Agilent Technologies 709-DS User manual

Agilent Technologies
708-DS / 709-DS
Dissolution Apparatus
Operator’s Manual

708-DS / 709-DS Operator’s Manual
Notices
© Agilent Technologies, Inc. 2014
No part of this manual may be reproduced
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United States and international copyright
laws.
Manual Part Number
70-9058
Edition
Rev D, February 2014
Agilent Technologies, Inc.
3501 Stevens Creek Blvd.
Santa Clara, CA 95052 USA
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Safety Notices
CAUTION
A CAUTION notice denotes a
hazard. It calls attention to an
operating procedure, practice, or
the like that, if not correctly per-
formed or adhered to, could result
in damage to the product or loss
of important data. Do not proceed
beyond a CAUTION notice until
the indicated conditions are fully
understood and met.
WARNING
A WARNING notice denotes a
hazard. It calls attention to an
operating procedure, practice,
or the like that, if not correctly
performed or adhered to, could
result in personal injury or
death. Do not proceed beyond a
WARNING notice until the
indicated conditions are fully
understood and met.

708-DS / 709-DS Operator’s Manual 3
Contents
Figures 7
Tab les 9
1Safety 11
Electrical Hazards 11
Warning 13
Caution 13
Note 13
Information Symbols 14
2 Introduction 15
Conventions Used in this Manual 17
Serial Number Format 18
3 Setting Up the 708-DS / 709-DS 19
Initial Setup 20
Unpacking Procedure 20
Environmental Requirements for Installation 22
Clearance 22
Equipment, Parts, and Accessories As Shipped 23
Parts and Accessories 23
Tubing / Cable Connections 24
Heater / Circulator Setup (708-DS) 24
Instrument Level / Water Bath Setup 25
Level Instrument 25

4 708-DS / 709-DS Operator’s Manual
Contents
DVH Power Controller Setup (709-DS) 28
Temperature Probe Installation (708-DS) 29
EVT Probe Installation (708-DS) 30
Power Cord Connections 30
708-DS / 709-DS Initial Power Up 30
Filling the Water Bath (708-DS) 31
Level Instrument - Re-verification 32
Heater / Circulator Power-up (708-DS) 32
Agilent 708-DS / 709-DS Setup 33
Vessel Isolation Chamber Installation (709-DS) 33
Vessel Installation 34
Sample Manifold Installation 35
Accessory Installation 37
Setting Basket (Apparatus 1) Heights 43
Setting Paddle (Apparatus 2) Heights 44
4 Operating the 708-DS / 709-DS 47
Main Screen - Options 48
Main Screen - Display Parameters 48
Main Screen - Sample Temperatures
49
Main Screen - Run 50
Main Screen - Stop 57
Main Screen - Drive Unit Up / Down 59
Manual Drive Unit Up / Down 60
Manual Sampling 61
Main Screen - Manifold Up / Down 62
Main Screen - Lock 63
Main Screen - Unlock 64
Main Screen - Remote Control 65
Main Screen - Alarms 65
Main Screen - Maintenance Due Icon 66

Contents
708-DS / 709-DS Operator’s Manual 5
Menu Screen - System Menu 67
Menu Screen - Method Editor 68
Menu Screen - Reports 77
Menu Screen - Alarms 80
Menu Screen - Instrument 82
Menu Screen - Calibration 87
Menu Screen - Diagnostics 90
Menu Screen - User Access 95
General 708-DS / 709-DS Conventions 96
Alphanumeric Data Entry 96
Numeric and Time / Date Entry 97
Parameter Limits / Ranges 98
Agilent 708-DS / 709-DS Notifications 100
Main Screen - Error Conditions 100
Dialog Screens (Green / Blue) 102
Warning Screens (Yellow) 104
Error Screens (Red) 109
5 Maintenance and Troubleshooting 115
Preventive Maintenance 116
Weekly Maintenance 116
Monthly Maintenance 116
Bi-Annual Maintenance 116
Sample Line / Paddle / Basket Care 117
Shafts 117
Baskets 118
Rinsing Sample Lines 119
Rinse Cups (Optional) 120
Vessels and Evaporation Covers 121
DVH Vessel Care (709-DS) 121
Water Bath and Temperature Probes (708-DS) 122

6 708-DS / 709-DS Operator’s Manual
Contents
Water Bath Care 122
Water Bath Temperature Probe Accuracy Test 123
Removing or Adjusting Cannulas / Probes 125
Manifold Maintenance 125
Removing the Manifold 125
Accessing the Top Cover 126
Removing Top Cover 126
Replacing the Top Cover 126
Printer Maintenance 127
Removing a Thermal Paper Roll 127
Inserting a Thermal Paper Roll (5095-0307) 130
Thermal Printer Test 133
Obtaining Warranty and Other Services 134
Index 135

708-DS / 709-DS Operator’s Manual 7
Figures
Figure 1. Unpacking 20
Figure 2. Removing the Apparatus 21
Figure 3. BATH HEATER Connector 24
Figure 4. Levelers and Stability Feet 25
Figure 5. Level-Adjustment Screw Caps 26
Figure 6. Raising the Stability Feet 27
Figure 7. DVH Power Controller 28
Figure 8. BATH TEMP Connector 29
Figure 9. Positioning the Temperature Probe 29
Figure 10. Filling the Water Bath 31
Figure 11. Vessel Bubble 34
Figure 12. Positioning the Manifold for Installation 35
Figure 13. Connecting AutoTemp 36
Figure 14. Affixing the Fasteners 37
Figure 15. Proper Sample Tubing Position 38
Figure 16. Installing Evaporation Covers on Shafts 39
Figure 17. Shaft Locking Collars 39
Figure 18. Dosage Delivery Module and Alignment Post 40
Figure 19. Inserting DDM into DDM Alignment Shaft 41
Figure 20. Attaching DDM to Alignment Post 42
Figure 21. Accessory Installation 43
Figure 22. Tightening the Shaft Locking Collar 44
Figure 23. Inserting Height Spheres 45
Figure 24. Main Screen - Display Parameters 48
Figure 25. Manual Lift Knob 60
Figure 26. Taking a Manual Sample 61
Figure 27. Agilent 708-DS / 709-DS Standard Evaporation
Cover 62
Figure 28. Rinse Cup 120

8 708-DS / 709-DS Operator’s Manual
Figures
Figure 29. Resistance Value of Temperature Probe 124
Figure 30. Near-empty Paper Roll 127
Figure 31. Accessing the Printer Handle 128
Figure 32. Open Printer Chamber 128
Figure 33. Removing the Thermal Paper Roll 129
Figure 34. Inserting a Thermal New Paper Roll 130
Figure 35. Leading Paper and Closing the Lid 131
Figure 36. Closing the Printer Chamber 131
Figure 37. Feeding Paper 132
Figure 38. Printer Test 133

708-DS / 709-DS Operator’s Manual 9
Tables
Table 1. Method - Start Options 52
Table 2. Method Properties Screen 1 69
Table 3. Method Properties Screen 2 70
Table 4. Method Properties Screen 2 72
Table 5. Menu Screen - Alarms 80
Table 6. Menu Screen - Instrument Settings Screen 1 82
Table 7. Menu Screen - Instrument Settings Screen 2 84
Table 8. Menu Screen - Instrument Settings Screen 3 85
Table 9. Menu Screen - Instrument Settings Screen 3 86
Table 10. Menu Screen - Diagnostics Screen 1 90
Table 11. Menu Screen - Diagnostics Screen 2 92
Table 12. Diagnostics - DVH Diagnostics Screen 1 93
Table 13. Numeric and Time / Date Entry 97
Table 14. Parameter Limits / Ranges 98
Table 15. Dialog Screens (Green / Blue) 102
Table 16. Warning Screens (Yellow) 104
Table 17. Error Screens (Red) 109

10 708-DS / 709-DS Operator’s Manual
Tables
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