Agilent Technologies 1260 Infinity User manual

Agilent Technologies
Agilent 1260 Infinity
Standard Autosampler
User Manual

Agilent 1260 Infinity Standard Autosampler User Manual
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Manual Part Number
G1329-90013
Edition
06/10
Printed in Germany
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Agilent 1260 Infinity Standard Autosampler User Manual 3
In This Book
In This Book
This manual covers the Agilent 1260 Infinity Standard Autosampler (G1329B).
1 Introduction to the Autosampler
This chapter gives an introduction to the autosampler, instrument overview
and internal connectors.
2 Site Requirements and Specifications
This chapter provides information on environmental requirements, physical
and performance specifications.
3 Installing the Autosampler
This chapter provides information on unpacking, checking on completeness,
stack considerations and installation of the module.
4 Using the Autosampler
This chapter provides information on how to set up the module for an analysis
and explains the basic settings.
5 Optimizing Performance
This chapter provides information on how to optimize the module.
6 Troubleshooting and Diagnostics
Overview about the troubleshooting and diagnostic features.
7 Error Information
This chapter describes the meaning of error messages, and provides
information on probable causes and suggested actions how to recover from
error conditions.

4 Agilent 1260 Infinity Standard Autosampler User Manual
In This Book
8 Maintenance
This chapter describes the maintenance of the module.
9 Parts and Materials for Maintenance
This chapter provides information on parts for maintenance.
10 Identifying Cables
This chapter provides information on cables used with the module.
11 Appendix
This chapter provides addition information on safety, legal and web.

Agilent 1260 Infinity Standard Autosampler User Manual 5
Contents
Contents
1 Introduction to the Autosampler 9
Introduction to the Autosampler 10
Early Maintenance Feedback (EMF) 20
Instrument Layout 21
Electrical Connections 22
Interfaces 24
Setting the 8-bit Configuration Switch (On-Board LAN) 30
2 Site Requirements and Specifications 39
Site Requirements 40
Physical Specifications 44
Performance Specifications Standard Autosampler 45
3 Installing the Autosampler 47
Unpacking the Autosampler 48
Optimizing the Stack Configuration 49
Installing the Autosampler 53
Installing the Thermostatted Autosampler 56
Flow Connections 60
Installing the Sample Tray 62
Transporting the Autosampler 63
4 Using the Autosampler 65
Sample Trays 66
List of Compatible Vials and Caps 68
5 Optimizing Performance 71
Optimization for Lowest Carry-over 72
Fast Injection Cycle and Low Delay Volume 75
Precise Injection Volume 77
Choice of Rotor Seal 79

6 Agilent 1260 Infinity Standard Autosampler User Manual
Contents
6 Troubleshooting and Diagnostics 81
Overview of the Sampler’s Indicators and Test Functions 82
Status Indicators 83
Maintenance Functions 85
Standard Autosampler Step Commands 92
Troubleshooting 94
Troubleshooting Guide for the Sample Transport Assembly 96
Agilent Lab Advisor Software 103
7 Error Information 105
What are Error Messages 107
General Error Messages 108
Autosampler Error Messages 115
8 Maintenance 125
Introduction into Maintenance and Repair 126
Maintenance Functions 129
Simple Repairs 130
9 Parts and Materials for Maintenance 147
Main Assemblies 148
Analytical-Head Assembly 150
Vial Trays 152
Standard Autosampler Accessory Kit G1329-68755 153
Maintenance Kit G1313-68719 153
Multi-Draw Kit 154
External Tray G1313-60004 154

Agilent 1260 Infinity Standard Autosampler User Manual 7
Contents
10 Identifying Cables 155
Cable Overview 156
Analog Cables 158
Remote Cables 160
BCD Cables 163
External Contact Cable 165
CAN/LAN Cables 166
Auxiliary Cable 167
RS-232 Cables 168
11 Appendix 169
General Safety Information 170
The Waste Electrical and Electronic Equipment (WEEE) Directive
(2002/96/EC) 173
Lithium Batteries Information 174
Radio Interference 175
Solvent Information 176
Sound Emission 178
Agilent Technologies on Internet 179

8 Agilent 1260 Infinity Standard Autosampler User Manual
Contents

9
Agilent 1260 Infinity Standard Autosampler User Manual
Agilent Technologies
1
Introduction to the Autosampler
Introduction to the Autosampler 10
Sampling Sequence 12
Sampling Unit 15
Transport Assembly 18
Early Maintenance Feedback (EMF) 20
Instrument Layout 21
Electrical Connections 22
Serial Number Information (ALL) 23
Electrical Connections 22
Interfaces 24
Overview Interfaces 26
Setting the 8-bit Configuration Switch (On-Board LAN) 30
Communication Settings for RS-232C 34
Special Settings 36
This chapter gives an introduction to the autosampler, instrument overview and
internal connectors.

10 Agilent 1260 Infinity Standard Autosampler User Manual
1Introduction to the Autosampler
Introduction to the Autosampler
Introduction to the Autosampler
Figure 1 Overview of the Autosampler
The Agilent 1260 Infinity autosamplers are designed for use with other
modules of the Agilent 1200 Infinity Series, 1200 Series and 1100 Series LC
system, or with other LC systems if adequate remote control inputs and
outputs are available. The autosamplerss are controlled by the Agilent control
module (G4208A Instant Pilot) or by Agilent control software (ChemStation
for LC, EZChrom Elite etc.).
Three sample-rack sizes are available for the autosamplers. The standard
full-size rack holds 100 × 1.8 mL vials, while the two half-size racks provide
space for 40 × 1.8 mL vials and 15 × 6 mL vials respectively. Any two half-size
rack trays can be installed in the autosamplers simultaneously. A specially
designed sample-rack holding 100 × 1.8 mL vials is available for use with
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