Thermo Electron HAAKE Phoenix II P1 User manual

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Table of Contents
1 HAAKE Phoenix II P1Version 3.07
1. Key to Symbols 4.............................
1.1 Symbols used in this manual 4..................
1.2 Symbols used on the unit (front) 4...............
1.3 Symbols used on the unit (rear) 4...............
1.4 Symbols used on the display 5..................
2. Quality Assurance 7..........................
3. Your Contacts at
Thermo Electron (Karlsruhe) GmbH 8..........
4. Thermo Electron (Karlsruhe)
Test Certificate for HAAKE Phoenix II P1 9......
5. Safety Notes 10................................
6. Unit Description 13............................
6.1 Safety features 13..............................
6.2 Safety class 3 according to DIN 12876 14.........
6.3 Applications 14................................
6.4 Temperature ranges 14.........................
7. Unpacking / Setting Up 15......................
7.1 Transportation damage? 15.....................
7.2 Contents 15...................................
7.3 Ambient conditions according to EN 61010 15.....
7.4 Resting time after transportation
(only for refrigerated circulators) 15...............
7.5 Ventilation 15..................................
7.6 Information concerning the CE sign 16............
7.7 Mounting onto baths and bath bridges 17.........
8. Functional Elements 18........................
8.1 Front Phoenix II P1 18..........................
8.2 Rear Phoenix II P1 19..........................
8.3 Bath vessel B5 (example model for B7 and B12) 20
8.4 Refrigerated bath C25P (example model C20P,
C35P, C40P, C41P, C50P and C75P) 21..........
9. Hoses 22......................................
9.1 Connecting Hoses 22...........................
9.2 Selecting Hoses 22.............................
9.2.1 Plastic and rubber hoses 23...............
9.2.2 Metal hoses 24..........................
9.3 Tap water cooling 25...........................
9.3.1 Connection to cooling (tap) water 25........
9.4 Pressure pump 26.............................
9.4.1 Temperature controlling an object in the
internal bath 26..........................
9.4.2 Connection of external closed systems 26...
9.4.3 Connection of external open systems 26....
10. Filling with Bath Liquid 27......................
10.1 Recommended bath liquids 27...................
10.2 Filling with heat transfer liquid 31.................
11. Draining 32....................................
12. Connecting Up 33..............................
12.1 Connecting to the mains 33.....................
12.2 Checking the liquid circuit 33....................
12.3 Changing the mains plug (e.g. for Great Britain) 33.
12.4 Fuses on the unit 34............................
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Table of Contents
2 HAAKE Phoenix II P1Version 3.07
13. Configuration 35...............................
13.1 Setting unit 35.................................
13.1.1 Display contrast adjustment 35............
13.1.2 Acoustic Signal 35.......................
13.1.3 Reset 36................................
13.1.4 Autostart 36.............................
13.1.5 Setting of time and date 36................
13.1.6 Language 37............................
13.1.7 Self test 37..............................
13.1.8 Multi functional port 37....................
13.2 Setting Regulation 38...........................
13.3 Setting Temperature 38.........................
13.3.1 Temperature display 38...................
13.4 Setting Interface 38............................
13.4.1 Interface RS232C 38.....................
13.4.2 Analog interface (option!) 38...............
13.5 Setting Status 39...............................
13.5.1 Version numbers 39......................
13.6 Operation status 39............................
13.7 Settings the pump speed 39.....................
14. Operating 40..................................
14.1 Switching on 40................................
14.2 Setting the desired set value 41..................
14.2.1 Setting the desired set temperature 41......
14.2.2 Setting and selecting the set values 41.....
14.2.3 Setting the RTA system correction value 42.
14.3 Change actual set value quickly 42...............
14.4 Ramp functions 43.............................
14.4.1 Entering a temperature program 43........
14.4.2 Viewing stored programs 44...............
14.4.3 Graphical display of the active temperature
program 44....................................
14.4.4 Deleting a program 44....................
14.4.5 Selecting beep 44........................
14.4.6 Running a temperature program 45........
14.4.7 Stopping the temperature program 45......
14.4.8 Example of a program 46.................
14.5 Working with internal or external control sensors 48
14.5.1 Selection between extern. and intern. control. 48
14.5.2 Speed of the external control. 48...........
14.5.2.1. Automatic setting 48...................
14.5.2.2. Manual adjustments 48.................
14.5.3 Differential control 49.....................
14.6 Working with or without cooling
(only in combination with cooling units) 50.........
14.7 Setting temperature limit values 50...............
14.8 Controlling heating and cooling 51................
14.9 Operating without control 51.....................
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Table of Contents
3 HAAKE Phoenix II P1Version 3.07
15. Excess Temperature Protection 52..............
15.1 Excess temperature protection dial 52............
15.1.1 Setting the excess temperature 53.........
15.1.2 Testing the cut-off point 53................
16. Fault Displays 54..............................
16.1 Excess temperature 54.........................
16.2 Low liquid level cut-off 54.......................
16.3 Pump or motor overloading 54...................
16.4 Sensor breakage or short circuit 55...............
16.5 External fault 55...............................
16.6 External fault RS232C 55.......................
16.7 Error in connection with cooling units 56..........
17. Testing the Safety Features 57..................
17.1 Excess temperature protection 57................
17.2 Low liquid level protection 57....................
18. External Connections 58.......................
18.1 Interface RS232C see chapter 19. 58.............
18.2 Multi--function connection 58....................
18.2.1 Remote alarm 58........................
18.2.2 Contact input for unit ON/OFF 58..........
18.2.3 Potential free contact for alarm triggering 58.
18.3 External Pt100 sensor 59.......................
18.4 I/O port (option!) 59............................
18.5 Shielded Cables 59............................
19. RS232C Interface 60...........................
19.1 Connecting to a computer 60....................
19.1.1 PC with an RS232C interface 60...........
19.2 Interface parameter 62..........................
19.3 Requirements made of external units 63..........
19.4 Setting the desired set value 63..................
19.5 Correction value 63............................
19.6 Controlling a circulator 63.......................
19.7 Sets of commands 64..........................
19.8 Operating status / Error message 70..............
19.9 Example definition of a ramp program by PC 71....
20. Cooling 74....................................
20.1 Abweichung der Kälteleistung 74.................
21. Maintenance 75................................
21.1 Cleaning the fins of the liquefier 75...............
21.2 Discarding the unit: 75..........................
22. Disassembly of Temperature Control Module
and Bath Vessel 76.............................
23. Technical Specifications 77.....................
23.1 Bridge Circulators 77...........................
23.2 Heating Circulators P1 77.......................
23.3 Refrigerated Circulators 78......................
23.4 Cryostats 78...................................
23.5 Fuse values 79................................
24. Appendix 80...................................
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Key to Symbols
4 HAAKE Phoenix II P1Version 3.07
1. Key to Symbols
1.1 Symbols used in this manual
Warns the user of possible damage to the unit, draws
attention to the risk of injury or contains safety notes
and warnings.
Denotes an important remark.
1Indicates the next operating step to be carried out and
…
⇒…what happens as a result thereof.
1.2 Symbols used on the unit (front)
Caution: Read the instruction manual before oper-
ating.
Instrument in ”off” position.
Instrument in ”on” position.
1.3 Symbols used on the unit (rear)
Pump connection: back flow (suction) from the
external object.
Pump connection: pressure to the external object.
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1.
2.
ALARM
IDENT
Key to Symbols
5 HAAKE Phoenix II P1Version 3.07
1.4 Symbols used on the display
ALARM flashes and heater element, pump and if avail-
able, cooling circuit have been switched off. Any cause
of the alarm is displayed in a second line.
Appears,
if heater is active and flashes during the control phase.
if cooling is active with full cooling capacity.
if cooling is active with partial cooling capacity.
Star 1 and 2 are blinking alternately when the cooling
is on.
The crossed out star is on when the cooling unit is off.
if ramp function is activated.
IDENT flashes: After starting the control and after ente-
ring a new set temperature, the controller determines
suitable control parameters. It can happen that heating
or cooling is interrupted during this process and the dis-
played temperature changes. This is because the con-
trol unit requires some time to determine the parame-
ters.
For this function the identification has to be activated
(“Settings„ / “Control„ menu).
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Key to Symbols
1.5 Menu Tree
6 HAAKE Phoenix II P1Version 3.07
Ramp functions
Start ramp
View / Selection
Settings Start / Stop Set values
S1
S2
S3
S4
Change
set value
Change
RTA value
Ports
RS232
Analog
Interface
Selection
Watchdog
Temp settings
Limits
Temp.
format
Cooling
Control
External
control
Identification
Diff. cont
Unit
LCD
contrast
Beep
OFF/ON
Reset
Multi funct.
port
Autostart
Time / Date
Control
Language
Self test
New ramp
Delete ramp
Beep
Reset ramp
Reset
customer
settings
Total reset
Control
PumpStatus
Activate
set value
Graph
Cange act. set val.
external
internal
Cykles
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Quality Assurance
7 HAAKE Phoenix II P1Version 3.07
2. Quality Assurance
Dear customer,
Thermo Electron (Karlsruhe) implements a Quality Manage-
ment System certified according to DIN/EN/ISO 9001:2000.
This guarantees the presence of organizational structures
which are necessary to ensure that our products are devel-
oped, manufactured and managed according to our custom-
ers expectations. Internal and external audits are carried out
on a regular basis to ensure that our QMS is fully functional.
We also check our products during the manufacturing pro-
cess to certify that they are produced according to the speci-
fications as well as to monitor correct functioning and to con-
firm that they are safe. This is why we initiate this monitoring
process of important characteristics already during
manufacturing and record the results for future reference.
The “Final Test” label on the product is a sign that this unit
has fulfilled all requirements at the time of final manufactur-
ing.
Please inform us if, despite our precautionary measures,
you should find any product defects. You can thus help us to
avoid such faults in future.
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Thermo Electron (Karlsruhe) GmbH
TYP
V/Hz
Dieselstr. 4
76227 Karlsruhe
Contacts at Thermo Electron (Karlsruhe) GmbH
8HAAKE Phoenix II P1 Version 3.07
3. Your Contacts at
Thermo Electron (Karlsruhe) GmbH
Please get in contact with us or the authorized agent who supplied
you with the unit if you have any further questions.
Thermo Electron Corporation
International / Germany
Thermo Electron (Karlsruhe) GmbH
USA
Thermo Electron
Dieselstrasse 4 25 Nimble Hill Rd.
D-76227 Karlsruhe, Germany Newington, NH 03801
Tel. [phone] Tel. [phone]
Fax [phone] Fax: [phone]
Hotline [phone]
[email protected] [email protected]
www.thermo.com/tc www.thermo.com/tc
France
Thermo Electron S.A.
Great Britain
Thermo Electron
16 Avenue du Québec Silic 765 Temperature Control Business
F--91963 Courtaboeuf Cedex Ion Path, Road Three
Winsford, Cheshire CW7 3GA
Tel.[phone] Tel.[phone]
Fax [phone] Fax [phone]
[email protected] [email protected]
www.thermo.com/tc www.thermo.com/tc
Benelux
Thermo Electron B.V.
Takkebijsters 1
NL--4817 BL Breda
Tel.[phone]
Fax[phone]
[email protected]
www.thermo.com/tc
The following specifications should be given when product
enquiries are made:
-- U n i t n a m e printed on the front of the unit,
-- T Y P as specified on the name plate.
-- V e r s i o n of the operating software
(see chap. 13.5.1).
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Test Certificate
9 HAAKE Phoenix II P1Version 3.07
4. Thermo Electron (Karlsruhe)
Test Certificate for HAAKE Phoenix II P1
This is to certify that the tempering device which you have
acquired and to which these instructions for operation refer
has been tested and equilibrated by Thermo Electron (Karls-
ruhe) GmbH in compliance with the regulations of a certified
Quality Assurance System according to DIN ISO 9001.
Testing for constancy of temperature has been carried out in
keeping with DIN standard DIN 12876 for laboratory equip-
ment. (follow--up standard to DIN standard 58966).
The measuring equipment used in the testing process is re-
gularly calibrated and can be traced back to the national
norms of the Physikalisch Technische Bundesanstalt (PTB)
Deutschlands1or to other national norms. In those cases
where there are no norms and standards on a national level,
the testing process is in keeping with currently valid technical
rules and regulations, norms and standards.
All required measuring data are listed on this page of the Test
Certificate.
Measuring conditions
Ambient temperature: + 20°C
Power supply / --frequency: 230V ±5V / 50 Hz
respectively 115V ±5V / 60Hz
System parameters
Volume: 8 litre
Liquid: Water
Rated temperature: +70°C
Measuring process
Checking constancy of temperature in bath according to
DIN 12876, part 2 (follow-up standard to DIN 58966, part 2,
paragraph 4.3)
Measuring agent
Type of sensor used for measuring
according to DIN IEC 751
Test results
Constancy of temperature (Width of control range)
Accuracy at +70°C
The individual test certificate for your thermostat will be pro-
vided upon request.
We and our partners shall gladly be at your disposal for
a calibration of your thermostat at your premises. Just
contact us.
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Safety Notes
10 HAAKE Phoenix II P1Version 3.07
5. Safety Notes
These notes are intended to draw your attention to risks
which only YOU can recognize and avoid or overcome. They
are intended to enhance your own safety consciousness.
We have set the highest quality standards for ourselves and
this unit during development and production. Every unit
meets relevant safety regulations. The correct unit usage
and proper handling is however solely your responsibility.
The intended workplace should correspond to a laboratory
or pilot plant environment. The user should have an educa-
tion level which is at least equivalent to a trained laboratory
worker or specialized chemist. The following list should be
seen as an example.
The device may not be operated if there are any doubts
regarding a safe operation due to the outer appearance
(e.g. damages).
A safe operation of the instrument cannot be guaran-
teed if the user does not comply with this instruction
manual.
Ensure that this manual is always at hand for every unit
operator.
Only use this unit solely for the intended application.
Repairs, alterations or modifications must only be car-
ried out by specialist personnel. Consider the manufac-
turer’s instruction manuals.
Considerable damage can be caused by improper re-
pairs. The Thermo Haake service department is at your
disposal for repair work.
Do not operate the unit with wet or oily hands.
Do not expose the unit to spray water or immerse it in
water.
Do not clean the unit with solvents (fire risk!) -- a wet
cloth soaked in household detergent is normally suffi-
cient.
This device is not designed according to the standard
EN 60601-1: 1990 (DIN VDE 0750-1 and IEC 601-1) and
should not be operated in rooms used for medical pur-
poses and/or in the vicinity of patients.
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Safety Notes
11 HAAKE Phoenix II P1Version 3.07
Many units parts can become hot as a result of normal
unit functioning - there is a high risk of burns!
The overall temperature of the marked zone (see fig.)
will become higher than 70°C when the bath tempera-
ture exceeds approx. 200°C. Please ensure that ade-
quate contact protection is provided.
Do not move the unit from the position where it was set
up during operation or when it is still hot. There is a high
risk of burns!
Only use the heat transfer liquids recommended by
Thermo Haake. Please refer to the respective EC Safety
Data Sheet.
The temperature controlling i.e. immersing of test
tubes, Erlenmeyer flasks or similar objects directly
within the circulator constitutes normal circulator
practise.
We do not know which substances are contained within
these vessels. Many substances are:
•inflammable, easily ignited or explosive
•hazardous to health
•environmentally unsafe
i.e.: dangerous
You alone are responsible for the handling of these sub-
stances!
Our advice:
•If in doubt, consult a safety specialist.
•Read the product manufacturer’s or supplier’s EC
Safety Data Sheet according to directive 91/155/EEC.
•Read relevant regulations concerning dangerous
materials.
•Observe relevant guidelines for laboratories in your
country.
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Safety Notes
12 HAAKE Phoenix II P1Version 3.07
The following measures were taken for the protection of
the operator:
•Protection Class I according to VDE 0106 T1 (IEC 536)
i.e. protection against electric shocks by grounding all
parts which carry the risk of electric contact.
The device must only be connected to mains recep-
tacles with a protective ground.
•Protection IP 30 according to EN 60529 for all Phoenix-
temperature control units, i. e. regarding the protection
against accidently touching live parts and damage by
foreign matter, it has been ensured that foreign bodies
with a thickness or diameter of more than 2.5 mm can-
not penetrate.
•Protection IP 20 according to EN 60529 for all cooling
units, i. e. regarding the protection against accidently
touching live parts and damage by foreign matter, it has
been ensured that foreign bodies with a thickness or di-
ameter of more than 12 mm cannot penetrate.
No special precautions were taken against the pe-
netration of water and dust. The device should there-
fore not be used in a dusty atmosphere or in the neigh-
borhood of spray water.
Do not insert wires or tools in any of the openings.
Complete separation from the mains is required
when:
-- all dangers caused by this device are to
be avoided,
-- cleaning is carried out,
-- repairs or maintenance work is about to be
carried out.
Complete separation means:
Pull out the mains plug!
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Unit Description
13 HAAKE Phoenix II P1Version 3.07
6. Unit Description
All units fulfill the requirements of safety class 3 according to
DIN 12876 and are thus suitable for unsupervised continu-
ous operation.
The circulator pump motor is protected against thermal over-
loading. All temperature sensors are permanently monitored
according to break or short circuit. The cooling machine is
integrated into the general safety circuit.
6.1 Safety features
The comprehensive safety system is designed on the princi-
ple of the concept of the “single fault” (EN 61010). This as-
sumes that two separate faults do not occur simultaneously.
This system therefore offers protection against one (single)
fault. This one fault will effectively occur automatically ...
•if you do not read this manual,
•if you do not correctly set the excess temperature
protection, i.e. the safety reserves have already been
used up.
Such faults can include e.g.:
Fault in the temperature control unit:
⇒Excess temperature ⇒poss. fire danger
Leakage in the liquid circuit or
Evaporation of heat transfer liquid:
⇒Low liquid level ⇒poss. fire danger
Pump blocked:
⇒poss. fire danger
Or also:
Excess temperature protection level not correctly set:
⇒poss. fire danger
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Unit Description
14 HAAKE Phoenix II P1Version 3.07
6.2 Safety class 3 according to DIN 12876
A variably adjustable excess temperature protection and in-
dependent low liquid level protection which is preset to the
lowest level allow the usage of different heat transfer liquids.
If a safety element is triggered…
•the cause for the fault is displayed,
•the safety-relevant components (heating element, mo-
tor and compressor) are switched off immediately i.e. the
safety circuit transfers the unit to a stable, safe condition,
•the temperature of the heat transfer liquid gradually
adjusts to ambient temperature.
6.3 Applications
As open-bath circulator:
For temperature controlling samples within the circula-
tor’s own bath.
As heating circulator:
For temperature controlling closed temperature control
circuits such reactors, heat exchangers or similar objects.
Temperature controlling of open vessels using the
built-in combined pressure and suction pump
6.4 Temperature ranges
Working temperature range:
The temperature range of the circulator without addi-
tional heating or cooling sources.
Operating temperature range:
The temperature range of the circulator which can be
reached if additional heating or cooling sources are used.
Tap water can be used as a cooling source. In this case
the minimum working temperature possible is approx.
3°C above that of the tap water temperature.
High operating temperatures mean the unit sur-
faces heat up. Protective measures must be taken!
Mains cable:
The mains cables used are specially designed for
usage with heating elements. They can be allowed to
come into contact with parts which are heated up to a
temperature of max. 250°C.
Mains cables may be changed only from autho-
rized technical personnel.
Warning for maintenance personnel: Use with the
replacement an original Thermo Electron spare
part (cable)! (Please get in contact with Thermo Elec-
tron service department.)
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B
CE
D
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Unpacking / Setting Up
15 HAAKE Phoenix II P1Version 3.07
7. Unpacking / Setting Up
7.1 Transportation damage?
•Notify carrier (forwarding merchant, railroad) etc.
•Compile a damage report.
Before return delivery:
•Inform dealer or manufacturer
(Small problems can often be dealt with on the spot).
7.2 Contents
2 Coupling Nuts E, 4 Hose clamps,
(already assembled) BOrder no. 000-2025
Order no. 001-0797 COrder no. 000-2716
2 Plug pieces D, 1 Instruction Manual
(already assembled) 1 Warranty Card
Order no. 001-0798 (please fill out and return)
2 Hose fittings Bfor hoses 8 mm ∅,
Order no. 001-1209
2 Hose fittings Cfor hoses 12 mm ∅
Order no. 001-1210
7.3 Ambient conditions according to EN 61010
•indoors, max. 2000 meters above sea level,
•ambient temperature 5 ... 40°C,
•relative humidity max. 80%/31°C(→50%/40°C)
•excess voltage category II, contamination level 2
7.4 Resting time after transportation
(only for refrigerated circulators)
As we can unfortunately not guarantee that our refrigerated
circulators are always transported according to our recom-
mendations (i.e. upright), lubrication oil can leak from the
compressor into the cooling circuit.
If the refrigerated circulator is started up whilst still in this
state, the compressor may be damaged to the lack of oil.
Therefore:
Rest the unit for 24 hours after setting up.
7.5 Ventilation
Keep all ventilation grids (on front and rear) free from
obstruction to ensure unhindered air circulation.
Blocked ventilation grids lead to increased unit
heating which in turn reduces the cooling capacity
and thus impairs correct functioning.
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Information concerning the CE sign
16 HAAKE Phoenix II P1Version 3.07
7.6 Information concerning the CE sign
The measuring and control instruments from Thermo Elec-
tron (Karlsruhe) carry the CE sign which confirms that they
are compatible with the EU guideline 89/336/EEC (electro-
magnetic compatibility). The tests are carried out according
to module H (official sheet L380 of the European Commu-
nity) as our quality assurance system is certified according
to DIN / ISO 9001.
It was tested according to the strict EMV test requirements
of the EN61326-1/A1 (EMV requirements for electrical
equipment for measuring technology, conduction techno-
logy and laboratory usage). This means it was tested for in-
terference resistance and interference emission according
to public low-voltage mains (household and commercial
usage).
The following basic standards were applied in detail:
Interference resistance:
EN61000--4--2 electrostatic discharge
EN61000--4--3 electromagnetic fields
EN61000--4--4 fast transients
EN61000--4--5 surge voltages
EN61000--4--6 wire--guided HF--signals
EN61000--4--8 magnetic field of mains frequency
EN61000--4--11 voltage drop/short--time interruption
Interference emission:
CISPR16/class B wire--guided interference emission
CISPR16/class B radiated interference emission
EN 61000--3--2 voltage variations and flickering
EN 61000--3--3 over-compensation voltage flows
The application in industrial and commercial (public mains)
environments is thus possible.
A declaration of conformity is supplied with the ordered unit
on request.
Our strict standards regarding operating quality and the re-
sulting considerable amount of time and money spent on de-
velopment and testing reflect our commitment to guarantee
the high level of quality of our products even under extreme
electromagnetic conditions. Practice however also shows
that even units which carry the CE sign such as monitors or
analytical instruments can be affected if their manufacturers
accept an interference (e.g. the flimmering of a monitor) as
the minimum operating quality under electromagnetic com-
patibility conditions. For this reason we recommend you to
observe a minimum distance of approx. 1 m from such units.
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Unpacking / Setting Up
17 HAAKE Phoenix II P1Version 3.07
7.7 Mounting onto baths and bath bridges
The temperature control unit and bath bridges will
be delivered unassembled by means of transpor-
tation.
Switch off the unit and pull out the mains plug.
1Guide the unit down into the opening in a curve.
Do not damage Floats, possibly easily raise.
2Attach the unit with 2 screws.
(Order no. 003-6401)
Tighten only by hand.
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Functional Elements
18 HAAKE Phoenix II P1Version 3.07
8. Functional Elements
8.1 Front Phoenix II P1
5
4
32
1
HAAKE
PHOENIX II
1Symbol: Read the instruction manual!
2Mains switch
3Excess temperature setting
410 control keys to the function and menu selection
5LC display
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