Thermo Scientific Auto Sample Changer 6 Operation and maintenance manual

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Thermo Scientific ASC6
Auto Sample Changer 6
Instruction Notice
AA83863 - A • October 2019

Contents
1Revision Table...................................................................................................3
2Introduction.......................................................................................................4
3Safety.................................................................................................................6
3.1 General Safety Guidelines...................................................................................6
3.2 Hazard Statements and Symbols.........................................................................7
4The Sample Holder Description.......................................................................8
5Installation.........................................................................................................9
5.1 Install the ASC6 in ARL EQUINOX......................................................................9
5.2 Connections to the Power Supply........................................................................9
5.3 Setting of the Incident Angle................................................................................9
6Sample Preparation Procedure......................................................................11
6.1 Preparation of the Sample Cup..........................................................................11
6.2 Insertion of the Sample Cup in the ASC6...........................................................12
7Maintenance and Cleaning.............................................................................14
8Troubleshooting..............................................................................................15
9Appendix 1: Conformity Certificate...............................................................16
10 Index ................................................................................................................17

Chapter | Revision Table
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Instruction Notice, Auto Sample Changer 6
Page 3
1 Revision Table
Revision
Date
ECO number
Description of Changes
A
10-OCT-2019
SDR19976
Initial release
Note This document is the original manual.
The information in this document is subject to change without notice.
We assume no responsibility for any errors that may appear in this document.

Chapter | Introduction
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Instruction Notice, Auto Sample Changer 6
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2 Introduction
ARL EQUINOX X-Ray diffractometers are designed for measuring of crystalline samples
(powder, bulk, metals, thin layers, etc...), phase identification, nanoscale structural analysis,
non-destructive quality control, as well as for many other applications.
Thermo Fisher Scientific develops and sells many sample holders that can be plugged in
Thermo Fisher Scientific diffractometers in order to analyze the samples. The sample holders
sometimes consist of moving parts and electronics which are needed for more complex
devices to control sample's movement.
All ARL EQUINOX instruments are shipped with a basic non-spinning sample holder suited for
powder measurement in reflection mode. This sample holder is necessary for adjustment and
alignment and can be used for measurement of samples as well.
This instrument is intended for professionals. The user is advised to read the following
instructions and any other additional information supplied by Thermo Fisher Scientific before
operating the instrument.
Thermo Fisher Scientific declines all responsibilities for improper use by unauthorized
personnel or non-authorized operation of the instrument.
For any additional information, contact Thermo Fisher Scientific.
Supplied Items
Before the shipment, the sample holders are tested and packed carefully. However damage
can occur during the transport.
If the sample holder or any additional supplied item has been damaged during transport, or
if you notice any signs of a possible damage, please contact both the transport company
representative and the Thermo Fisher Scientific representative as soon as possible.
Furthermore, if you notice that any part is missing or you have any questions about
the delivered items, contact the Thermo Fisher Scientific representative.
Storage
The storage where the instrument is stored has to meet following ambient specifications:
Temperature: 0 –50°C, relative humidity: < 95% (without condensation).
Assistance
The Thermo Fisher Scientific worldwide technical support network consists of highly trained
field service engineers, technical support specialists and service coordinators who are ready
to quickly assist the customers with answers and solutions to service needs and application
questions. If you need any help, please contact the local Thermo Fisher Scientific
representative.

Chapter | Introduction
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Instruction Notice, Auto Sample Changer 6
Page 5
Manufacturer
THERMO FISHER SCIENTIFIC INEL SAS
71 rue d’Orléans
45410 ARTENAY, FRANCE
Tel : [phone]

Chapter | Safety
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Instruction Notice, Auto Sample Changer 6
Page 6
3 Safety
3.1 General Safety Guidelines
•Before using your sample holder, read its instruction manual completely and understand it.
Please take notice of all warnings, cautions and notes to ensure the correct and safe
functioning of the instrument.
•Never place the sample holder near an open flame or in an excessively hot environment.
It must not be installed in an ATEX explosive hazard area.
•Never place the sample holder in locations where excessive moisture or corrosive
materials are present.
•The sample holder construction provides protection against the risk of electrical shock by
grounding the appropriate metal parts. The protection may not work properly unless
the ARL EQUINOX power cord is connected to a properly grounded socket. It is
customer's responsibility to assure that a proper ground connection is provided.
•Never use flammable or corrosive fluids with this unit.
•If the sample holder is used in a manner not specified by Thermo Fisher Scientific,
the protection provided by the sample holder may be impaired.
•Only accessories that comply with Thermo Fisher Scientific specifications are allowed to
be used with ARL EQUINOX X-Ray diffractometers.
•Transport of the sample holder should be done with extreme care.
•Never operate a damaged sample holder.
•Never operate the sample holder with a damaged power cord.

Chapter | Safety
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Instruction Notice, Auto Sample Changer 6
Page 7
3.2 Hazard Statements and Symbols
The following messages are used throughout the manuals to highlight information.
Note A Note message indicates the information in it requires special attention.
CAUTION!
A Caution message indicates a potentially hazardous situation that, if not avoided,
may result in moderate or minor injury. It may also be used to alert against unsafe
practices.
SERVICE!
A Service message indicates that the described procedure should be performed by
qualified personnel only.
DANGER!
A danger message indicates a risk of injury. In this case the risk concerns the hand
or finger.

Chapter | The Sample Holder Description
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Instruction Notice, Auto Sample Changer 6
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4 The Sample Holder Description
The ASC6 (Auto Sample Changer 6) sample holder enables to analyze automatically 6
powder samples in reflection mode.
1- 30 mm diameter axis
2- Incidence angle indicator
3- SUB D 9 Connector for the power supply
and the communication
4- Moving part
5- Analysis position for the sample cup
6- Anti-scattering knife
CAUTION!
Do not touch the anti-scattering knife (6). This operation has to be done by service
only.
DANGER!
The item 4 is a moving part! Do not put your finger: risk of finger pinch!

Chapter | Installation
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Instruction Notice, Auto Sample Changer 6
Page 9
5 Installation
5.1 Install the ASC6 in ARL EQUINOX
Insert the sample holder in the sample holder mounting hole of the instrument, do not use
any unnecessary force. The sample holder and the mounting hole (Ø 30 mm) are designed
to avoid any mechanical clearance resulting in irreproducible results. The pin of the
sample holder has to be inserted in the reference hole.
For more detailed information refer to the ARL EQUINOX instruction notice.
5.2 Connections to the Power Supply
The ASC6 sample holder is supplied by 12 VDC and 24 VDC.
The power supply plug for the spinning sample holder is located below the sample area in
the ARL EQUINOX.
Refer to the ARL EQUINOX reference manual for more details.
5.3 Setting of the Incident Angle
The incidence angle indicator consists of two rings. One ring is fixed while the second one is
free. This allows the sample holder to rotate in order to change the incidence angle. This
second ring can be tightened to avoid changes of the incidence angle. The way of reading
the incidence angle indicator is described in the picture below. The longest line represents
the incidence angle equal to 0° (2). Each short line represents 2° of incidence angle (4).
The medium long lines represent 10° of incidence angle (3). Then, the indicator (1) serves to
read the total incidence angle.
The sample holder is equipped with a positioning pin to avoid any position mistake and
an incidence angle indicator to read the incidence angle.

Chapter | Installation
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Instruction Notice, Auto Sample Changer 6
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1- Reading indicator
2- Incidence angle equal to 0°
3- Medium line 10° of incidence angle
4- Short line 2° of incidence angle

Chapter | Sample Preparation Procedure
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Instruction Notice, Auto Sample Changer 6
Page 11
6 Sample Preparation Procedure
6.1 Preparation of the Sample Cup
In order to prepare your sample, you will need a powder mount,
a spatula, a glass slide (as used for microscopes) and a sample
cup.
If the powder to be measured is too coarse, it is necessary to
grind it a bit using a small mortar.
Fill the sample powder cup with the powder.
Use a glass slide to make the surface flat and homogeneous.
The surface of the powder must not exceed the level of the
surface of the powder mount, in order to avoid line displacement
error due to height error.

Chapter | Sample Preparation Procedure
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Instruction Notice, Auto Sample Changer 6
Page 12
6.2 Insertion of the Sample Cup in the ASC6
Before the insertion of cups, the half-moon must be in the position that allows the insertion.
If it is not the case connect the sample holder in the ARL Equinox in order to obtain this
position by rotating the half-moon by pushing the black button 1 (see the picture below).
Insert the cup on the sample holder by pushing down and laterally in order that the cup is in
analysis position.

Chapter | Sample Preparation Procedure
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Instruction Notice, Auto Sample Changer 6
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ASC6 with the six samples ready to be inserted in the ARL EQUINOX 100.

Chapter | Maintenance and Cleaning
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Instruction Notice, Auto Sample Changer 6
Page 14
7 Maintenance and Cleaning
The sample holder can be cleaned with a soft and dry duster. The sample positioning platform
can be cleaned with a moist duster or with some domestic alcohol.

Chapter | Troubleshooting
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Instruction Notice, Auto Sample Changer 6
Page 15
8 Troubleshooting
•Check the state of the power supply cord, be sure it is properly plugged in.
•Check if the software driver is properly installed.
•If the problem persists, contact Thermo Fisher Scientific.

Chapter | Appendix 1: Conformity Certificate
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9 Appendix 1: Conformity Certificate
Thermo Fisher Scientific has certified by internal assessment that the ASC6 ample holder
complies with the CE mark according to the following standards and directives:
•EN 61010-1 (2010): Safety requirements for electrical equipment for measurement,
control, and laboratory use - Part 1: General requirements,
•2011/65/EC: restriction of the use of certain hazardous substances in electrical and
electronic equipment, RoHS2.
Thermo Fisher Scientific has certified by an independent control authority that the ASC6
complies with:
•EN 61326-1 (2013): Electrical equipment for measurement, control and laboratory use -
EMC requirements - Part 1: General requirements.

Chapter | Index
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Instruction Notice, Auto Sample Changer 6
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10 Index
A
Appendix 1
Conformity Certificate • 17
C
Connections to the Power Supply • 10
G
General Safety Guidelines • 6
H
Hazard Statements and Symbols • 7
I
Insertion of the Sample Cup in the ASC6 • 13
Install the ASC6 in ARL EQUINOX • 10
Installation • 10
Introduction • 4
M
Maintenance and Cleaning • 15
P
Preparation of the Sample Cup • 12
R
Revision Table • 3
S
Safety • 6
Sample Preparation Procedure • 12
Setting of the Incident Angle • 11
T
The Sample Holder Description • 8
Troubleshooting • 16

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