Thermo Scientific iCAP 6000 Series User manual

2007 Thermo Fisher Scientific. All rights reserved.
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iCAP 6000 Series
Pre-Installation Manual
Version 4.2
Part number 8499 400 30001

Thermo Fisher Scientific iCAP 6000 Series Pre-Installation Manual v4.2 ii
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Thermo Fisher Scientific iCAP 6000 Series Pre-Installation Manual v4.2 iii
Contents
Contents ............................................................................................iii
Introduction....................................................................................1-1
System Accessories.........................................................................2-2
Transportation ...............................................................................3-1
Package Size .................................................................................3-1
Short Term Storage .......................................................................3-2
Transit Damage.............................................................................3-2
Warranty .......................................................................................3-2
Working Area Requirements........................................................4-1
Introduction...................................................................................4-1
Location ........................................................................................4-1
Environmental Requirements........................................................4-2
Electrical .......................................................................................4-2
Spectrometer Size .........................................................................4-4
Gas Requirements .........................................................................4-5
Water Temperature Control ..........................................................4-5
Waste Storage ...............................................................................4-6
Spectrometer Fume Extraction .....................................................4-6
Sample Fume Extraction...............................................................4-8
Communications Interface............................................................5-9
On the Spectrometer .....................................................................5-9
On the Data Station.......................................................................5-9
Pre-Installation Checklist............................................................6-11
Special Agreements........................................................................7-1
Chapter 1
Chapter 2
Chapter 3
Chapter 4
Chapter 5
Chapter 6
Chapter 7

iv iCAP 6000 Series Pre-Installation Manual v4.2 Thermo Fisher Corporation
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Thermo Fisher Scientific iCAP 6000 Series Pre-Installation Manual v4.2 1-1
Chapter 1
Introduction
This manual is designed to help ensure that your iCAP 6000 Series
ICP-OES Spectrometer will be installed efficiently and will be able
to meet your requirements quickly and completely.
It will minimise installation time if the services and facilities detailed
here are available before the equipment is delivered.
Properly installed and maintained, your system will provide you with
years of reliable service. Please inform your local Thermo Fisher
organisation what aspects of support are most important to you and a
tailored agreement can be provided to prolong the life of your
instrument.
This manual describes the environment and the resources required at
the installation site of the iCAP 6000 Series ICP-OES Spectrometer
and associated equipment. Safety requirements for the installation are
also detailed.
WARNING: The installation of all services must comply with the
appropriate rules and regulations required by the local authorities
responsible for those services in the workplace, at the installation
site. An installation engineer is not responsible for the fitting, or
compliance of the facilities, or services.
The choice of an operating site for the instrument will be influenced
by local considerations for example, ease of access and availability
of electrical power.
Logical planning of the installation can save both time and money.
The objective of this manual is to provide information that will
enable the best site to be chosen and to highlight the essential
requirements.
If further information or advice is required, contact your local
Thermo Fisher organisation. A list of Thermo Fisher organisations
and agents can be found on http://www.thermofisher.com.
Installation of the system will include some familiarisation training;
however comprehensive method development and software training
will require additional training that should be ordered separately.

System Accessories
Package Size
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Chapter 2
System Accessories
Required:
Recirculating chiller unit (see specification)
Data Station (see specification)
Optional:
Cetac ASX-520 Autosampler (requires dedicated RS232 on Data
Station)
Cetac ASX-260 Autosampler (requires dedicated RS232 on Data
Station)
Cetac EXR-8 Autosampler (requires dedicated RS232 on Data
Station)
Cetac ASX 1400 Autosampler (Stirring)
Cetac U-6000AT+ Ultrasonic Nebuliser
Elemental Scientific, Inc. SC SC4 Autosampler
Elemental Scientific, Inc. SC4 Fast Autosampler
Argon Humidifier
SSEA – Solid sampling device (requires dedicated RS232 on
Data Station and iCAP 6000 accessory board)
Laser – Solid sampling device (requires dedicated RS232 on Data
Station and iCAP 6000 accessory board)
High Solids Sample Introduction kit
HF Acid Sample Introduction kit
Organics Sample Introduction Kit
Volatile Organics Sample Introduction kit
Please request site requirement guides for any purchased accessories

Thermo Fisher Scientific iCAP 6000 Series Pre-Installation Manual v 4.0 3-1
Chapter 3
Transportation
The spectrometer is supplied with all compatible accessories that
have been purchased to meet the customer's system requirements.
Items may be shipped in separate packages.
WARNING: All items should be transported to the installation site
on pallets, in their original packaging and the right way up. Under no
circumstances may any package be moved without its pallet unless
under the direct control of an authorised Thermo Fisher service
engineer.
Proposed routes from the customer receiving area to the installation
site must be checked for suitability. The largest pallet size should be
used to calculate clearances.
WARNING: The boxed Spectrometer should be moved using a
mechanical lift. Five people should be used if it has to be moved by
hand taking appropriate precautions. Care should be taken in
doorways, corridors or when lowering to avoid trapping fingers.
The instrument will be supplied inside especially designed
packaging. The dimensions are:
Table 3–1. Packaged Dimensions and Weight
Width Depth Height Weight
980 mm 900 mm 920 mm 95 Kg
(38.6 in) (35.4 in) (36.2 in) (210 Ib)
Transportation to some destinations may necessitate additional
packaging, for example a packing crate. Dimensions and exact
specifications may vary.
Package Size

Transportation
Short Term Storage
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To maintain the instrument in serviceable condition and to comply
with the conditions of warranty, ensure that storage of each item is
maintained within the stated parameters detailed for the Working
Area Requirements below. Make sure that the packages are stored
the correct way up.
Note: Do not open the Packages without the permission of the
Thermo Fisher engineer
When the packages are opened prior to installation, the contents will
be checked against the packing list(s).
Before accepting delivery of any equipment, the packages should be
inspected for signs of obvious damage. The nature of the damage
should be noted on the delivery notice and signed by the carrier's
representative.
Within the time stated in the Thermo Fisher terms and conditions an
inspection should be made for concealed damage. The local Thermo
Fisher organisation should be advised of any damage in writing and,
on receipt of specific instructions, the customer should return the
equipment complete and in the original packing material.
Note that the instrument is warranted against defects in material and
workmanship for a period of 12 months from installation, or 15
months from shipment, whichever comes first. This warranty does
not cover damage sustained as a result of improper storage by the
customer prior to installation, or resale to a third party.
Note: Warranty is not transferable to a third party without Thermo
Fisher approval.
Short Term
Storage
Transit Damage
Warranty

Thermo Fisher Scientific iCAP 6000 Series Pre-Installation Manual v 4.2 4-1
Chapter 4
Working Area Requirements
The choice of site will be influenced by the dimensions and weights
of the spectrometer and accessories. Other factors are the
environment and the availability of electricity, water and gas
supplies, as well as the need for a suitable ventilation system to
dispose of the exhaust gases. All of these factors are covered in the
following sections.
Pre-installation visits can be made on request, but may be
chargeable.
Prior to installation make sure that the proposed area is compatible
with the conditions specified. The laboratory must offer a dry, even
temperature and dust-free conditions, with no possibility of
condensation forming. Sample preparation activities and corrosive
materials should be located in a separate room to avoid problems due
to corrosive fumes.
A comprehensive ‘Risk Assessment’ should be carried out that is
specific to the handling of solvents, samples and sample preparation.
Particular consideration should be taken to avoid direct sunlight,
proximity to heat sources, draughts and vibration. Do not locate the
system where sudden changes in temperature can occur, for
example near a door or window, care should be taken with the
location of items such as air conditioning vents and heating vents.
The instruments are designed for use on a normal laboratory bench.
Ideally the instrument should be placed on a moveable bench with
0.5 meters of access behind the instrument. The mounting surface
must be level and the instruments must not be placed on any type of
cushioning as this could block ventilation.
The mounting arrangements should be capable of supporting the
weight of the spectrometer and its accessories. Make sure that the
working surface is sufficiently rigid to prevent vibration as this may
affect the optical alignment of the spectrometer and accessories.
To avoid the possibility of liquid ingress into the top of the
spectrometer the location should ensure it is not possible to store
sample or other liquids directly above the instrumentation.
Organic or volatile solvents should not be stored, even for a short
time, near the instrument.
Introduction
Location

Working Area Requirements
4-2 iCAP 6000 Series Pre-Installation Manual v3.1 Thermo Fisher Corporation
Do not position the equipment so that it is difficult to operate the
extraction, electrical supply, cooling water, purge gas and plasma gas
controls.
The atmospheric temperature requirement is 15 to 35°C (60 to 95°F),
the temperature should not change by more than 2°C per hour.
Atmospheric humidity should be 20 to 80% m/v for an ambient
temperature between 15 and 30°C and 20 to 60% m/v for an ambient
temperature between 30 and 35°C. Atmospheric conditions must be
non-condensing. The instrument room should be at a positive
pressure with respect to rooms with a corrosive atmosphere.
Warning:Argon is an asphyxiant; if the extraction is turned off
sufficient air must be supplied to prevent the concentration of Argon
reaching a harmful level.
The spectrometer will require an electrical supply at 200 to 240 VAC
4 KVA 50/60 Hz. The spectrometer will be supplied with a 2.5m
mains cord.
For customers in the USA and Canada the mains cord supplied will
terminate in a NEMA L6-20P Twist&Lock plug. (Coding is black (X
– ac high), white (Y – ac low), green (G – earth/ground).
Figure 4–1. NEMA L6-20P plug for USA/Canada
For customers in the rest of the world the mains lead is shipped with
no terminating plug, but with wires ready for a suitable 20 A plug.
Coding is blue (neutral), brown (live), green/yellow (earth/ground).
Connection to the laboratory supply should be with an appropriately
rated plug conforming to local electrical guide lines and local
requirements. It must be possible to electrically isolate the
instrumentation.
Environmental
Requirements
Electrical