Parker FTIR3 User manual

FTIR3 OIL ANALYZER
User Guide
MA-K31014-KW FTIR Issue 1.indd 1 14/03/2017 20:16

MA-K31014-KW FTIR Issue 1.indd 2 14/03/2017 20:16

FTIR3 Oil Analyzer
1
FTIR3 Oil Analyzer MA-K31014-KW
FTIR3
Oil Analyzer
MA-K31014-KW FTIR Issue 1.indd 1 14/03/2017 20:16

FTIR3 Oil Analyzer
2
Contents
1 Introduction 4
1.1 About the FTIR3 Oil Analyzer 4
1.1.1 FTIR3 Oil Analyzer Specications 4
1.1.2 FTIR3 Oil Analyzer Approved Methods 5
1.2 Part Numbers 5
1.2.1 FTIR3111 5
1.2.2 Spares 6
1.3 About Safety 6
1.3.1 General Safety 6
1.3.2 Electrical Safety 6
1.3.3 Laser Safety 7
1.4 Maintenance and Servicing 7
1.4.1 Maintenance 7
1.4.2 Returns and Packaging 7
1.4.3 Recalibration 7
2 Unpacking and Installation 8
2.1 Inspection 8
2.2 Unpacking 8
2.3 Installation 8
2.3.1 Site Requirements 8
2.3.2 Parts of the FTIR3 Oil Analyzer 9
2.3.3 Rear Panel LEDs 10
2.3.4 Sampling Cell 11
2.3.5 Sampling Assembly 12
2.3.6 Setting up the FTIR3 13
2.3.7 Stand-by Mode 13
3 Sample Analysis 14
3.1 Equipment Management Screen 15
3.1.1 Creating a new Equipment le 16
3.1.2 Viewing Archived Analyses 16
3.1.2 (a)“Details” Tab 17
3.1.2 (b) “Trend” Tab 20
3.1.2 (c) “Results” Tab 21
3.1.2 (d) “Spectra” Tab 21
3.2 Testing Mode 22
3.2.1 Sample Identication 23
MA-K31014-KW FTIR Issue 1.indd 2 14/03/2017 20:16

FTIR3 Oil Analyzer
3
3.2.2 Sampling Procedure 23
4 Maintenance 27
4.1 Advanced Options 27
4.1.1 Oil Types tab 27
4.1.2 Oil Parameters tab 29
4.2 Maintenance and Diagnostic Options 29
4.2.1 Spectrometer Tab 29
4.2.1 (a) Acquire New Background 29
4.2.1 (b) Acquire Spectrum 29
4.2.2 User Accounts 30
4.3 Sampling Cell 30
4.4 Desiccant 30
4.5 Software Updates 31
4.6 Laptop Computer 31
4.7 Troubleshooting 32
` 4.7.1 FTIR3 Helper 32
MA-K31014-KW FTIR Issue 1.indd 3 14/03/2017 20:16

FTIR3 Oil Analyzer
4
1 Introduction
1.1 About the FTIR3 Oil Analyzer
The FTIR3 Oil Analyzer is a portable, user-friendly diagnostic instrument intended for lubricant con-
dition monitoring in the eld or in the lab. It is designed for durability, reliability, and ease of use. This
manual is organised to aid set-up and operation of the FTIR3 Oil Analyzer and the FTIR3 software.
The FTIR3 Oil Analyzer comprises two main components:
• FTIR spectrometer & Sampling System
• Portable computer (Windows operating system)
The FTIR3 Oil Analyzer is congured to ASTM D7418 Standard Practice and the FTIR3 software
comes pre-loaded with the complete range of JOAP and ASTM approved methods (see Section 1.1.2)
used for the condition monitoring of in-service lubricants.
1.1.1FTIR3OilAnalyzerSpecications
Spectral range 5000 - 450 cm-1
Resolution 2 cm-1
Interferometer Permanently adjusted
Beam diameter 25 mm
Beam splitter ZnSe
Cell window ZnSe
Scanner Mechanical frictionless bearing
Frequency reference system VCSEL laser, 850 nm
IR Source Ceramic, air cooled, 12 V, 20 W
IR Detector Room temperature Deuterated triglycine sulphate
Data acquisition 24 bit ADC
Dimensions 22 x 33 x 12 cm
Weight 7 kg
Power consumption 24 VDC, max 48 W
Temperature environment 18°C to 35°C
Humidity environment Below 80%, non-condensing
MA-K31014-KW FTIR Issue 1.indd 4 14/03/2017 20:16

FTIR3 Oil Analyzer
5
1.1.2FTIR3OilAnalyzerApprovedMethods
The results produced by the FTIR3 Oil Analyzer conform to the following internationally-approved
methods and practices:
1.2 Part Numbers
The FTIR3 Oil Analyzer is supplied as shown in Section 1.2.1. Spares are available as shown in
Section 1.2.2.
1.2.1 FTIR3111
ASTM E 2412-10 Condition Monitoring of In-Service Lubricants by Trend Analysis Using Fourier
Transform Infrared (FTIR) Spectrometry
ASTM D 7412-09 Trend Analysis of Phosphate Antiwear Additives by FTIR Spectrometry
ASTM D 7414-09 Trend Analysis of Oxidation by FTIR Spectrometry
ASTM D 7415-09 Trend Analysis of Sulphate By-Products by FTIR Spectrometry
ASTM D 7624-10 Trend Analysis of Nitration by FTIR Spectrometry
Description Notes
FTIR3 spectrometer
FTIR3 Cleaning uid 2 x 500 ml bottle
FTIR3 laptop Pre-installed software and drivers
FTIR3 PSU With regional mains cable
Laptop PSU With regional mains cable
Ethernet cable For connection between FTIR3 and laptop. 1 m
FTIR3 user manual
Pouring caps 2 x for dispensing cleaning uid into a beaker
Waste container 500 ml bottle
Manual lling accessories Luer taper ttings, cones and tubing
5 ml syringe Pack of 100 for oil sample delivery
20 ml syringe Pack of 4 for cleaning uid delivery
60 ml syringe Pack of 2 for air purge
Shipping carton Retain all original packaging
MA-K31014-KW FTIR Issue 1.indd 5 14/03/2017 20:16

FTIR3 Oil Analyzer
6
1.2.2Spares
In addition to the above, FTIR3 Oil Analyzer spares may be ordered using the following part numbers:
1.3 AboutSafety
1.3.1 GeneralSafety
The FTIR3 Oil Analyzer has been designed to comply with a wide variety of international standards governing
the safety of laboratory equipment. Under normal circumstances, the FTIR3 Oil Analyzer poses virtually no risk
to the user. Following these simple precautions will help ensure the continued safe operation of the instrument:
DO make sure that FTIR3 Oil Analyzer instrument is properly connected to the electrical supply; in particular
make sure that the ground (earth) is securely connected.
DO maintain the FTIR3 Oil Analyzer instrument in a dry location. Avoid spilling liquids into or on the instrument.
Clean all spills immediately. If anything spilled enters the instrument, switch o the power and call a service
engineer.
DO NOT open the instrument underside covers. THERE ARE NO USER SERVICEABLE PARTS INSIDE.
Opening these covers of the instrument poses electrical hazards and will void all manufacturer warranties.
DO NOT use ammable gas near the FTIR3 Oil Analyzer. The instrument contains a hot infrared source,
which could cause re or explosion.
DO NOT make any adjustments, maintenance or repairs to the FTIR3. Repairs should only be carried out by
qualied service engineers.
IF DAMAGE IS SUSPECTED, disconnect the power otherwise the instrument may become unsafe. Some
potential indicators:
• The FTIR3 shows visible damage;
• It fails to perform the intended measurement;
• It has been subjected to prolonged storage in ambient conditions that exceed the use and operating
parameters;
• It has been subjected to severe transport stresses
1.3.2 ElectricalSafety
The FTIR3 Oil Analyzer instrument has been designed and tested in accordance with the safety requirements
of the International Electrotechnical Commission (IEC). The instrument conforms to IEC publication 61010.1 as
it applies to IEC Class 1 (earthed) appliances. The FTIR3 Oil Analyzer instrument is rated:
•IEC Installation Category II - Suitable for connection to local level power supplies.
•IEC Pollution Degree 2 - Usually only non-conductive atmospheric pollution of the equipment occurs,
however, a temporary conductivity caused by condensation must be expected.
Connect the FTIR3 Oil Analyzer instrument to a power supply line that includes a switch or other adequate
means of disconnection from the electrical supply. Only connect the instrument into a properly- grounded
electrical outlet. If a fuse must be replaced, ensure that the replacement is the proper type and proper current
rating.
Parker Part Number Description Notes
ACCK05001 Sampling cell
ACCK05002 Manual lling accessories
ACCK05003 Cleaning uid & syringes 2 x 500 ml bottles and pack of 100 syringes
MA-K31014-KW FTIR Issue 1.indd 6 14/03/2017 20:16

FTIR3 Oil Analyzer
7
1.3.3 LaserSafety
The FTIR3 instrument complies with the following laser safety regulations:
• British Standard BS EN 60825 (1992) – “Radiation safety of laser products, equipment classication,
requirements and user’s guide”. BS EN 60825 implements CENELEC European Normalization document EN
60825 (CENELEC is the European Committee for Electrotechnical Standardization).
•IEC Publication 825 (1984) – “Radiation safety of laser products, equipment classication, requirements
and user’s guide” and “amendment 1 to Publication 825 (1990).
The FTIR3 Oil Analyzer instrument contains a CDRH Class I (BS EN 60825 and IEC 825 Class 1) VCSEL or
diode laser module, which emits red visible, continuous wave radiation and has a maximum output power of
less than 1 mW.
1.4 MaintenanceandServicing
1.4.1 Maintenance
Regular cleaning of the Sampling Cell is recommended using the Cleaning Fluid & Syringe kit ACCK05003. Do
not attempt to dismantle the Sampling Cell or any other part of the FTIR3 Oil Analyzer. The warranty will be void
if the cell or instrument show signs of tampering. For calibration, maintenance and repair needs, contact Parker
Kittiwake.
For continued best performance, Parker Kittiwake recommends that the FTIR3 Oil Analyzer is maintained in a
clean condition. In particular, the following points should be noted:
1. Care should be taken to avoid spills in the sample compartment – if this should occur, quickly mop up the spill
with absorbent cloth or similar. Avoid the use of harsh cleaning chemicals, a mild detergent and a damp cloth
should be sucient to remove any nal oil residues.
2. To prevent leakage from the sample cell, the integrity of the tube ttings should be checked before rst use
outside of the sample compartment and periodically as a further precaution.
3. Do not touch or otherwise contaminate the two IR windows located on the internal sidewalls of the sample
compartment. If these become dirty, the signal level will degrade causing a reduction in the quality of the spectra
recorded by the spectrometer. If gross contamination is suspected, contact Parker Kittiwake for advice.
4. Care should be taken to prevent contamination of the external faces of the sample cell windows. If this does
occur, it may be possible to clean the windows by rinsing with a suitable solvent. This procedure should only be
undertaken by a competent person, contact Parker Kittiwake for advice if unsure of how to proceed.
5. Similarly, and as noted above, the sample cell should be kept free of internal contamination by regularly ushing
with the cleaning uid between, and following, measurements on dirty oils.
6. A nal ush through of the sample cell with air, using the largest syringe supplied, is also recommended to
remove the bulk of the cleaning uid at the end of any measurement series and particularly before storing the
cell for an extended downtime period.
7. The spectrometer exterior should be cleaned with mild detergent and a damp cloth only.
1.4.2 ReturnsandPackaging
Return instrument to Parker Kittiwake for all servicing and repair. Please retain all original instrument packaging for
return shipping. All uids must be removed from the equipment and the FTIR3 Oil Analyzer cleaned appropriately
before return. Parker Kittiwake will not be liable for damage to returned goods resulting from inadequate packaging.
1.4.3 Recalibration
The FTIR3 Oil Analyzer does not require periodic recalibration. The spectrometer performs a series of self-tests
on start-up and at predened intervals – warnings will be given should any of these tests fail. Consult
Parker Kittiwake if this should occur.
MA-K31014-KW FTIR Issue 1.indd 7 14/03/2017 20:16

FTIR3 Oil Analyzer
8
2 Unpacking and Installation
2.1 Inspection
As soon as the shipment arrives:
• Carefully check the exterior of the shipping container(s) for any external damage. Unusual marks on
the container(s) may indicate exposure to water etc.
• If the shipping container(s) appear to be damaged (water damage, crushed package, etc.) contact
the supplier and carrier immediately.
CAUTION!
Do not open the shipping containers at this time.
• Do not accept packages with obvious puncture damage. All other damage should be noted on the
shipping document and signed by the delivery agent.
• Check sales invoice against bill of lading and the identifying labels on the containers. Notify supplier
and shipping agent of any apparent discrepancies.
• If satised that all boxes have been delivered and appear to be undamaged, place them where their
contents can come to the recommended room temperature.
CAUTION!
Do not open any packages until the equipment inside has reached room temperature.
This is to prevent condensation from forming and damaging the optics and mirrors.
2.2 Unpacking
a) Move the box to the location where the instrument will be used.
b) Carefully unpack the instrument from the shipping container(s). (Save the packing material for use if
the instrument needs to be returned to supplier for service).
c) Visually inspect all equipment.
d) Remove any secondary fasteners, shipping tape, plastic wraps, etc.
e) Notify supplier of any problems, such as obviously broken equipment, missing components, etc.
2.3 Installation
2.3.1SiteRequirements
The FTIR3 Oil Analyzer should be placed on a rm and vibration-free table with easy access.
The conditions below are required for proper operation of the FTIR3 Oil Analyzer.
• Power supplies must be properly grounded in accordance with local regulations.
• Ambient air should be free from corrosive and/or ammable fumes
• Operating temperature range: 18°C to 38°C
• Maximum temperature gradient: 1°C / hour
• Relative humidity: 80% max, non-condensing
Do not install devices such as large electric motors, heaters, welding equipment, radio transmitting
equipment, NMR instruments or high-powered lasers in close vicinity to the spectrometer. These
devices can cause a spectrometer malfunction.
MA-K31014-KW FTIR Issue 1.indd 8 14/03/2017 20:16

FTIR3 Oil Analyzer
9
2.3.2PartsoftheFTIR3OilAnalyzer
Figure 2-1
1 Main body
2 Status LED
3 Sampling compartment lid (open)
4Sampling cell
4
3
2
1
MA-K31014-KW FTIR Issue 1.indd 9 14/03/2017 20:16

FTIR3 Oil Analyzer
10
AUSB port (unused)
BEthernet port to connect between spectrometer and computer
CStatus LED TKD – see section 2.3.3
DStatus LED ACC – see section 2.3.3
EStatus LED DIR/ERR – see section 2.3.3
F“Ext Accessory” port (unused)
GTAP – Test Access Port, diagnostic use only
HCFG dip switch. Switches 1,3 and 4 must be in the DOWN position, switch 2 must be in
the UP position
IStand-by button – see section 2.3.7
JPower jack and retaining clip. Use the supplied power cord with mains adaptor
KKensington security slot – for optional anti-theft lock (not supplied)
2.3.3RearPanelLEDs
TKD (TaKe Data) • Green: the interferometer mirror is within data acquisition range
• During data acquisition the light intensity changes to bright green
ACC (ACCess) • Yellow: the Ethernet connection is communicating with the optics
• During data transfer the LED will be bright yellow
DIR/ERR (DIRection/ERRor) • Flashing red: normal operation, the interferometer is scanning
• Permanent red: Interferometer fault
Figure 2-2
MA-K31014-KW FTIR Issue 1.indd 10 14/03/2017 20:16

FTIR3 Oil Analyzer
11
2.3.4SamplingCell
Important: The sampling cell must be kept clean for consistent results. Follow all instructions
for ushing with cleaning uid and visually inspect regularly to check whether extra cleaning is
required.
Figure 2-3
During factory calibration, each sampling cell is paired with its FTIR3 Oil Analyzer unit to ensure
that the exact optical pathlength is included in the analytical calculations. For this reason, it is not
recommended to use dierent sampling cells or interchange between units.
Do not dismantle the sampling cell without rst consulting your Service Engineer. This will alter
the optical pathlength and may invalidate future analysis.
The sampling cell has been designed to be robust and as such, breakage of the Zinc Selenide (ZnSe)
windows during ordinary usage is not expected. However, in the event of a breakage, contain all
fragments and contact your Service Engineer. Note: Zinc Selenide fragments are harmful when ingested.
1 Sampling cell
2Inlet Port
3 Outlet Port
4 Blanking Plug
Figure 2-2
MA-K31014-KW FTIR Issue 1.indd 11 14/03/2017 20:16

FTIR3 Oil Analyzer
12
2.3.5SamplingAssembly
To prepare the sampling assembly for use:
1. Cut an appropriate length of tubing to connect between the FTIR3 Oil Analyzer and the waste
receptacle.
2. Insert in/out tting nut and yellow ferrule. This is the OUT tubing as shown in Figure 2-4.
Figure 2-4
3. Cut a 5 cm length of tubing and repeat the previous step for both ends. Screw the Luer tting on to
one end. This is the IN tubing as shown in Figure 2-5.
Figure 2-5
4. Fit onto sampling cell as shown in Figure 2-6. Close the remaining port with the blanking plug as
shown. Screw in the ttings such that they are hand-tight. The IN and OUT ttings may be swapped
if desired, but this setup reects best practise in minimising the introduction of air bubbles during
sampling.
Figure 2-6
MA-K31014-KW FTIR Issue 1.indd 12 14/03/2017 20:16

FTIR3 Oil Analyzer
13
2.3.6SettinguptheFTIR3
A dedicated portable computer is provided with the FTIR3 Oil Analyzer with FTIR3 software installed
and congured.
1. Connect the power supply of the FTIR3 Oil Analyzer to the corresponding connector (J) on the rear
of the instrument (see Figure 2-2).
2. Connect the Ethernet cable to the corresponding connector on the rear of the instrument and to the
USB Ethernet adaptor provided, then plug into the computer.
3. Turn on the computer if it is not already on.
4. Ensure that the FTIR3 Oil Analyzer sample compartment is empty (i.e. the sampling cell assembly
is removed).
5. Launch the FTIR3 software (refer to Section 3 for complete software instructions).
6. Upon starting for the rst time or after a power cycle, the FTIR3 Oil Analyzer will automatically run
diagnostic self-tests. These may take up to ten minutes.
The status indicator LED light on the top of the FTIR3 Oil Analyzer unit will illuminate.
• A green light indicates the unit is functioning and communicating properly.
• A red light indicates the unit requires a self-test, or may not be communicating.
2.3.7Stand-byMode
The spectrometer can be set into stand-by mode by pressing the SBY/RES button (I) located next to
the power input. Hold the button pressed for up to two seconds. The spectrometer will beep and the
status LED on top of the unit will ash green
To deactivate stand-by mode, hold the SBY/RES button for up to two seconds again. The spectrometer
will beep and the status LED on top of the unit will turn yellow to indicate that the interferometer is
waking up. After about 10 minutes, the status LED will turn green, indicating that the unit is ready for
use again.
During stand-by mode, the IR source, laser and detector are switched o to reduce power consumption.
The spectrometer is not switched o entirely in this mode and will still draw power.
MA-K31014-KW FTIR Issue 1.indd 13 14/03/2017 20:16

FTIR3 Oil Analyzer
14
3 Sample Analysis
Launch the FTIR3 software by clicking the shortcut on the desktop.
User Name: admin Default Password: admin
Note: the User name and password are case-sensitive.
The software opens to the Main Options screen (Figure 3-1). From here, the user is able to check the
status of the instrument connection (top status bar), dene or select the equipment and samples to be
tested, or run a new analysis.
Figure 3-1
The top status bar will display a green icon when the spectrometer and the computer are communicating
properly. If the icon is red, then verify the connections to the FTIR3 Oil Analyzer by disconnecting and
reconnecting the Ethernet cable.
If this does not work:
1. Ensure the sample compartment is empty.
2. Restart the software.
3. Disconnect the Ethernet cable, reboot the computer and the spectrometer, and then reconnect the
Ethernet cable. If the problem persists, please contact your Service Engineer.
Close any pop-up windows in the lower right corner (Figure 3-2). From power-up, the unit will require a
few minutes to perform self-tests and for the infra-red source to reach a stable operating temperature.
Figure 3-2
MA-K31014-KW FTIR Issue 1.indd 14 14/03/2017 20:16

FTIR3 Oil Analyzer
15
Before a new sample is run, the user must rst dene an equipment prole for the sample, by clicking
the icon. This will open the “View Equipment and Results” window and allow the user to enter
information on the equipment, type of oil, analysis to be done, and other parameters (see Section 3.1:
Equipment Management Screen for further information).
To run a sample from a piece of equipment that already exists in the database, click the icon to open
the existing prole and add information for the new sample.
The user can then click the “View the Equipment and Results” icon after a sample has been analysed.
To exit the program, click the button in the lower right-hand corner, and then click to conrm.
3.1 EquipmentManagementScreen
Clicking the icon from the main screen will open the Equipment Management screen (Figure 3-3),
where the user can select an existing Equipment Prole, or create a new one.
Figure 3-3
Selecting a saved piece of equipment from the list on the left hand side of the screen will display all
the information relating to that item. The user can then view results of any archived analyses, add new
equipment, or edit equipment information. This window also displays the graphic and numeric results
of the analysis.
Click on the button to add a new equipment prole to the list.
To delete an equipment prole, select it from the list and click the button.
Click on the icon to export a set of results or spectra, or on the icon to import.
MA-K31014-KW FTIR Issue 1.indd 15 14/03/2017 20:16

FTIR3 Oil Analyzer
16
3.1.1CreatinganewEquipmentle
1.Click the icon to open the Equipment Details dialog (Figure 3-4).
Figure 3-4
2. In the “Name” eld, enter a name to identify the new equipment, such as “Compressor #3”.
3. Enter any pertinent Comments. (This eld may be left empty if desired.)
4. Select the Oil Type (Engine Oil, Gear Oil or Transmission Oil) from the drop-down menu.
5. Enter the Oil Name (brand, grade, etc).
6. Enter the Interval Units that will be used in for trending (hours, km, etc.).
7. Once all the information is entered, click the “Add” icon to save the new equipment, or click the
“X” icon to exit the dialog without saving the changes.
3.1.2ViewingArchivedAnalyses
The user can view the results of previous analyses (Figure 3-5).
Figure 3-5
MA-K31014-KW FTIR Issue 1.indd 16 14/03/2017 20:16

FTIR3 Oil Analyzer
17
Select an equipment prole from the list in the left pane. The “Filter” eld can be used to easily sort through
a long list of equipment names. The information pertaining to the selected Equipment is displayed in the
right-hand pane, divided into four tabs.
At any time, click on the “Back” arrow to return to the Main Options screen.
Analysis results for individual interval points can be viewed by clicking on the Equipment name in the
left-hand pane and selecting the desired interval point (Figure 3-6). If there is any warning or alert in any
of the sample analyses, it will be highlighted in the left-hand pane. Refer to sections 3.1.2 (c) and 3.1.2
(d) for further information.
Figure 3-6
3.1.2(a)“Details”Tab
The Details tab (Figure 3-7) displays the Equipment information that was entered in Section 3.1.1,
as well as the quantitative and spectral results of the Last Sample to be analysed and any applicable
Messages and Warnings. The icons in the upper portion of the screen allow the user to access various
functions:
Figure 3-7
MA-K31014-KW FTIR Issue 1.indd 17 14/03/2017 20:16

FTIR3 Oil Analyzer
18
Set Reference Point: Select a reference result from the list, as shown in Figure 3-8.
Figure 3-8
View Analysis Information: Opens a pop-up window that displays the results of analysis
(Figure 3-9). Click the check mark icon in the lower right corner to exit.
Figure 3-9
Update Oil Type / Re-trend Data: This screen (Figure 3-10) allows the user to set a new oil
type, and to re-trend the data collected with the parameters set in the new oil type. Refer to
Section 4.1.1 for information on Oil Types.
Figure 3-10
MA-K31014-KW FTIR Issue 1.indd 18 14/03/2017 20:16