Shimadzu ICPE-9000 User manual

Read the instruction manual thoroughly before you use the product.
Keep this instruction manual for future reference.
Shimadzu Multitype ICP Emission Spectrometer
ICPE-9000 Hardware
INSTRUCTION MANUAL
305-34043C

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Before Use
Introduction
Read this manual thoroughly before using the product.
Thank you for purchasing this product.
This manual describes the installation and operation procedures for the product and provides precautionary
information and details on accessories and options. Read this manual thoroughly before using the product.
Use the product in accordance with the instructions given here. Keep this manual for future reference.
IMPORTANT • Familiarize yourself with the contents of this manual before using the product.
• If this product is borrowed or changes ownership, provide this manual to the next user.
• If this manual or the warning labels on the product are lost or damaged, promptly contact
your Shimadzu representative.
• To ensure safe operation, be sure to read "Safety Precautions" before using the product.
• Installation is performed by Shimadzu-designated service engineers. To ensure safety, do
not perform installation yourself or allow anybody other than a Shimadzu-designated
service engineer to perform installation.
COPYRIGHT This publication may not be reproduced in whole or in part without written permission
from Shimadzu Corporation. Since Shimadzu products are frequently upgraded and
improved, information in this publication is subject to change without notice. We
appreciate notification of any errors or omissions.
Copyright © 2005 Shimadzu Corporation. All rights reserved.

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Warranty and After-Sales Service
Warranty 1. Warranty Period
Contact your Shimadzu representative.
2. Scope
If a fault that can be attributed to Shimadzu occurs during the warranty period,
Shimadzu will repair the product or provide the necessary replacement parts free of
charge.
3. Limitations
This warranty does not cover faults that can be associated with any of the following:
1) misuse;
2) repairs or modifications made by any company other than Shimadzu or a
Shimadzu-designated company;
3) external factors;
4) operation in severe conditions, such as environments subject to high temperatures,
high humidity levels, corrosive gases, or vibrations;
5) conditions beyond Shimadzu's control, including fires, earthquakes and other forces
of nature, contamination by radioactive or toxic substances, wars, riots, and criminal
activity;
6) moving or transporting the product after its initial installation;
7) items or parts that can be regarded as consumable (e.g., parts for which the service
life depends on the operation conditions, such as LCDs and program tape);
8) use in combination with hardware or software not designated by Shimadzu;
9) faults in equipment or damage to software, including the OS, or data caused by
computer viruses;
10) faults in equipment or damage to software, including the OS, or data caused by power
failures, including blackouts and momentary voltage drops;
11) faults in equipment or damage to software, including the OS, or data caused by
turning OFF the power to equipment without performing the proper shutdown
procedures.
After-Sales Service
If this product does not operate correctly, inspect it and take the appropriate corrective
action as described in this manual. If the problem persists, or it is not covered in this
manual, contact your Shimadzu representative.

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Replacement Parts Availability
Replacement parts will be available for this product for a period of seven (7) years after
its discontinuation. Thereafter, replacement parts may cease to be available. Note,
however, that the availability of parts not manufactured by Shimadzu shall be
determined by the relevant manufacturers.

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Safety Precautions
• To ensure safe operation, read these safety precautions thoroughly before using the product.
• Be sure to observe all the safety precautions given here. They are extremely important for ensuring safety.
• In this manual, precautionary information is indicated using the following conventions.
WARNING
Indicates a potentially hazardous situation which, if not
avoided, could result in death or serious injury.
CAUTION
Indicates a potentially hazardous situation which, if not
avoided, may result in minor or moderate injury, or
equipment damage.
NOTE
Indicates information provided to improve efficiency or
clarify explanations.

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Safety Precautions Related to Installation Location
WARNING
•Some of the solvents used for measurement are flammable or toxic. Be sure to
ventilate the room properly.
Not doing so may result in poisoning or fire.
•Organic solvents are sometimes used for measurement. Therefore, do NOT use
open flames near the product and do NOT install the product in the same room as
equipment that generates sparks.
Doing so may result in fire.
As a safety measure, provide a fire extinguisher.
•A sink is required near the product
If solvent gets into your eyes or you come in contact with toxic solvent, you must wash away the solvent
immediately. Provide a sink as near the product as possible.
CAUTION
•Consider the weight of the entire measurement system when installing the product.
Install the product on a surface (e.g., a table) that is flat, stable, and easily capable of withstanding the
weight of the entire measurement system. Otherwise, the equipment may fall or topple over.
•Do NOT install the product in locations subject to large amounts of dirt, dust,
corrosive gases, or gases containing halides.
Otherwise, performance specifications may not be attained or the service life of the equipment may be
reduced.

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Safety Precautions Related to Installation Work
WARNING
•Take steps to ensure that the equipment does not fall over due, for example, to
earthquakes.
Otherwise, vibrations may cause the equipment to fall over and cause injury.
•The power supply voltage and power consumption for the product are given below.
The power supply voltage is displayed on the label and voltage selector on the back
of the product. Connect to a power supply that complies with this voltage.
Connecting to a noncompliant power supply may result in fire or electric shock. If the power supply
voltage is unstable or if the power supply capacity is insufficient, performance specifications may not be
attained. Provide a power supply that complies with the power supply capacity required by the entire
system.
•Ground the product.
If the product is not grounded, electric shock may occur when there is faulty operation or current
leakage. This is also important for ensuring stable operation.
•Do NOT insert the adapter's ground wire into, or allow it to make contact with, the
power outlet.
Doing so may cause fire or electric shock.
•Do NOT place heavy objects on, or thermal appliances near, the power cord.
Otherwise, the cord may break and cause fire, electric shock, or faulty operation. If the cord is damaged,
promptly contact your Shimadzu representative.
•Do NOT modify or stretch the power cord, or bend it excessively.
Otherwise, the cord may break and cause fire or electric shock. If the cord is damaged, promptly contact
your Shimadzu representative.

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CAUTION
•Be careful not to trap your fingers in gaps in the equipment during installation.
Otherwise, your fingers may be injured.
•Be careful not to trap your fingers when opening and closing doors.
Otherwise, your fingers may be injured.
Safety Precautions Related to Installation Work
WARNING
•Be sure to take measures for preventing accidents due to static electricity.
Otherwise, the sample may catch fire and cause a serious accident involving fire or explosions.
•Wear protective glasses and gloves when handling solvents and samples.
If solvent gets into your eyes, your eyesight may be damaged.
If solvent does get into your eyes, wash away the solvent immediately, and seek treatment by a medical
professional.
•Wear protective gloves when handling samples that are toxic or that may spread
biological contagion.
•Do NOT use flammable sprays (e.g., hair sprays or insecticide sprays) near the
product.
Otherwise, the spray may ignite and cause a fire.

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Safety Precautions Related to Repairs and Maintenance
WARNING
•Remove the power plug from the outlet before performing inspections or repairs or
replacing parts.
Not doing so may result in an accident due to an electric shock or short circuit.
•Do NOT remove the main unit's cover under any circumstances.
Doing so may result in injury or faulty operation.
It is not necessary to remove the main unit's cover for standard repairs and maintenance. Contact your
Shimadzu representative to request repairs requiring the removal of the main unit's cover.
•Replace fuses only with those of the type specified in this instruction manual.
Using a different type of fuse may result or fire.
Contact your Shimadzu representative to inquire about fuses not specified in this instruction manual.
•If dust adheres to the power plug's pins or pin-side face, remove the power plug and
wipe it clean with a dry cloth.
Supplying power with dust on the power plug may result in fire.
•Replace parts only with those specified in this instruction manual.
Using other parts may result in damage to those parts and make it impossible to use the product.
•Do NOT leave the product in a wet state and do NOT clean it using alcohol- or
thinner-based solvents.
Doing so may result in rust or discoloration.
•Dispose of waste in accordance with your country's laws and regulations.

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Warning Labels
In order to ensure safety, warning labels are attached in places requiring caution. If a warning label is lost or
damaged, obtain a new label through your Shimadzu representative and attach it in the correct position. See
"Warning Labels on the Equipment" in this instruction manual for details on the positions where the labels
are attached. (See page ⅹⅱ)
Warning Label Positions
The warning labels shown below are attached to the equipment.
(1) Bottom Left of Outer Casing
037-72017-10 LABEL, WARN, SA50-017P (Japanese)
037-72020-10 LABEL, WARN, SA50-020P (English)
(2) Cylindrical Funnel
037-72522-02 LABEL, WARN, SB60-522P (Japanese)
037-72525-01 LABEL, WARN, SB60-525P (English)

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(3) Plasma Stand Door
037-72122-00 LABEL, WARN, SA40-122P (Japanese)
037-72125-00 LABEL, WARN, SA40-125P (English)

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1
3
2
Warning Labels

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Action for Environment
To all user of Shimadzu equipment in the European Union:
Equipment marked with this symbol indicates that it was sold on or after 13th August 2005,
which means it should not be disposed of with general household waste. Note that our equipment
is for industrial/professional use only.
WEEE Mark
Contact Shimadzu service representative when the equipment has reached the end of its
life. They will advise you regarding the equipment take-back.
With your co-operation we are aiming to reduce contamination from waste electronic and
electrical equipment and preserve natural resource through re-use and recycling.
Do not hesitate to ask Shimadzu service representative, if you require further information.

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Handling Precautions
Thank you for purchasing the Shimadzu ICPE-9000 multitype ICP emission spectrometer.
Read the following items before using the product.
1. Handling High-Pressure Gas
This product uses argon gas. Read the section entitled "Handling High-Pressure Gas".
2. Use of Radio Frequency
(1) As previously communicated, this product uses a radio frequency (27.120 MHz). In accordance
with the Japan's Radio Law, it is necessary to apply for permission to use radio frequencies.
Check that the appropriate procedures have been completed. Contact your Shimadzu
representative if there are any points requiring clarification.
(2) This product emits a radio frequency that is within the range specified by the Radio Law. If you
use a pacemaker, consult a medical professional to confirm that there is no risk of an accident.
3. Analysis Samples
Exercise great care when handling toxic samples.
4. Waste Processing
With this product, most samples generate waste that requires processing. Be sure to process the waste
properly.
5. Ventilation
This product uses argon gas and so, if the installation location is poorly ventilated, the ambient
environment may become oxygen deficient. Ensure that the installation location is properly
ventilated.
6. Chemical Resistance
Due to the nature of the coating and the resin materials used in the outer casing of this product,
contact with certain chemicals may cause deterioration of the casing. If chemicals adhere to the casing,
promptly remove them.
7. Installation Location and Work Environment
Do not use this product in environments subject to potential hazards, such as corrosive gases.
8. Moving and Disposing of the Product
Contact your Shimadzu service representative before moving or disposing of this product.
9. Handling
Explanations on the methods used to operate and handle this product are covered in the following
manuals.
(1) Hardware, English: 305-34043, INSTRUCTION MANUAL, ICPE-9000H/W, E
(2) Software, English: 305-34045, INSTRUCTION MANUAL, ICPE-9000S/W, E

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10. You may not reproduce all or any part of the contents of this manual without consent.
11. The contents of this manual are subject to change without prior notice.
12. Contact your Shimadzu representative if you find any errors in this manual.
13. Shimadzu accepts no responsibility for any events that result from the use of this product.

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Handling High-Pressure Gas
Thank you for your continuing support of Shimadzu Corporation products.
Many of our products require the use of high-pressure gas. We trust you are already aware of the increasing
demand for more stringent levels of safety management with regard to these gases. Although we trust you are
already implementing the items listed below, we ask that you review these items and exercise the utmost care
in the handling of high-pressure gases.
Note the following points regarding the handling of high-pressure gases in Japan:
1)By law, permission is required to use cylinders containing more than 300 m3.
2)When using gas of a pressure that exceeds 980.665 kPa (10 kg/cm2) inside the equipment at room
temperature, the equipment is regarded as high-pressure gas equipment and, by law, notification of use
must be submitted.
We ask that you refer to your government laws and regulations related to high pressure gas control , liquefied
petroleum gas control, general high pressure gas control , and fire defense.
Handling Precautions
1. Install the gas cylinder in a well-ventilated outdoor location that is not exposed to direct sunlight and
convey the gas indoors via a pipe. Regarding liquefied gases in particular, this setup is required by law in
Japan.
2. Ensure that the temperature of the gas cylinder never exceeds 40°C. Also, ensure that there are no open
flames within 2 m of the gas cylinder.
3. Ensure that the location where high-pressure gas is used is well ventilated and, as part of initial
inspection, check for gas leaks with soapy water.
4. Prevent the cylinder from falling or toppling over by securing it with rope. Be sure not to let liquefied-gas
cylinders (e.g., acetylene, propane, or nitrous oxide) topple over into a horizontal position.
5. Be sure to use oil-free decompression valves with oxygen gas cylinders. Also, do not use pipes in which
oil adheres to the internal pipe surfaces that oxygen gas comes in contact with.
6. After using the gas, close the cylinder's main valve immediately.
7. Inspect the functional capability of the pressure gauge at least once every three months.
8. Do not use the cylinder until it is empty. Otherwise, the inside of the cylinder will be contaminated.

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