your thermoregu-
lator are NOT included. You will require hoses with an M30x1.5 female connection or
appropriate adapters. See below for hoses, adapters and suitable thermoregulators.
Glass Lids
• N200 Glass Lids fit all Vessel sizes...
• Choice of 6 or 7 Rodaviss glass joints.
• Custom lid designs are available on request.
• See page 8 for full lid specifications.
RR236000 6 Neck Lid N200 - 1xB19, 1xB24, 1xB29, 2xB34, 1xB45
RR236002 7 Neck Lid N200 - 1xB19, 1xB24, 1xB29, 3xB34, 1xB45
RR236000/US 6 Neck Lid N200 - 1xA19, 1xA24, 1xA29, 1xB34, 1xA34,
1xA45
RR236002/US 7 Neck Lid N200 - 1xA19, 1xA24, 1xA29, 1xB34, 2xA34,
1xA45
Reaction Vessel Kits
• Kits include; process vessel, turbine stirrer paddle, PTFE Pt100
temp. probe with Lemo plug and PTFE temperature probe adapter.
• Choice of single or vacuum jacketed vessels.
• Custom vessel designs are available on request.
RR220005 5L Single Jacketed Pilot Process Vessel Kit
RR220015 10L Single Jacketed Pilot Process Vessel Kit
RR220025 15L Single Jacketed Pilot Process Vessel Kit
RR220035 20L Single Jacketed Pilot Process Vessel Kit
RR220010 5L Vacuum Jacketed Pilot Process Vessel Kit
RR220020 10L Vacuum Jacketed Pilot Process Vessel Kit
RR220030 15L Vacuum Jacketed Pilot Process Vessel Kit
RR220040 20L Vacuum Jacketed Pilot Process Vessel Kit
RS Overhead Stirrers
Please note that other overhead stirrer options are available on request,
please contact Radleys for further information.
RR91302 RS27 Standard Overhead Stirrer 230v UK Plug
RR91302/EURO RS27 Standard Overhead Stirrer 230v Euro Plug
RR91306 RS37 igital Plus Overhead Stirrer 230v UK Plug
RR91306/EURO RS37 igital Plus Overhead Stirrer 230v Euro Plug
RR91308 RS50 Control Overhead Stirrer 230v UK Plug
RR91308/EURO RS50 Control Overhead Stirrer 230v Euro Plug
RR91312 RS100 Control Plus Overhead Stirrer with 230v UK Plug
RR91312/EURO RS100 Control Plus Overhead Stirrer with 230v Euro Plug
Huber Thermoregulators (others available)
HB1000.0001.05 Unistat Tango Nuevo
HB1002.0003.05 Unistat 405
HB1005.0002.05 Unistat 425
HB1005.0001.05 Unistat 510w
HB1007.0001.05 Unistat 610w
HB1014.0001.05 Unistat 825
HB1014.0002.05 Unistat 825w
Important: For technical advice on selecting the thermoregulator, thermofluid or hoses
for your application please contact our technical sales team on Tel: [phone]
or e-mail: [e-mail]
Thermoregulator Hoses, Adapters & Thermofluid
M24 Insulated Hose with TFE Inner (12mm ID x 37mm OD)
HB9325 M24x1.5 x 1m Insulated PTFE Hose -60°C to +260°C
HB9326 M24x1.5 x 1.5m Insulated PTFE Hose -60°C to +260°C
HB9327 M24x1.5 x 2m Insulated PTFE Hose -60°C to +260°C
HB9328 M24x1.5 x 3m Insulated PTFE Hose -60°C to +260°C
M30 Insulated Hose with TFE Inner (20mm ID x 44mm OD)
HB9612 M30x1.5 x 1m Insulated PTFE Hose -60°C to +260°C
HB9613 M30x1.5 x 1.5m Insulated PTFE Hose -60°C to +260°C
HB9614 M30x1.5 x 2m Insulated PTFE Hose -60°C to +260°C
HB9615 M30x1.5 x 3m Insulated PTFE Hose -60°C to +260°C
M24 Insulated Hose with Metal Inner (12mm ID x 44mm OD)
HB9274 M24x1.5 x 1m Insulated Metal Hose -100°C to +350°C
HB9275 M24x1.5 x 1.5m Insulated Metal Hose -100°C to +350°C
HB9276 M24x1.5 x 2m Insulated Metal Hose -100°C to +350°C
HB9277 M24x1.5 x 3m Insulated Metal Hose -100°C to +350°C
M30 Insulated Hose with Metal Inner (20mm ID x 56mm OD)
HB6426 M30x1.5 x 1m Insulated Metal Hose -100°C to +350°C
HB6386 M30x1.5 x 1.5m Insulated Metal Hose -100°C to +350°C
HB6427 M30x1.5 x 2m Insulated Metal Hose -100°C to +350°C
HB6428 M30x1.5 x 3m Insulated Metal Hose -100°C to +350°C
Thermoregulator Adapters & Thermofluid
M24 Adapters
HB9268 M24x1.5 Male to M30x1.5 Female Adapter
HB6723 M24x1.5 Female to M30x1.5 Male Adapter
HB9256 M24x1.5 90 degree Adapter
HB12634 M24x1.5 Nut
HB9471 M24x1.5 Hose Connector NW12
HB9236 M24x1.5 Isolating Ball Valve
M30 Adapters
HB6612 M30x1.5 Male to M38x1.5 Female Adapter
HB6984 M30x1.5 Female to M38x1.5 Male Adapter
HB6461 M30x1.5 90 degree Adapter
HB5992 M30x1.5 Nut
HB6451 M30x1.5 Isolating Ball Valve
Thermofluid
HB6161 SilOil M20.235.20, 5 Litre -20°C to +235°C
HB6162 SilOil M20.235.20, 10 Litre -20°C to +235°C
HB6163 SilOil M40.165.10, 5 Litre -40°C to +165°C
HB6164 SilOil M40.165.10, 10 Litre -40°C to +165°C
HB6165 SilOil M60.115.05, 5 Litre -60°C to +115°C
HB6166 SilOil M60.115.05, 10 Litre -60°C to +115°C
HB6479 W-Therm M90.200.02, 10 Litre -90°C to +200°C

Page 5
Reactor-Ready Pilot - Lab Reactor
5. Reactor-Ready Pilot and Accessories - Continued
Glassware Accessories
RR139005 Condenser Liebig 250mm B29 + GL14 + fittings
RR139007 Condenser ouble Surface 200mm B29 + GL14 + fittings
RR139009 Condenser Jacket Coil Rodaviss B29 + GL14 + fittings
RR139300 Large ouble Coil Rodaviss Condenser 60mm B34 + GL18 + fittings
RR139302 Large ouble Coil Rodaviss Condenser 85mm B34 + GL18 + fittings
RR139011 Right Angle Adapter B29 + GL14 + PTFE fittings
RR139012 Right Angle Adapter B34 + GL14 + PTFE fittings
RR139017 250ml Graduated ropping Funnel Equalising Arm B24
RR139019 500ml Graduated ropping Funnel Equalising Arm B24
RR139021 1000ml Graduated ropping Funnel Equalising Arm B24
RR139304 2000ml Graduated ropping Funnel Equalising Arm B29 6mm Bore
RR139308 Swan Neck Adapter Vertical B24 to Vertical B24
RR139310 Swan Neck Adapter Vertical B29 to Vertical B29
RR139312 Swan Neck Adapter Vertical B34 to Vertical B34
RR139079 PTFE Flexible Bellows B24
RR139081 PTFE Flexible Bellows B29
RR139083 PTFE Flexible Bellows B34
RR139025 Gas Purge Adapter B24 + GL14 + fittings
RR139027 Glass Cone Stopper B19
RR139029 Glass Cone Stopper B24
RR139031 Glass Cone Stopper B29
RR139033 Glass Cone Stopper B34
RR139378 Glass Cone Stopper B45
RR139034 Enlarging Adapter B19 to B24
RR139035 Enlarging Adapter B24 to B29
RR139036 Enlarging Adapter B19 to B29
RR139037 Enlarging Adapter B29 to B34
RR139038 Enlarging Adapter B19 to B34
RR139039 Reducing Adapter B24 to B19
RR139041 Reducing Adapter B29 to B19
RR139043 Reducing Adapter B29 to B24
RR139045 Reducing Adapter B34 to B19
RR139047 Reducing Adapter B34 to B24
RR139049 Reducing Adapter B34 to B29
RR139051 Oil Bubbler Type 1 B24 + GL14 + fittings
RR139314 Oil Bubbler Type 1 B29 + GL14 + fittings
RR139053 Solid Additions Funnel B34 (with extended tube)
RR139316 Solid Additions Funnel B45 (with extended tube)
RR139057 Valved Right Angled Liquid Inlet Adapter B24 to GL14
RR139318 Valved Right Angled Liquid Inlet Adapter B29 to GL14
RR139320 Reflux ivider Head B34 + GL18 + fitting
RR139322 Reflux ivider Head B34 + GL18 + fitting + B14 temp probe port
RR139133 Pt100 PTFE Temp. Probe (Reflux ivider Head) + 2m Cable + Lemo
RR139135 PTFE Temperature Probe Adapter (B14 for Reflux ivider Head)
RR139063 PTFE Hose Adapter B19 to 12mm I (NW12)
RR139065 PTFE Hose Adapter B24 to 15mm I
RR139324 500ml Receiver Flask 3 x B24 Socket, + B24 Cone & Tap
RR139326 1000ml Receiver Flask 3 x B24 Socket, + B24 Cone & Tap
RR139328 2000ml Receiver Flask 3 x B24 Socket, + B24 Cone & Tap
RR139330 5000ml Receiver Flask 3 x B24 Socket, + B24 Cone & Tap
RR139085 Adapter Rodaviss B19 to GL25
RR139332 Adapter Rodaviss B24 to GL25
RR139334 Adapter Rodaviss B29 to GL25
RR139087 Adapter Rodaviss B34 to GL25
RR139089 Adapter Rodaviss B19 to GL14
RR139091 Adapter Rodaviss B24 to GL14
RR139336 Adapter Rodaviss B29 to GL14
RR139093 Adapter Rodaviss B19 to 2 x GL14
RR139095 Adapter Rodaviss B24 to 2 x GL14
RR139338 Adapter Rodaviss B29 to 2 x GL14
RR139340 Vertical Run-Off Adapter B24 to Plain Stem
RR139137 Run-Off Secondary Valve, B24 to Stopcock
RR139111 Screw Cap with Aperture GL14, pk 10
RR139113 Silicone Seal with PTFE Washer GL14, 6mm, pk 10
RR139115 Screw Cap GL14, with PTFE seal, pk 10
RR139119 Screw Cap with Aperture GL25, pk 10
RR139121 Silicone Seal with PTFE Washer GL25, 12mm, pk 10
RR139117 Screw Cap GL25, with PTFE seal, pk 10
RR139342 GL14 HT Compression Fitting for 4mm O Tubing
RR139344 GL14 HT Compression Fitting for 6mm O Tubing
RR139346 GL25 HT Compression Fitting for 8mm O Tubing
RR139348 GL25 HT Compression Fitting for 10mm O Tubing
RR139350 GL25 HT Compression Fitting for 12mm O Tubing
RR139352 GL18 PTFE Hose Connector for 10mm I Tubing
RR139354 PTFE Tubing 10mm I x 12mm O - 1m length
Important: For assistance in identifying the accessories you require or a custom glass-
ware quote please contact your local Radleys distributor or call Tel: [phone].
US ‘A Length Joints’. For US ‘A Length’ glass cones and sockets please add a suffix
/US to the catalogue number when placing your glassware order.
Reflux Divider Kits...
RR239200 Pilot Reflux ivider Kit
RR139320 - Reflux ivider Head, B34 + GL18 fittings
RR139300 - Large ouble Coil Rodaviss Condenser 60mm
B34 + GL18 + fittings
RR139012 - Right Angle Adapter B34 + GL14 + PTFE fittings
RR139332 - Adapter Rodaviss B24 to GL25
RR139350 - GL25 HT Compression Fitting for 12mm O Tubing
RR139354 - PTFE Tubing 10mm I x 12mm O - 1m length
RR139360 - 3 x Pilot Boss Head - 22-35mm, 8-12mm
RR139372 - 4-Prong Large Clamp - 10mm rod, 30-80mm
RR139376 - Lower Support Ring - 10m rod, 76mm I
RR139374 - Universal Clamp Cork Jaws - 10mm rod, 0-80mm
Note: A suitable receiver flask/s RR13924/6/8/30 is required to complete this kit.
RR239202 Pilot Reflux ivider Kit with Vapour Temperature Probe
RR139322 - Reflux ivider Head, B34 + GL18 fittings
+B14 temp port
RR139300 - Large ouble Coil Rodaviss Condenser 60mm
B34 + GL18 + fittings
RR139012 - Right Angle Adapter B34 + GL14 + PTFE fittings
RR139332 - Adapter Rodaviss B24 to GL25
RR139350 - GL25 HT Compression Fitting for 12mm O Tubing
RR139354 - PTFE Tubing 10mm I x 12mm O - 1m length
RR139133 - Pt100 PTFE Temp. Probe (Reflux ivider Head)
+ 2m Cable
RR139135 - PTFE Temperature Probe Adapter
(B14 for Reflux ivider Head)
RR139360 - 3 x Pilot Boss Head - 22-35mm, 8-12mm
RR139372 - 4-Prong Large Clamp - 10mm rod, 30-80mm
RR139374 - Universal Clamp Cork Jaws - 10mm rod, 0-80mm
RR139376 - Lower Support Ring - 10m rod, 76mm I
Note: A suitable receiver flask/s RR13924/6/8/30 is required to complete this kit.

Reactor-Ready Pilot - Lab Reactor
5. Reactor-Ready Pilot and Accessories - Continued
Reaction Vessel Support Collar
RR210018 Pilot Vessel Support Collar
Important: Support collar is required to support vessels within the quick-release
clamp. One support collar is supplied with each Reactor-Ready ilot Core.
We recommend one support collar per vessel.
Jacketed Reaction Vessels
RR235050 5L Single Jacketed Pilot Vessel
RR235100 10L Single Jacketed Pilot Vessel
RR235150 15L Single Jacketed Pilot Vessel
RR235200 20L Single Jacketed Pilot Vessel
Vacuum Jacketed Reaction Vessels
RR235052 5L Vacuum Jacketed Pilot Vessel
RR235102 10L Vacuum Jacketed Pilot Vessel
RR235152 15L Vacuum Jacketed Pilot Vessel
RR235202 20L Vacuum Jacketed Pilot Vessel
PTFE Stirrer Shafts
RR258051 Anchor PTFE Stirrer Shaft - 5L Pilot Vessels
RR258052 Retreat Curve PTFE Stirrer Shaft - 5L Pilot Vessels
RR258053 Turbine PTFE Stirrer Shaft - 5L Pilot Vessels
RR258101 Anchor PTFE Stirrer Shaft - 10L Pilot Vessels
RR258102 Retreat Curve PTFE Stirrer Shaft - 10L Pilot Vessels
RR258103 Turbine PTFE Stirrer Shaft - 10L Pilot Vessels
RR258151 Anchor PTFE Stirrer Shaft - 15L Pilot Vessels
RR258152 Retreat Curve PTFE Stirrer Shaft - 15L Pilot Vessels
RR258153 Turbine PTFE Stirrer Shaft - 15L Pilot Vessels
RR258201 Anchor PTFE Stirrer Shaft - 20L Pilot Vessels
RR258202 Retreat Curve PTFE Stirrer Shaft - 20L Pilot Vessels
RR258203 Turbine PTFE Stirrer Shaft - 20L Pilot Vessels
RR258300 Adjustable PTFE 4 Blade 45˚ Rotor 16mm O 100mm Rotor
RR258302 Adjustable PTFE 2 Blade Vertical Rotor 16mm O 100mm Rotor
PTFE Pt100 Temperature Probes & Adapters
RR145000 Pt100 PTFE Temp. Probe 9mm + Lemo Plug - 5L to 10L Vessels
RR146000 Pt100 PTFE Temp. Probe 9mm + Lemo Plug - 15L to 20L Vessels
RR140015 PTFE Temperature Probe Adapter - 9mm
PTFE Baffles + PTFE Probe Baffles
RR257000 PTFE Baffle, 16mm O Shaft, 35mm x 600mm long
RR257002 PTFE Baffle, 16mm O Shaft, 35mm x 700mm long
RR257004 Pt100 PTFE Baffle Probe + Lemo, 16mm O Shaft,
35mm x 600mm long
RR257006 Pt100 PTFE Baffle Probe + Lemo, 16mm O Shaft,
35mm x 700mm long
RR257008 B24 to 16mm PTFE Compression Fitting
RR257010 B29 to 16mm PTFE Compression Fitting
RR257012 B34 to 16mm PTFE Compression Fitting
Polypropylene Drip Trays
RR210062 rip Tray Polypropylene 7L Capacity
RR210064 rip Tray Polypropylene 22L Capacity
RR210066 rip Tray Polypropylene 45L Capacity
Clamps + Bosses
RR139360 Pilot Boss Head - 22-35mm, 8-12mm
RR139362 Rod Extender - 10mm, 100mm long, for 10mm rods
RR139364 Rubber Belt Clamp - 10mm rod, 60-170mm
RR139366 Chain Clamp - 10mm rod, 40-120mm
RR139368 Chain Clamp - 10mm rod, 80-150mm
RR139370 Chain Clamp - 10mm rod, 100-170mm
RR139372 4-Prong Large Clamp - 10mm rod, 30-80mm
RR139374 Universal Clamp Cork Jaws - 10mm rod, 0-80mm
RR139376 Lower Support Ring - 10m rod, 76mm I
Pilot Core Height Reduction Kits
RR210070 Reactor-Ready Pilot Core - 200mm Height Reduction Kit
RR210072 Reactor-Ready Pilot Core - 300mm Height Reduction Kit
mportant: Designed to reduce the overall height of the ilot Core by 200 or 300mm.
General Maintenance Accessories
RR210100 Reactor-Ready Pilot Maintenance Kit (includes all items listed below)
Does not include Chemraz O-Rings or 25mm iston.
RR121027 Oil Wipe for Support Rods, pk 10
RR121136 Stirrer Guide Bearing Seal B34, 16mm
RR121138 Stirrer Guide Ferrule & Shaft Seal B34, 16mm
RR121071 23mm Viton O-Rings for Quick Release Hose Coupling, pk 2
RR210050 34mm Viton O-Rings for Quick Release Hose Coupling - NW20, pk 2
RR210022 FEP Encapsulated Silicone Vessel O-Ring - 200mm
RR166104 Replacement 25mm Piston Top O-Ring FEP, pk 2
RR166106 Replacement 25mm Piston Middle O-Ring FEP
Important: For temperatures above 150˚C we recommend the use of high perfor-
mance Chemraz piston O-Rings to prevent possible weeping. Chemraz O-Rings are
suitable for temperatures from 0˚C to +230˚C and should not be used below 0˚C.
RR210074 Replacement 25mm Piston Top O-Ring Chemraz (0˚C to 230˚C), pk 2
RR166070 Piston 25mm for Single & Vacuum Jacketed Vessels
Spare Parts
RR210010 Base Rigid Foot
RR210012 Base Foot Nut
RR210014 Wheel with Lock
RR121027 Oil Wipe for Support Rods
RR210016 Pilot Stirrer Support I-Beam
RR210018 Pilot Vessel Support Collar
RR121050 Safety Stop Collar
RR121132 Stirrer Guide Assembly B34 16mm
RR210058 Stirrer Guide B34 PTFE Guide & Shaft
RR210060 Stirrer Guide B34 Metal Cap & Pins
RR121140 Stirrer rive rop-in Coupling B34 16mm
RR210020 Pilot Vessel + Lid Clamp
RR210022 FEP Encapsulated Silicone Vessel O-Ring - 200mm
RR210024 PTFE Support Collar for FEP O-Ring - 200mm
RR121136 Stirrer Guide Bearing Seal B34 16mm
RR121138 Stirrer Guide Ferrule & Shaft Seal B34 16mm
RR210030 Upper Return Manifold with Vent Valve - NW20
RR210032 Lower Supply Manifold with rain Valve - NW20
RR210034 Manifold Elbow Adapter 1" Female to M30x1.5 Male
RR210036 Manifold 1" Male to 1" Male Adapter
RR210038 Manifold 1" owty Seal
RR210040 Manifold 1/2" owty Seal
RR210042 Manifold 1/2" Ball Valve
RR210044 Manifold 1/2" Hose Barb Fitting
RR210046 Manifold 1/2" Filter
RR210049 Quick-Release Insulated Hose 80cm HT Vessel-to-Manifold -NW20
RR121071 23mm Viton O-Rings for Quick Release Hose Coupling - NW12 & NW20
RR210050 34mm Viton O-Rings for Quick Release Hose Coupling - NW20
RR210052 Locking Ring for Quick Release Hose Coupling - B34
RR210054 B34 Locking Cap for Quick Release Hose Coupling - B34
RR210056 Allen Key Set - 5mm & 6mm
RR121098 M8 Nylon Knob
RR139098 Secondary valve, B24 stopcock
RR210019 Pilot Collar PTFE Liner Replacement Unit, pk 4
Important: For assistance in identifying the accessories you require or a custom
glassware quote please contact your local Radleys distributor or call
Tel: [phone].
US ‘A Length Joints’. For US ‘A Length’ glass cones and sockets please add a suffix
/US to the catalogue number when placing your glassware order.
Page 6

Page 7
3
8
4
Reactor-Ready Core System
1. Base Frame Assembly
2. Support Rods
3. Vessel Support Platform
4. Vessel Clamp
5. Vessel FEP O-Ring seal and PTFE centering collar
6. N200 Vessel Collar + PTFE Liner
7. Brace Bars
8. Stirrer Support Rods
9. Stirrer Support I-Beam
10. B34 Stirrer Guide
11. Stirrer Coupling
12. Inlet Manifold + rain (Lower Supply Manifold)
13. Outlet Manifold + Vent (Upper Return Manifold)
14. Safety Stop Collars
15. Quick Release Insulated Hoses, 70cm
16. Hose Tidies
17. Adjustable Feet
18. Locking Wheels
2
13
12
1
7
9
14
15 16
18
17
6
5
10
11
Reactor-Ready Pilot - Lab Reactor
6. Component and Vessel Guide

Reactor-Ready Pilot - Lab Reactor
Page 8
Reaction Vessel Kits
A. Reaction Vessel with PTFE Stopcock (1.25 to 1 ratio)
B. PTFE Turbine Stirrer
C. Sidearm Couplings (connecting cap and connecting clip)
. Pt100 PTFE Temperature Probe
E. PTFE Temperature Probe Adapter
A
B
D
E
C
RR236000 - 6 Neck DN200 Lid
• 1 x B34 central vertical - stirrer
• 1 x B19 side vertical - probe
• 1 x B24 side vertical - gas purge
• 1 x B29 side vertical - drop funnel/bubbler/liquid inlet adapter
• 1 x B34 side vertical - condenser & reflux
• 1 x B45 side angled - solid additions
RR236002 - 7 Neck DN200 Lid
• 1 x B34 central vertical - stirrer
• 1 x B19 side vertical - probe
• 1 x B24 side vertical - gas purge
• 1 x B29 side vertical - drop funnel/bubbler/liquid inlet adapter
• 2 x B34 side vertical - condenser & reflux
• 1 x B45 side angled - solid additions
RR239200 - Pilot Reflux Divider Kit
• Reflux ivider Head
• Large double coil Rodaviss Condenser
• Rodaviss Adapter
• Compression fitting
• PTFE Tubing
• 3 x Pilot Boss Heads
• 4-Prong Large Clamp
• Lower Support Ring
• Universal Clamp Cork Jaws
Note: Receiver flask/s
RR13924/6/8/30 is required to complete this kit.
RR239202 - Pilot Reflux Divider
with Vapour Temp Kit
• Reflux ivider Head with temp probe port
• Large double coil Rodaviss Condenser
• Rodaviss Adapter
• Compression fitting
• PTFE Tubing
• PTFE Pt100 Temp Probe
• PTFE Temp Probe Adapter
• 3 x Pilot Boss Heads
• 4-Prong Large Clamp
• Lower Support Ring
• Universal Clamp Cork Jaws
Note: Receiver flask/s RR13924/6/8/30 is required to complete this kit.
6. Component and Vessel Guide - Continued

Page 9
Reactor-Ready Pilot - Lab Reactor
6. Component and Vessel Guide - Continued
Single jacket
Popular choice, best suited for
heating only applications.
Vacuum jacket
The outer vacuum jacket provides
faster cooling, lower temperatures,
and prevents frosting for improved
contents visibility.
5 litre
Single Jacketed
Vessel
10 litre
Single Jacketed
Vessel
15 litre
Single Jacketed
Vessel
20 litre
Single Jacketed
Vessel
Cat No. (Reaction Vessel Only) RR235050 RR235100 RR235150 RR235200
Cat No. (Reaction Vessel Kit) RR220005 RR220015 RR220025 RR220035
Nominal Capacity 5 Litres 10 Litres 15 Litres 20 Litres
Total Working Volume 5.6 Litres 12.9 Litres 16.4 Litres 22.7 Litres
Internal iameter 180mm 240mm 260mm 290mm
External iameter 250mm 300mm 315mm 350mm
Jacketed Height 230mm 300mm 325mm 363mm
External Height (piston open) 526mm 606mm 640mm 674mm
Thermofluid Jacket Volume 4.6 Litres 6.2 Litres 5.7 Litres 8.3 Litres
Heat Transfer Area 0.16m20.27m20.31m20.38m2
Flange N200
Sidearm 20mm I Reactor-Ready
Piston Zero ead Space 25mm Glass Filled PTFE
Piston Run-off B24 Rodaviss Socket
5 litre
Vacuum Jacketed
Vessel
10 litre
Vacuum Jacketed
Vessel
15 litre
Vacuum Jacketed
Vessel
20 litre
Vacuum Jacketed
Vessel
Cat No. (Reaction Vessel Only) RR235052 RR235102 RR235152 RR235202
Cat No. (Reaction Vessel Kit) RR220010 RR220020 RR220030 RR220040
Nominal Capacity 5 Litres 10 Litres 15 Litres 20 Litres
Total Working Volume 5.6 Litres 12.9 Litres 16.4 Litres 22.7 Litres
Internal iameter 180mm 240mm 260mm 290mm
External iameter 300mm 350mm 350mm 415mm
Jacketed Height 225mm 300mm 325mm 363mm
External Height (piston open) 541mm 623mm 653mm 689mm
Thermofluid Jacket Volume 3.9 Litres 5.4 Litres 4.4 Litres 7.1 Litres
Heat Transfer Area 0.16m20.27m20.31m20.38m2
Flange N200
Sidearm 20mm I Reactor-Ready
Piston Zero ead Space 25mm Glass Filled PTFE
Piston Run-off B24 Rodaviss Socket

7.6 Screw 2 x stirrer support rods into the
locating holes on the vessel support platform.
Tighten the locking screws.
Reactor-Ready Pilot - Lab Reactor
7. Quick Start Guide
Page 10
7.1 Identify a clear unobstructed site within
your fumehood near two suitable power
outlets. You will require a power supply for
your thermoregulator and for your overhead
stirrer. Reactor-Ready Pilot should not be
moved after assembly so take care to locate
it in its final position. Position the base on a
flat surface. Lock the wheels in place.
7.2 Slide the 2 side support rods into the
locating bushes on the base.
o NOT tighten the locking screws.
7.5 Locate the lower end fitting of the brace
bar into the brace bracket on the base, and
secure with the retaining screw. Repeat with
second brace bar.
Locate the upper end socket of each brace
bar into the support platform brace bracket,
and secure with the retaining screw.
The vessel support platform may now be
levelled (with the aid of the level indicator)
by shortening or extending either or both of
the brace bars.
7.3 Slide down the Lower Supply Manifold
first and then the Upper Return Manifold
onto the left hand support rod.
7.4 Then slide down the vessel support
platform onto the support rods. Carefully
slide the rods through the lower hole in the
vertical brace and then into the upper hole
until it is full inserted.
The locking screws on the base bushes and
support platform may now be tightened.
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
MPORTANT NOTE
Once the stirrer support rods
are assembled in the support
platform, they should be
wiped evenly with the oil
lubricating cloth supplied.

Reactor-Ready Pilot - Lab Reactor
7. Quick Start Guide - Continued
Page 11
7.7 Slide two safety stop collars on to the
stirrer support rods, one on each rod,
followed by the stirrer support I-beam. Hand
tighten all knobs securely.
7.8 Assemble the Vessel Support Collar with
PTFE Liners onto the vessel neck and tight-
en.
7.11 Position the Stirrer Guide in the central
lid port and hand tighten the red (Rodaviss)
screw cap fitting to secure. Slide the stirrer
shaft into the Stirrer Guide so that the top just
protrudes from the recess of the aluminium
stirrer guide cap and tighten the cap to lock
the shaft in place.
7.9 Position the glass reactor on the vessel
support platform.
7.10 Assemble the Vessel O-Ring Seal and
PTFE Support Collar and place onto the
vessel neck flange.
7.12 Position the lid onto the O-Ring Seal
(on the vessel flange), close the clamp jaws
and lock with the fastening clip.
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
MPORTANT NOTE
Correct alignment of the Vessel
Support Collar is essential for
smooth operation of the clamp.
See section 8.8.

Reactor-Ready Pilot - Lab Reactor
7. Quick Start Guide - Continued
Page 12
7.13 Attach the Insulated Hoses to the Lower
Supply Manifold and Upper Return Manifold
by screwing the stainless female fitting onto
the stainless steel horizontal screw thread
fitting on the Manifolds. Tighten fully using a
spanner to ensure no leakage.
7.14 Attach the upper and lower Insulated
Hoses to the vessel sidearms, and tighten
the red (Rodaviss) screw cap fittings until
they are finger tight.
7.17 Adjust the height of the overhead stirrer
by loosening the locking knobs, and sliding
the Stirrer Support I-Beam down so that the
pins of the Stirrer rive Coupling engage with
the pins within the metal cap on the Stirrer
Guide.
7.18 Attach any additional accessories (drop-
ping funnels, solids addition funnels, temper-
ature probes etc) to the lid ports and secure
by hand tightening the red (Rodaviss) screw
cap fittings.
7.15 Slide the spindle of the Stirrer rive
Coupling into the overhead stirrer chuck, and
fully tighten the chuck.
7.16 Locate the rod of the overhead stirrer
into the hole in the sliding boss on the Stirrer
Support I-Beam.
7.19 Connect the thermoregulator Inlet and
Outlet hoses to the Reactor-Ready Pilot
Lower Supply Manifold and Upper Return
Manifold.
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
MPORTANT NOTE
The maximum operating
stirring speed for PTFE stirrer
guides in general is 500rpm
for continuous operation and
800rpm for short periods,
but for the large vessel
volumes in Reactor-Ready
Pilot, slower speeds should
be used.

Reactor-Ready Pilot - Lab Reactor
8. Set-Up and Operation
8.1 Optimising thermal performance
The thermal performance, whether heating or cooling, will be affected by:-
a. Ambient temperature and atmospheric conditions
b. Liquid load to be heated/cooled
c. Heating and cooling power of the thermoregulator
d. Nature of the thermofluid
Please take care to consider and optimise these parameters if you wish to maximise the
performance of your Reactor-Ready Pilot system.
8.2 Operating temperature range
Reactor-Ready Pilot can be used from -70°C to +230°C (thermofluid temperature) without
damage to the unit (Chemraz O-Rings are recommended for use above +150˚C). The
working reaction temperature range will vary depending on thermoregulator, vessel size,
contents volume etc as stated above.
Page 13
Warning - Risk of burns from hot or cold parts - Reactor-Ready
Pilot will remain hot or cold for some considerable time after the heating/cool-
ing source has been switched off. A temperature probe or temperature
sensitive label can be used to indicate when components are too hot or cold
to touch. Always wear suitable protective equipment such as gloves, face
protection, aprons etc.
!
Warning - Reactor-Ready Pilot should only be operated by trained and
competent personnel. As with all chemistries, a full risk assessment should be
performed prior to starting, and care should be taken to monitor reactions at
all stages. uring operation Reactor-Ready Pilot should not be left unattended
unless in a supervised area.
!
Warning - Always refer to the manufacturers specifications for the therm-
ofluid before using it with Reactor-Ready Pilot to be sure of any limitations or
safety restrictions.
!
Warning - Always refer to the manufacturer’s operating instructions for the
overhead stirrer before using it with Reactor-Ready Pilot to be sure of any
limitations or safety restrictions.
!
Warning - Always refer to the manufacturer’s operating instructions for your
thermoregulator before using it with Reactor-Ready Pilot to be sure of any
limitations or safety restrictions.
!
Warning - Please note that the Heidolph Hei-Torque 100 Value & Precision
stirrer motor models can create a minor low level vibration at speeds between
115 and 200rpm, which can result in the Reactor-Ready ‘drop-in coupling’
making a knocking noise. We recommend the use of the Hei-TORQUE 200
and 400 Value or Precision units with Reactor-Ready.
!

8.3 Setting up the base
8.3.1 Reactor-Ready Pilot comes as standard with swivel wheels. If you wish to replace
these with feet, please ensure this is done before proceeding any further with the set-up. See
step 8.3.2 for instructions on fitting the feet or ‘skip to step 8.3.3’ .
8.3.2 Replacing the wheels with feet
8.3.2.1 Carefully prise off the plastic end cap from the base. Invert the base so the wheels
are facing upwards.
8.3.2.2 Using an allen key, undo the bolt securing the wheel and remove the wheel from the
base.
Rotate the locking nut attached to the foot to the end of the thread nearest the foot, then
screw the foot into the thread inset in the base until approximately 10mm of the thread is
protruding inside the cavity.
8.3.2.3 Screw the separate nut on to the
exposed thread of the foot (inside the cavity)
until the thread is flush with the top of the nut.
o not screw the nut down tight.
8.3.2.4 Continue screwing the foot into the base
until it is at approximately the correct height.
Repeat with all 4 feet.
8.3.2.5 Replace the plastic cap.
8.3.2.6 Invert base and place it on the floor
where Reactor-Ready Pilot will be operated.
Adjust the height of the individual feet by
screwing in or out, until the 4 feet are firmly
engaging with the floor and the base is completely level.
Once level, tighten the locking nut on each foot with a spanner, ensuring that the foot doesn’t
move whilst this is being done. Finally, check that the base is still level, and completely stable
on the floor.
8.3.3 Position the Reactor-Ready Pilot
Identify a level and clear floor space within your fumehood to site your Reactor-Ready Pilot
assembly.
You will require two power outlets for an overhead stirrer and thermoregulator, cooling water
supply for the reflux condenser, inert gas and vacuum supply for operating under an inert
atmosphere.
Make sure there is sufficient room for connections to the thermoregulator and that all
thermofluid hoses can be positioned and supported safely.
8.3.4 When using wheels make sure the wheels are locked in place before set-up begins.
Reactor-Ready Pilot - Lab Reactor
8. Set-Up and Operation - Continued
Page 14
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
MPORTANT NOTE - If wheels are fitted, the ‘empty’ framework may be
safely moved from one location to another, but should not be moved once
loaded with a vessel or other accessories.
8.3.2.1
8.3.2.2
8.3.2.4 8.3.2.5
Locked Unlocked
8.3.4
8.3.2.6
8.3.2.3

8.3.5 Slide the 2 side support rods into the holes in the locating bushes on the base. The rods
are a loose fit. o not to tighten the locking screws on the bushes at this stage.
8.4 Assembling the Manifolds
8.4.1 Reactor-Ready Pilot features independent Supply and Return Manifolds to simplify the
connection between the thermoregulator and reaction vessel. The manifolds are attached to
the support rods and feature precision bore slide bearings. These allow for smooth and
independent vertical adjustment and horizontal rotation, providing flexibility in accommodating
different vessel sizes.
8.4.2 With the drain tap pointing down slide the Lower Supply Manifold (Inlet Manifold with
rain) down the left hand Support Rod. Tighten the locking knob to secure the Manifold to
the Support Rod. Ensure that you leave enough space below the Manifold to allow
thermoregulator hoses to be attached.
8.4.3 With the ball valve vent pointing upwards slide the Upper Return Manifold (Outlet
Manifold with Vent) down the left hand Support Rod. Tighten the locking knob to secure the
Manifold to the Support Rod. Ensure that you leave enough space below the Manifold to
allow thermoregulator hoses to be attached.
Reactor-Ready Pilot - Lab Reactor
8. Set-Up and Operation - Continued
MPORTANT NOTE - Moving parts should be kept clean and free from any
obstructions or surface contamination. Parts relying on sliding motion may
benefit from regular application of a thin surface coating of lubricating oil
(a lubricating cloth is supplied with all systems, RR121027).
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
8.3.5
8.4.3
8.4.1
Page 15
8.4.2
Upper Return Manifold
Lower Supply Manifold
MPORTANT NOTE - The Upper Return Manifold should be positioned on the
Support Rod such that the ball valve vent is pointing upwards. Failure to
observe this may result in leakage of thermofluid from the valve during
drainage.
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
MPORTANT NOTE - The Supply and Return Manifolds can be positioned on
either of the Side Support Rods, but it is recommended that the left rod only
is used, as this allows the most ergonomic alignment of hoses, vessel and
other system components. If it is necessary to use the right rod to support the
manifolds, go to 8.5.
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
MPORTANT NOTE - The Lower Supply Manifold should be positioned on the
Support Rod such that the drain tap is pointing downward. Failure to observe
this will result in incomplete drainage of the vessel.
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
MPORTANT NOTE - Ensure that the valves on the Supply and Return
Manifolds are in the closed positions.
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Warning - If using rigid feet with the Reactor-Ready Pilot it is important to
make sure that base is level and stable and the feet locking nuts fully
tightened. Failure to observe this may lead to incorrect alignment of
framework assembly and reaction vessel, leading to instability and potential
damage.
!

8.5 Assembling the Manifolds on the right hand rod
If space requirements dictate assembly of manifolds on the right hand rods, fittings on the
upper and lower manifolds must be reconfigured. This will require that, counter intuitively, you
locate the Upper Return Manifold at the bottom and the Lower Supply Manifold at the top of
the right hand rod (the opposite way round to that described in 8.4).
8.5.1 Firstly, with the ball valve vent pointing down, slide the Upper Return Manifold (Outlet
Manifold with Vent) down the right hand Support Rod. Tighten the locking knob to secure the
Manifold to the Support Rod. Ensure that you leave enough space below the Manifold to
allow thermoregulator hoses to be attached.
8.5.2 Secondly, with the drain tap pointing upwards, slide the Lower Supply Manifold (Inlet
Manifold with rain) down the left hand Support Rod. Tighten the locking knob to secure the
Manifold to the Support Rod. Ensure that you leave enough space below the Manifold to
allow thermoregulator hoses to be attached.
8.5.3 With the use of a suitable spanner remove the drain spout on the Lower Supply
Manifold and retain.
8.5.4 With the use of a suitable spanner remove the air bleed fitting on the Upper Return
Manifold and retain.
8.5.5 Refit the air bleed fitting on the Lower Supply Manifold. This now becomes the Upper
Return Manifold.
8.5.6 Refit the drain spout on the Upper Supply Manifold. This now becomes the Lower
Supply Manifold.
8.5.7 Re-tighten the drain spout and air bleed fitting on both manifolds to ensure that they
seal.
8.5.8 Realign the 90 degree, M30 fittings by loosening the female swivel connector, moving
the fitting to the correct orientation and re-tighten the connector.
8.5.9 When using the manifolds assembled on the right hand rods, it is also necessary to
reposition the hose tidies. Remove the 2 hose tidies from the left hand side vertical brace, by
unscrewing bolts using the allen key provided. Refit the hose tidies in the 2 locating holes on
the right hand side brace. Retighten the bolts.
Reactor-Ready Pilot - Lab Reactor
8. Set-Up and Operation - Continued
Page 16
MPORTANT NOTE - When using the manifolds on the right hand rod, the
relative positioning of the vessel side arms and hose tidies is different to when
using the left hand rod and it may be difficult to connect the hose to the
vessel or access the hose tidies with some vessel sizes.
Therefore it may be necessary to rotate the vessel collar on the vessel (away
from the centre line) to optimise alignment with the hoses and/or hose tidies.
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
8.5.3
8.5.6
8.5.5
8.5.4
8.5.8

8.6 Locating the support platform
8.6.1 Locate the Vessel Support Platform on to the side support rods, by first engaging the
lower bracket on each side of the platform down onto the rods, then sliding down to engage
the upper bracket. Ensure that the upper bracket is fully pushed down onto the support rods
on each side.
8.6.2 Insert and tighten the locking screws on the base locating bushes (2 on each bush)
8.6.3 Insert and tighten the locking screws on the vessel support platform to secure the
framework.
8.6.4 It is advisable to partly tighten each locking screw initially, before fully tightening, to aid
alignment. If framework is not straight, loosen the 8 screws, realign the poles, and re-tighten.
8.7 Assembling the Brace Rods & Leveling the Framework
8.7.1 To provide maximum stability, and to aid alignment,
Reactor-Ready Pilot features adjustable, lockable rear brace
bars.
The brace bars feature a threaded adjustable fitting, with lock
ring, at each end. Fittings have opposite threads, left hand
reverse thread is indicated with a groove.
8.7.2 For each brace bar, loosen the locking nut at each end so that it is well away from the
bar. Partly unscrew the end fitting at each end, so that there is a reasonable length of thread
showing, with roughly equal thread at each end.
Roughly position the brace bar in the framework so that the end fittings are engaged in the
upper and lower brace brackets on the vessel platform and base respectively to check for
length. Through-holes in the brace bar end fittings should line up with the through-holes in
the brace brackets. If the holes do not line up, adjust one, or both end fittings on the bar until
they do, taking care to ensure that roughly equal lengths of thread remain exposed at each
end.
8.7.3 Insert the retaining screws (x4) both top and bottom, on both braces, and tighten with
allen key.
8.7.4 Once secured in the framework, the lengths of the brace bar may be adjusted, by
turning the bar clockwise or anticlockwise. This allows the vessel platform to be fully braced,
and allows fine adjustment on the levelling of the platform.
To lengthen the brace bar, ensure that the locking rings at each end are loosened, then twist
the bar clockwise (looking from above). To shorten the brace bar, twist the bar anticlockwise.
8.7.5 Use built-in spirit level on Vessel Support Platform to view level.
8.7.6 Once brace bars have been fully adjusted, tighten the locking rings at each end.
Reactor-Ready Pilot - Lab Reactor
8. Set-Up and Operation - Continued
8.6.1
8.6.2
8.7.2
8.7.3
8.6.3
8.7.1
Page 17
8.7.4 8.7.6
8.7.5
Warning - In some circumstances, overtightening or over-extending the
brace bars may result in twisting of the frame and one or more wheels/feet
lifting off the floor. Under no circumstances should the framework be assembled
such that any of the wheels/feet are not in proper contact with the floor.
!
MPORTANT NOTE - Brace bar fittings have opposite threads on each end.
The left hand reverse thread is indicated with a groove.
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,

Reactor-Ready Pilot - Lab Reactor
8. Set-Up and Operation - Continued
8.8 Assembling the Stirrer Support
8.8.1 Screw two Stirrer Support Rods into the threaded holes on the Vessel Support
Platform. Ensure the rods are fully tightened, with no exposed thread.
Insert and tighten the locking screws on the Vessel Support Platform to fully secure the rods.
8.8.2 The Stirrer Support I-Beam is designed to support an overhead stirrer and features
precision bore slide bearings enabling smooth height adjustment - offering maximum user
flexibility in configuring the system.
8.8.3 Slide the two Safety Stop Collars onto the Stirrer Support Rods (one to each rod),
sliding to the required position and tightening the locking knobs to secure.
8.8.4 Slide the Stirrer Support I-Beam down the Stirrer Support Rods to the required position
then secure with the two locking knobs. Ensure that the
I-Beam is orientated such that the two knobs on the central
sliding boss are pointing upwards and forwards.
8.8.5 Adjust the Safety Stop Collars so that they are located
directly under the Stirrer Support I-Beam and re-tighten.
8.9 Preparing the Reaction Vessel
8.9.1 Reactor-Ready Pilot is capable of supporting a range of dedicated reaction vessels
ranging in size from 5 litres to 20 litres in either single jacket or vacuum jacket format.
8.9.2 Invert the vessel by resting the flange on a flat surface.
8.9.3 Add the 4 x PTFE Liners to the support collar as pic 8.9.3.
8.9.4 Undo the bolts on the Support Collar and place the collar around the straight sided neck
of the vessel, resting squarely on the step around the glass neck of the vessel. Ensure that
the lower edge of the Support Collar (the side nearer the flange of the vessel) is faced with
the white PTFE liners. Partly tighten the bolts using an allen key.
8.9.5 Rotate the Support Collar so that the
tabs with the fastening bolts are parallel
with the vessel side arms.
8.9.6 Tighten the bolts carefully on each
side of the collar. When fully tightened
there should be NO gap between the two
halves of the collar.
8.8.1
8.8.3 8.8.4
8.8.1
MPORTANT NOTE - Moving parts should be kept clean and free from any
obstructions or surface contamination. Parts relying on sliding motion may
benefit from regular application of a thin surface coating of lubricating oil.
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
MPORTANT NOTE - The Reactor-Ready Pilot
vessel Support Collar is NOT designed to accept
reactors from other manufacturers. The vessel
neck, flange and lid geometry are specifically
engineered to ensure a safe and leak tight seal.
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
` mportant Note - Correct positioning of the Vessel Support Collar is critical for
proper alignment of the vessel when operating the clamp. If after assembling
the vessel collar, the vessel is not vertically aligned when positioned on the
platform, remove and refit the vessel collar as described in 8.9.3.
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Page 18
8.9.3
No Yes 8.9.48.9.5
8.9.2
8.8.5
8.9.3

8.9.7 To locate the vessel into the Pilot framework, support with two
hands, slightly tilt the vessel top away from you and carefully locate
the lug at the back of the Vessel Support Collar into the central
cut-out in the Vessel Support Platform.
8.9.8 Then by returning the vessel to the perpendicular plain, the two
side lugs on the Vessel Support Collar will locate into the two
rectangular recesses on the arms of the Vessel Support Platform.
The vessel is now fully supported.
mportant Note - When the vessel is supported
on the Vessel Support Clamp some movement of
the vessel is still possible until the lid is located
and vessel clamp is closed.
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Page 19
8.9.6
8.9.9 Assemble the FEP O-Ring Seal and PTFE O-Ring Support Collar and place the
assembly onto the vessel flange, ensuring that the retaining lip is fully located within the glass
neck of the vessel.
8.10 Assembling the vessel lid, stirrer guide and probe
Before attaching the lid to the reaction vessel the
stirrer assembly must be attached to the lid.
8.10.1 Position the Stirrer Guide in the central B34
lid port. Hand tighten the central red (Rodaviss)
screw cap to secure.
8.10.2 Loosen the metal cap on the Stirrer Guide
8.10.3 Slide the stirrer shaft through the Stirrer
Guide from below
8.10.4 Ensure the top of the stirrer shaft is sitting just
above the top of the metal cap.
8.10.5 Hand tighten the metal cap to lock the stirrer
shaft in place.
8.10.6 Locate the lid on the vessel by guiding the
stirrer shaft through the neck of the vessel before
positioning the lid over the upper lip of the PTFE
O-Ring Support Collar sitting on the vessel flange.
Ensure that the vessel, O-Ring and lid are all sitting
flush.
8.9.8
Reactor-Ready Pilot - Lab Reactor
8. Set-Up and Operation - Continued
mportant Note - The glass lid is supplied with (Rodaviss) red sealing caps
that are used to blank off the ports when not in use. The sealing caps have
PTFE-faced inners for an inert seal.
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
8.9.8
8.9.7
8.10.2
8.10.4 8.10.5
8.10.3
8.10.1
8.10.6
mportant Note - The FEP O-Ring Seal and PTFE O-Ring Support Collar
must always be used with all size vessels otherwise the vessels and lid will
not seal.
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,
Important, Important,