Agilent Technologies InfinityLab LC Series User manual

Agilent Technologies
Agilent InfinityLab LC Series
Vialsamplers
User Manual

Agilent InfinityLab LC Series Vialsamplers User Manual
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Manual Part Number
G7129-90010 Rev. D
Edition
08/2018
Printed in Germany
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Agilent InfinityLab LC Series Vialsamplers User Manual 3
In This Book:
In This Book:
This manual covers the following modules:
•Agilent 1260 Infinity II Vialsampler (G7129A)
•Agilent 1290 Infinity II Vialsampler (G7129B)
•Agilent 1260 Infinity II Vialsampler (G7129C)
1Introduction
This chapter gives an introduction to the module and instrument overview.
2 Site Requirements and Specifications
This chapter provides information on environmental requirements, physical
and performance specifications.
3 Using the Module
This chapter provides information on how to use the module.
4 Installation of the Optional Sample Cooler or Thermostat
This chapter describes the installation of the optional sample cooler or
thermostat.
5 Preparing the Module
This chapter explains the operational parameters of the module.
6 Optimizing Performance
This chapter provides information on how to optimize the module.
7 Troubleshooting and Diagnostics
Overview about the troubleshooting and diagnostic features.

4 Agilent InfinityLab LC Series Vialsamplers User Manual
In This Book:
8 Error Information
This chapter describes the meaning of error messages, and provides
information on probable causes and suggested actions how to recover from
error conditions.
9 Maintenance and Repair
This chapter describes the maintenance and the repair of the module.
10 Parts and Materials for Maintenance
This chapter provides information on parts for maintenance.
11 Identifying Cables
This chapter provides information on cables used with the Agilent 1200
Infinity Series modules.
12 Hardware Information
This chapter describes the detector in more detail on hardware and
electronics.
13 LAN Configuration
This chapter provides information on connecting the module to the Agilent
ChemStation PC.
14 Appendix
This chapter provides addition information on safety, legal and web.

Agilent InfinityLab LC Series Vialsamplers User Manual 5
Contents
Contents
1Introduction 9
Product Description (G7129A) 10
Features (G7129A) 11
Product Description (G7129B) 12
Features (G7129B) 13
Product Description (G7129C) 14
Features (G7129C) 15
Overview of the Module 16
Operating Principle 18
Leak and Waste Handling 28
2 Site Requirements and Specifications 35
Site Requirements 36
Physical Specifications 40
Performance Specifications 41
Specifications of the Sample Cooler 47
Specifications of the Sample Thermostat 49
Specifications of the Integrated Column Compartment 51
3 Using the Module 53
Magnets 54
Turn on/off 55
Status Indicators 57
Exchange Drawers 58
Install the Integrated Column Compartment 60
Install the Column Shelf 66
Install the External Tray 70
Install a Column (ICC) 72
Remove a Column (ICC) 76
Sample Trays 78
Choice of Vials and Caps 81
Transporting the Sampler with a Sample Cooler or Sample Thermostat Installed 84
Agilent Local Control Modules 86

6 Agilent InfinityLab LC Series Vialsamplers User Manual
Contents
4 Installation of the Optional Sample Cooler or Thermostat 89
Damaged Packaging 90
Install the Sample Cooler or Thermostat 91
Using the Sample Cooler or Thermostat in an Infinity II Sampler 97
5 Preparing the Module 105
Leak and Waste Handling 106
Preparing the Module 107
Solvent Information 108
Capillary Color Coding Guide 114
Installing Capillaries 115
Flow Connections to the Vialsampler 117
Setting up the Vialsampler 119
6 Optimizing Performance 131
Optimization for Lowest Carry-over 132
Fast Injection Cycle and Low Delay Volume 136
Precise Injection Volume 138
Choice of Rotor Seal 140
7 Troubleshooting and Diagnostics 141
Overview of the Module’s Indicators and Test Functions 142
Maintenance Functions 144
Step Commands 153
Test s 155
Troubleshooting 156
Troubleshooting Guide for the Sample Transport Assembly 158
Agilent Lab Advisor Software 161
8 Error Information 163
What are Error Messages 165
General Error Messages 166
Sampler Error Messages 172
Sample Cooler Error Messages 180
Integrated Column Compartment (ICC) Heater Error Messages 183

Agilent InfinityLab LC Series Vialsamplers User Manual 7
Contents
9 Maintenance and Repair 185
Introduction to Maintenance 186
Warnings and Cautions 187
Overview of Maintenance 189
Cleaning the Module 190
Remove and Install Doors 191
Exchange the Needle Assembly 192
Exchange the Needle Seat Assembly 197
Exchange the Sample Loop Assembly 202
Exchange the Rotor Seal 206
Exchange the Metering Seal and Piston 212
Exchange the Gripper Arm 216
Replace the Peristaltic Pump Cartridge 219
Exchange the Wash Port Assembly 222
Replace the Module Firmware 228
10 Parts and Materials for Maintenance 229
Main Assemblies 230
Standard Parts 232
Drawer Assembly 233
External Tray 235
Analytical Head Assembly (40 μL) 236
Analytical Head Assembly (100 µL) 237
2ps 6pt Injection Valve 1300 bar 238
2ps 6pt Injection Valve 800 bar 239
2ps 6pt Injection Valve 600 bar 240
Integrated Column Compartment 241
Cabinet Kit 242
Sample Thermostat 244
Standard Vialsampler Accessory Kit 246
Multi-Draw Kit 248
Additional Part List 249
Column Identifier Kit 2C (G4751A) 250

8 Agilent InfinityLab LC Series Vialsamplers User Manual
Contents
11 Identifying Cables 251
Cable Overview 252
Analog Cables 254
Remote Cables 256
CAN/LAN Cables 260
RS-232 Cables 261
USB 262
12 Hardware Information 263
Firmware Description 264
Electrical Connections 267
Interfaces 269
Setting the 6-bit Configuration Switch 277
Instrument Layout 281
Early Maintenance Feedback (EMF)282
13 LAN Configuration 283
What You Have to Do First 284
TCP/IP parameter configuration 285
Configuration Switches 286
Initialization Mode Selection 287
Dynamic Host Configuration Protocol (DHCP) 289
Manual Configuration 292
PC and Agilent ChemStation Setup 297
14 Appendix 307
General Safety Information 308
Waste Electrical and Electronic Equipment (WEE) Directive 314
Refrigerant 315
Radio Interference 318
Sound Emission 319
Solvent Information 320
Agilent Technologies on Internet 321

9
Agilent InfinityLab LC Series Vialsamplers User Manual
Agilent Technologies
1
Introduction
Product Description (G7129A) 10
Features (G7129A) 11
Product Description (G7129B) 12
Features (G7129B) 13
Product Description (G7129C) 14
Features (G7129C) 15
Overview of the Module 16
Operating Principle 18
Sampling Sequence 18
Needle Parkstation 23
Hydraulic Box 24
Transport Assembly 26
Leak and Waste Handling 28
Leak Sensor 32
Waste Guidance 32
Waste Concept 33
This chapter gives an introduction to the module and instrument overview.

10 Agilent InfinityLab LC Series Vialsamplers User Manual
1 Introduction
Product Description (G7129A)
Product Description (G7129A)
The Agilent 1260 Infinity II Vialsampler is designed for the reliability, safety,
and ease-of-use needed for routine pharmaceutical tasks and quality control,
as well as for environmental and food analyses. It can house optionally the
integrated column compartment for two LC columns with temperature control
up to 80 °C as well as a sample cooler/sample thermostat for stable
temperatures down to 4 °C or from 4 °C up to 40 °C, all within one module.
Figure 1 Overview of the Vialsampler
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