Agilent Technologies 708-DS User manual

Agilent Technologies
708-DS
Dissolution Apparatus
Operator’s Manual

708-DS Operator’s Manual
Notices
© Agilent Technologies, Inc. 2016
No part of this manual may be reproduced
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tion into a foreign language) without prior
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lent Technologies, Inc. as governed by
United States and international copyright
laws.
Manual Part Number
70-9058
Edition
Rev E, February 2016
Agilent Technologies, Inc.
3501 Stevens Creek Blvd.
Santa Clara, CA 95052 USA
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Safety Notices
CAUTION
A CAUTION notice denotes a
hazard. It calls attention to an
operating procedure, practice, or
the like that, if not correctly per-
formed or adhered to, could result
in damage to the product or loss
of important data. Do not proceed
beyond a CAUTION notice until
the indicated conditions are fully
understood and met.
WARNING
A WARNING notice denotes a
hazard. It calls attention to an
operating procedure, practice,
or the like that, if not correctly
performed or adhered to, could
result in personal injury or
death. Do not proceed beyond a
WARNING notice until the
indicated conditions are fully
understood and met.

708-DS Operator’s Manual 3
Contents
Figures 7
1Safety 11
Electrical Hazards 12
Warning 13
Caution 13
Note 13
Information Symbols 14
2 Introduction 15
Conventions Used in this Manual 17
Serial Number Format 18
3 Setting Up the 708-DS 19
Initial Setup 20
Unpacking Procedure 20
Environmental Requirements for Installation 22
Clearance 22
Equipment, Parts, and Accessories As Shipped 23
Parts and Accessories 23
Tubing / Cable Connections 24
708-DS Heater / Circulator Setup 24
Instrument Level / Water Bath Setup 25
Level Instrument 25
Bath Temperature Probe Installation 28
Handheld Probe Installation 29

4 708-DS Operator’s Manual
Contents
Power Cord Connections 29
708-DS Initial Power Up 29
Filling the Water Bath 30
Level Instrument - Re-verification 31
Heater / Circulator Power-up 31
Agilent 708-DS Setup 32
Vessel Installation 32
Sample Manifold Installation 32
Accessory Installation 36
Setting Basket (Apparatus 1) Heights 42
Setting Paddle (Apparatus 2) Heights 43
4 Operating the 708-DS 45
Main Screen - Options 46
Main Screen - Display Parameters 46
Main Screen - Sample Temperatures 47
Main Screen - Run 48
Main Screen - Stop 55
Main Screen - Drive Unit Up / Down 58
Manual Drive Unit Up / Down 58
Manual Sampling 59
Main Screen - Manifold Up / Down 60
Main Screen - Lock 61
Main Screen - Unlock 62
Main Screen - Remote Control 63
Main Screen - Alarms 64
Main Screen - Maintenance Due Icon 64
Menu Screen - System Menu 65
Menu Screen - Method Editor 66
Menu Screen - Reports 75
Menu Screen - Alarms 78
Menu Screen - Instrument 79

Contents
708-DS Operator’s Manual 5
Menu Screen - Calibration 84
Menu Screen - Diagnostics 87
Menu Screen - User Access 90
General 708-DS Conventions 91
Alphanumeric Data Entry 91
Numeric and Time / Date Entry 92
Parameter Limits / Ranges 93
Agilent 708-DS Notifications 95
Main Screen - Error Conditions 95
Dialog Screens (Green / Blue) 97
Warning Screens (Yellow) 99
Error Screens (Red) 103
5 Maintenance and Troubleshooting 107
Preventive Maintenance 108
Weekly Maintenance 108
Monthly Maintenance 108
Bi-Annual Maintenance 108
Sample Line / Paddle / Basket Care 109
Shafts 109
Baskets 110
Rinsing Sample Lines 111
Rinse Cups (Optional) 112
Vessels and Evaporation Covers 113
Water Bath and Temperature Probes 113
Water Bath Care 113
Water Bath Temperature Probe Accuracy Test 114
Removing or Adjusting Cannulas / Probes 116
Manifold Maintenance 116
Removing the Manifold 116

6 708-DS Operator’s Manual
Contents
Accessing the Top Cover 117
Removing Top Cover 117
Replacing the Top Cover 117
Printer Maintenance 118
Removing a Thermal Paper Roll 118
Inserting a Thermal Paper Roll (5095-0307) 121
Thermal Printer Test 124
Obtaining Warranty and Other Services 124

708-DS Operator’s Manual 7
Figures
Figure 1. Unpacking 20
Figure 2. Removing the Apparatus 21
Figure 3. BATH HEATER Connector 24
Figure 4. Levelers and Stability Feet 25
Figure 5. Level-Adjustment Screw Caps 26
Figure 6. Raising the Stability Feet 27
Figure 7. BATH TEMP Connector 28
Figure 8. Positioning the Temperature Probe 28
Figure 9. Filling the Water Bath 30
Figure 10. Positioning the Manifold for Installation 33
Figure 11. Connecting AutoTemp 34
Figure 12. Affixing the Fasteners 35
Figure 13. Proper Sample Tubing Position 36
Figure 14. Installing Evaporation Covers on Shafts 37
Figure 15. Shaft Locking Collars 37
Figure 16. Dosage Delivery Module and Alignment Post 38
Figure 17. Inserting DDM into DDM Alignment Shaft 39
Figure 18. Attaching DDM to Alignment Post 40
Figure 19. Accessory Installation 41
Figure 20. Tightening the Shaft Locking Collar 42
Figure 21. Inserting Height Spheres 43
Figure 22. Main Screen - Display Parameters 46
Figure 23. Sample Temperatures 47
Figure 24. Select Start Type 48
Figure 25. Select Method 49
Figure 26. Start Options 50
Figure 27. Manual Operation 52
Figure 28. Data Entry 53
Figure 29. Main Screen - Stop 55

8 708-DS Operator’s Manual
Figures
Figure 30. Pause Method 55
Figure 31. Method Paused 56
Figure 32. Pause Duration Alarm 57
Figure 33. Manual Lift Knob 58
Figure 34. Taking a Manual Sample 59
Figure 35. Agilent 708-DS Standard Evaporation Cover 60
Figure 36. Lock the Instrument 61
Figure 37. Unlock the Instrument 62
Figure 38. Remote Control 63
Figure 39. Alarm Time Expired 64
Figure 40. System Menu 65
Figure 41. Method Editor 66
Figure 42. Method Properties Screen 1 67
Figure 43. Method Properties Screen 2 68
Figure 44. Method Properties Screen 3 70
Figure 45. Method Properties Screen 4 72
Figure 46. Timepoint Properties 72
Figure 47. Are You Sure? 74
Figure 48. Reports 75
Figure 49. Select Method to Print 76
Figure 50. Reports 77
Figure 51. Alarms 78
Figure 52. Menu Screen - Instrument Settings Screen 1 79
Figure 53. Menu Screen - Instrument Settings Screen 2 81
Figure 54. Menu Screen - Instrument Settings Screen 3 82
Figure 55. Menu Screen - Instrument Settings Screen 4 83
Figure 56. Paddles/Baskets Sampling Depth 84
Figure 57. Regulatory Calibration Date 86
Figure 58. Diagnostics Screen 1 87
Figure 59. Menu Screen - Diagnostics Screen 2 89
Figure 60. User Level Settings 90
Figure 61. Data Entry 91
Figure 62. Time / Date Entry 92

708-DS Operator’s Manual 9
Figures
Figure 63. Main Screen with Red Error Conditions 95
Figure 64. Rinse Cup 112
Figure 65. Resistance Value of Temperature Probe 115
Figure 66. Near-empty Paper Roll 118
Figure 67. Accessing the Printer Handle 119
Figure 68. Open Printer Chamber 119
Figure 69. Removing the Thermal Paper Roll 120
Figure 70. Inserting a Thermal New Paper Roll 121
Figure 71. Leading Paper and Closing the Lid 122
Figure 72. Closing the Printer Chamber 122
Figure 73. Feeding Paper 123
Figure 74. Printer Test 124

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Figures
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