ABB ICOS GLA431-MCIA User manual

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ABB MEASUREMENT & ANALYTICS | USER MANUAL
User Manual | ICOS
GLA431-MCIA Enhanced Performance
Benchtop Continuous Flow Analyzer

USER%MANUAL!| ICOS | INSTRUCTIONS | UM/ICOS-EN REV. B.2
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Table of Contents
Disclaimer....................................................................................................................................... 5%
Cyber Security............................................................................................................................ 5%
Patent.............................................................................................................................................. 5%
Copyright........................................................................................................................................ 5%
Safety .............................................................................................................................................. 6%
Class of Laser Equipment........................................................................................................ 6%
Certification ............................................................................................................................... 6%
WEEE Directive........................................................................................................................... 6%
Labels........................................................................................................................................... 7%
Operator Safety ......................................................................................................................... 7%
Electrical Hazards...................................................................................................................... 7%
Laser Hazards ............................................................................................................................ 8%
Safety Provisions for a Chemical Spill................................................................................... 8%
Text Formats and Warning Icons........................................................................................... 9%
Transportation and Storage of Boxed Analyzers ................................................................. 10%
Positioning the analyzer............................................................................................................ 10%
Warranty ........................................................................................................................................11%
Customer Support.......................................................................................................................11%
1%Analyzer Overview........................................................................................................................... 12%
Performance Specifications ..................................................................................................... 12%
Ambient Humidity ................................................................................................................... 12%
Operating Temperature......................................................................................................... 12%
Maximum Altitude................................................................................................................... 12%
Power Requirements .............................................................................................................. 12%
Fuse Ratings............................................................................................................................. 12%
Cable Plugs and Voltage for EC Countries ......................................................................... 12%
Standard Components .............................................................................................................. 13%
Optional Components ............................................................................................................... 13%
Power Connections .................................................................................................................... 15%
Data Interface Connection Ports............................................................................................. 16%
Plumbing Diagram.......................................................................................................................17%
Inlet/Outlet Connections .......................................................................................................... 18%
Warning Labels and Descriptions............................................................................................ 19%
Specifications..............................................................................................................................20%
2%Analyzer Setup................................................................................................................................. 21%
Connect the Power Cords...................................................................................................... 21%
Connect the Data Interface Connections........................................................................... 21%
Connect the Inlet/Outlet Plumbing Connections............................................................. 21%
The Pretreatment Box ............................................................................................................ 22%
Connect the Pretreatment Box, Pump, and Analyzer....................................................... 23%
Attach&and&Tighten&the&Swagelok&Connectors .................................................................................24%

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3%Initialize and Run the Analyzer ..................................................................................................... 25%
File System Integrity Check ...................................................................................................... 26%
Thermal Stabilization................................................................................................................. 26%
The Launch Service Screen........................................................................................................ 27%
The Auto Launch Screen............................................................................................................28%
Login to Access Menu Options ................................................................................................ 29%
Main Panel ....................................................................................................................................30%
User Interface Control Bar..................................................................................................... 31%
Main Panel Displays.................................................................................................................... 33%
Numeric Display....................................................................................................................... 33%
Alarm Status Display ..............................................................................................................34%
Spectrum Display .................................................................................................................... 37%
TimeChart Display................................................................................................................... 39%
Rate Control.................................................................................................................................40%
File Transfer Menu ...................................................................................................................... 42%
Standard Data File ..................................................................................................................42%
Transfer Data Files..................................................................................................................43%
Types of directories in the local hard drive ...........................................................................45%
Daily Directory..........................................................................................................................45%
Archive Directory .....................................................................................................................46%
File Transfer Error Screen ......................................................................................................... 47%
Setup Menu ..................................................................................................................................48%
Time/Files Tab.........................................................................................................................49%
Calibration Tab ........................................................................................................................ 52%
Laser Adjust Tab......................................................................................................................54%
MIU tab ......................................................................................................................................56%
DCS Tab (Optional) ................................................................................................................. 57%
Service .......................................................................................................................................58%
Shutting Down the Analyzer .....................................................................................................59%
4%Maintenance....................................................................................................................................60%
Daily Operation Checklist..........................................................................................................60%
Mirror Ring-Down Time and Maintenance.............................................................................60%
Replace the Power Inlet Fuse.................................................................................................... 61%
Appendix A:%Accessing Data Using the Ethernet ........................................................................ 62%
Additional Notes .........................................................................................................................63%
Appendix B:%Wireless Router Setup................................................................................................64%
To use the wireless router: ....................................................................................................64%
Connect to a Windows Computer........................................................................................65%
Reconfiguring the Wireless Router...................................................................................... 67%
Appendix C:%Set Up Devices for Remote Access Using VNC Software ................................... 76%
Appendix D:%Multi-Port Inlet Unit (Optional)................................................................................89%
Appendix E:%External Dynamic Dilution System (Optional).......................................................94%
Appendix F:%Batch Mode Operation (Optional)...........................................................................99%
Appendix G:%Isotope Definitions ..................................................................................................108%

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Appendix H:%Cables .........................................................................................................................109%
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Disclaimer
This document contains product specifications and performance statements that may be
in conflict with other ABB published literature, such as product flyers and product catalogs.
All specifications, product characteristics, and performance statements included in this
document are suggested specifications only. In case of conflict between product
characteristics in this document and specifications in the official ABB product catalogs, the
latter takes precedence.
ABB reserves the right to make changes to the specifications of all equipment and
software, and to the contents of this document, without obligation to notify any person or
organization of such changes. Every effort has been made to ensure that the information
contained in this document is current and accurate. Please contact ABB-LGR if you find any
error in this document, so we can make appropriate corrections.
Cyber Security
This product is designed to be connected to and to communicate information and data via
a network interface. It is your sole responsibility to provide and continuously ensure a
secure connection between the product and your network or any other network (as the
case may be). You shall establish and maintain any appropriate measures (such as, but not
limited to, the installation of firewalls, application of authentication measures, encryption
of data, etc.) to protect the product, the network, its system and the interface against any
kind of security breaches, unauthorized access, interference, intrusion, leakage and/or
theft of data or information. ABB and its affiliates are not liable for damages and/or losses
related to such security breaches, any unauthorized access, interference, intrusion, leakage
and/or theft of data or information.
Patent
The analyzer technology is protected by patents:
•7,468,797
•6,839,140
•6,795,190
•6,694,067
Copyright
© 2020 ABB Inc. All rights reserved. No information contained in this document may be
reproduced in any form, in full or in part, without prior written consent from ABB.

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Safety
The following pages provide important safety precautions.
Class of Laser Equipment
The analyzer is a Class 1 laser instrument when the case cover is closed for normal
operation, and the lock is installed.
Certification
The analyzer certifications are listed in Table 1.
Table 1: Safety Certifications
Symbols
Standards Tested and Met
2004/108/EU (EMC), EN61326-1
Title 21 Code of Federal Regulations, chapter 1, sub-chapter J
WEEE Directive
The analyzer is not subject to WEEE Directive 2002/96/EC (Waste Electrical and Electronic
Equipment) or relevant national laws (e.g. ElektroG in Germany).
The product must be disposed of at a specialized recycling facility. Do not use municipal
garbage collection points. According to the WEEE Directive 2002/96/EC, only products
used in private applications may be disposed of at municipal garbage facilities.

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Labels
The following labels are at specific locations on or in the analyzer to identify
hazardous areas. (Figure 1)
Figure 1: Radiation Labels
These labels are located on the enclosure covering the ICOS cell. The fiber laser is
visible only when the insulated enclosure is removed from the ICOS cell.
Operator Safety
When the case cover is closed and locked into position, the analyzer runs safely, without
risk to the operator. Modifying the analyzer to operate with the case cover open can injure
personnel.
Bypassing the analyzer interlock switch to open the case cover during
analyzer operations can cause serious bodily injury. Even though the
analyzer provides a second layer of protection, such as a laser cover to
prevent the user from the invisible laser beam or any secondary reflection
from the laser on a reflective surface, it is not recommended to modify the
analyzer to operate in an unsafe condition.
Electrical Hazards
The analyzer poses no electrical hazards. The analyzer components operate at ≤6.8 V DC.

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Laser Hazards
The analyzer is a Class 1 laser product that complies with:
•21 CFR 1040.10 and 1040.11
•EN 60825-1:2014
The laser is classified as a Class IIIb when exposed.
Only trained service personnel are authorized to open the housing or
service the laser.
Using this analyzer in a manner not specified by ABB-LGR may result in
damage to the analyzer and render it unsafe to operate.
Only authorized persons may open the analyzer cover or perform internal
maintenance. Contact ABB-LGR for maintenance instructions and
maintenance kits. Make sure the analyzer is unplugged before working
with the internal components. Failure to do so may result in damage to
the analyzer and electric shock.
Safety Provisions for a Chemical Spill
Follow these precautions when dealing with all chemicals:
•Keep all chemical containers away from heat, sparks, and open flames.
•Use only on grounded equipment and with non-sparking tools.
•Store in a cool, dry, and well-ventilated place, away from incompatible materials.
If a spill occurs:
•Make sure all handling equipment is electrically grounded.
•Mop or wipe up, and then place all chemical-soaked items in containers approved
by the US Department of Transportation (DOT) or the appropriate local regulatory
agency.

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Text Formats and Warning Icons
Text Formats
This section describes text formats and warning icons used in this manual.
• Italicized text is used for emphasis in text and also to emphasize the names
of screens or text fields.
•Bold text is used to show text that you type in fields and also button
choices that you enter.
Warning Icons
Table 2 shows and describes the warning icons used in this manual.
Table 2: Warning Icon Descriptions
Icon
Meaning
Emphasizes facts and conditions important to analyzer operation.
WARNING!
General Warning Icon: gives general safety information that must be
followed to avoid hazardous conditions.
WARNING!
Electrical Warning Icon: warns of potential electrical shock hazard.
WARNING!
Laser Warning Icon: warns of potential laser hazard.

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Transportation and Storage of Boxed
Analyzers
When transporting and storing boxed analyzers:
•Analyzers may be shipped in non-pressurized aircraft.
•Analyzers are fragile: Do not drop or smash boxed analyzers.
•Do not store analyzers outside in wet weather.
•Do not stack boxes more than five high.
•Analyzers may be safely stored at temperatures between -20oC and +60oC.
Save the original shipping materials to use when returning the analyzer to
ABB-LGR if factory service or repair is needed.
Table 3 lists and describes the safety icons on ABB-LGR shipping boxes. Follow these
instructions when transporting and storing boxed analyzers.
Table 3: Transportation and Storage Icon Descriptions
Icon
Meaning
Store your analyzer in a sheltered, dry area. Do not let the box get
wet.
Transport and store the analyzer box with the arrows on the box
pointing up.
The analyzer is fragile. Transport carefully. Do not drop the box.
Positioning the analyzer
Positioning the analyzer is a two-person task. With one person on each side, lift the
analyzer out of the box and onto a flat surface. Leave four inches of free space on each side
of the analyzer for proper ventilation.

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Warranty
Warranty terms and conditions are covered by terms and condition agreed upon during the
sales process.
Please contact icos.suppor[email protected]bb.com and your local sales representative for more
details.
Customer Support
ABB provides product support services worldwide. To receive product support, either in or
out of warranty, contact the ABB office that serves your geographical area, or the office
indicated below:
ABB Inc. Measurement & Analytics
3400, rue Pierre-Ardouin
Quebec, (Quebec) G1P 0B2 Canada
Tel: [phone] (North America)
Tel: [phone] (Worldwide)
Fax: [phone]
Technical Support: Icos.[email protected]
Please contact icos.[email protected].com and your local sales representative for more
details.
Please provide the serial number or sales order number of the analyzer.

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1 Analyzer Overview
The ABB-LGR GLA431-MCIA1 Methane Carbon Isotope Analyzer measures gas
concentrations in parts per million (PPM), and isotope ratios in parts per thousand (per
mil). It provides accurate isotope ratio measurements rapidly and with high precision.
This analyzer is a Class 1 laser product.
Performance Specifications
Ambient Humidity
•<99% relative humidity non-condensing
Operating Temperature
•0 - 45oC
Maximum Altitude
•6,000 Feet
Power Requirements
•115/230 VAC, 50/60 hz
•150 W (steady state)
•550 W with the ACC DP3H external pump
Fuse Ratings
•250 VAC
•10 Amps
Cable Plugs and Voltage for EC Countries
•See page 109
Always use the power supply cord provided by ABB-LGR. See page 109 for
a description of power cords for a specific country.
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Standard Components
This section describes the analyzer components. Verify that each of the system
components has arrived before installation.
The standard components include:
Basic free-flow system:
•Analyzer
•Analyzer power cord
•User guide (this document)
•USB flash drive
•Serial port connection cable (null modem type)
•Exhaust Muffler
•Pretreatment box:
oOne - 6’ x ¼”
oTwo - 6’ x 3/8”
•External pump (ACC DP3H)
oPump connection kit
oPump slave power cord
•Pump orifice for low flow mode.
Optional Components
Multiport Inlet Unit (8 or 16 channels)
•Power Cable for MIU
•25-pin connection cable for control signal
Batch injection system
•Syringe injection port
•140mL syringe
•Centering needle
•Septa (box of 50)
•Septum Puller
Dilution Control System (EDDS)
•Control Cable
•Sample Line
•One 6’ x ¼” Zero-air (connects to house air supply)
•Line to sample supply
•Tee connector for the analyzer inlet port
This analyzer has been CE certified using data cables three meters long or
less. Connecting the analyzer using longer data-cables is not
recommended.
If you have not received all of these components, contact ABB-LGR at
[e-mail].

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Figure 2 shows the front of the analyzer.
Figure 2: Front Panel
Figure 3 shows the back of the analyzer with connections.
Figure 3: Back Panel

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Power Connections
Figure 4 shows the power connections on the back panel, and Table 4 describes the
connections.
Figure 4: Power Connections and AC Voltage Selection Switch
Table 4: Power Connections and AC Voltage Selection Switch Description
Connector
Description
AC Voltage Selection
Toggles the input voltage to the analyzer’s power supply
between 115 VAC and 230 VAC, determined by the country where
the analyzer is used.
Setting an incorrect voltage may damage the analyzer. When
changing the supply voltage verify that both the:
•Analyzer is powered off or not connected to power.
•AC voltage selection on the analyzer matches the AC
voltage being supplied from your power supply.
AC Power In
Connects the analyzer to the power supply
EXT. Pump Power
Provides power to an external pump when operating the
analyzer.
If you require a different power source, please contact ABB-LGR.

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Data Interface Connection Ports
This section describes the data interface connections as shown in Figure 5. These
connections may vary depending on analyzer types.
•Ethernet port – Connects the analyzer to a local area network (LAN) and allows
access to the data directory using an external computer.
•USB ports – Used for transferring data to a USB memory device, or to connect a
USB keyboard and mouse.
•Serial port (9 pin D-sub) – For real-time digital measurement output.
•DCS port (BNC male port) – Used to control the External Dynamic Dilution System
(EDDS)
•Video port (15 pin D-sub) – Connects an external monitor to the analyzer.
•MIU (25-pin data port) – For connecting the optional Multiport Inlet Unit (MIU).
Figure 5: Data Interface Connection Ports
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Plumbing Diagram
The plumbing diagram measures the internal flow of gas through the analyzers.
The external pump draws gas through the Sample Inlet port (
1/4” Swagelok)
on the back
panel of the analyzer, and the waste is exhausted through the To External Pump port (3/8”
Swagelok). The inlet gas pressure range is 0 to 5 psig.
Figure 6 shows the plumbing diagram.
Figure 6: Plumbing Diagram
If the analyzer flow is greater than 200sccm, it must be restricted with an orifice, which is
connected in between the pump and the Pretreatment Box. (Figure 7) The provided 450um
orifice will throttle the analyzer flow to less than 180 sccm. This is primarily used to switch
between the External Dynamic Dilution System (EDDS) and Batch Mode Operation.
Refer to Appendix E: on page 94 for External Dynamic Dilution System (EDDS) details.
Refer to Appendix F: on page 99 for Batch Mode Operation.
Figure 7: Orifice for decreasing analyzer flow

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Inlet/Outlet Connections
The inlet and outlet ports are located on the back panel of the analyzer. (Figure 3) These
ports are shown in detail in Figure 8.
The unit ships with inlets and outlets capped for protection. The connections use
Swagelok fittings ISO thread size 1/4” and 3/8”. (Figure 8)
Figure 8: Inlet/Outlets
Exhaust ports:
•The exhaust is located on the external pump. It can either be connected to the
provided muffler to expel exhaust into the room air, or the exhaust can be routed to
the facility ventilation system.
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Warning Labels and Descriptions
This section describes the warning labels shown on the analyzer.
•Table 5 gives a description of the warning labels.
•Figure 9 shows the location of the labels on the analyzer.
Table 5: Warning Labels and Descriptions
Label
Description
The laser is rated Class 3 (invisible laser radiation) when the
housing is open.
Only trained maintenance personnel may open the analyzer
housing.
General laser warning label.
Figure 9: Warning Label Locations

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Specifications
This section provides the weight and dimensions of the analyzer.(Figure 10)
External Dimensions
11” H x 38” W x 22” D
Weight
40 kg
Figure 10: Front Panel Dimensions