Fisher Scientific 280A User manual

Model 280A Vacuum Oven
nstallation and Operating nstructions
Catalog No.
13-262-280A
13-262-281A
102265 • 2/5/10

Performance and Physical Data..........................................................................................................................3
Controls and ndicators ......................................................................................................................................4
Operation ............................................................................................................................................................5
Packing Checklist ........................................................................................................................................5
Temperature Adjustment ..............................................................................................................................6
Operation in a Static Environment................................................................................................................6
Operation in a Controlled Environment ........................................................................................................6
Operation in a Vacuum Environment............................................................................................................7
Vacuum Sealing Agents................................................................................................................................7
Out Gassing..................................................................................................................................................7
Safety Precautions........................................................................................................................................8
Maintenance and Servicing ................................................................................................................................9
Cleaning Suggestions ..................................................................................................................................9
Periodic Maintenance ..................................................................................................................................9
Gasket Replacement..............................................................................................................................9
Accessories and Replacement Parts ................................................................................................................10
Accessories ................................................................................................................................................10
Replacement Parts ....................................................................................................................................10
Schematics ........................................................................................................................................................11
Warranty ............................................................................................................................................................12
2
Table of Contents

Mo el No. 280A
Catalog No. 13-262-280A (120V), 13-262-281A (240V)
Vacuum Range Atmosphere to 30" Hg.* with adequate pump
Vacuum Leak Rate < .2” Hg per 24 hours
Temperature Range Ambient to 200°C
Shelf Capacity 2.0 ft2
Insi e Dimensions 11.125”D x 9.75”W x 9.75”H
Outsi e Dimensions 16”D x 15”W x 20”H
Stan ar Electrical Service 1000 Watts, 120 VAC
50/60 Hz. 8.4 Amps
Optional:
1000 Watts, 240 VAC,
50/60 Hz , 4.2 Amps
Net Weight (Poun s) 65 lb.
*Within 10 Mic ons
3
Performance and Physical Data

1. Power Switch: Applies power to the oven tem-
perature control.
2. Temperature Control: Regulates the oven oper-
ating temperature.
3. Heating ndicator: ndicates when the oven is
being heated.
4. Thermometer: 0° - 200°C dial thermometer with
2° divisions.
5. Vacuum Gauge: ndicates chamber vacuum in
inches of me cu y.
6. Control Valves: Used for evacuating chamber,
controlling vacuum, or for bleeding air and other
gasses into chamber.
4
Controls and ndicators

1. Refer to the packing checklist for the list of
accessories sent with this unit. Make certain
you have all accessories before destroying the
shipping container and packing material. Also
verify that all-packing material and tape has
been removed from inside the oven before oper-
ating.
Packing Checklist
Qty Description
1 Model 280A Vacuum Oven
1 nstruction Manual (PN 102265)
1 Vacuum Grease Tube
2 Shelf Trays
1 Warranty Card
2. Place the oven on a bench or stand at a con-
venient working height. Maintain a minimum of
12 inches of clearance between the oven and
any combustible surfaces.
3. Turn temperature control to low position and
turn power switch off.
4. Check voltage and watts stamped on the data
plate for compatibility before connecting oven to
power source. The data plate can be found
near the power cord.
5. Connect a vacuum pumping system, including a
suitable trap, to the serrated fitting on the valve
designated as vacuum. Use 1/4” D heavy
walled tubing and secure the connection with a
hose clamp.
6. f desired, connect a purge gas supply to the
remaining serrated fitting. Use a two-stage gas
flow regulator if gas is to be supplied by a pres-
surized cylinder.
5
Operation
Note
Recommended vacuum tubing and
vacuum pumps are listed under the
Accessory tems section of this man-
ual.

Temperature Adjustment
1. Turn the power switch on to supply power to the
oven.
2. Turn the Temp. Control knob fully clockwise.
The "Heating" indicator will glow when the unit is
heating. When the temperature reaches the
desired operating level (as indicated on the ther-
mometer) turn the Temp. Control knob counter-
clockwise until the "Heating" indicator turns off.
Allow the temperature to cycle on and off sever-
al times (3 to 4 hours) to make sure the oven
has stabilized. Adjust the Temp. Control knob
up or down as necessary.
3. When temperature is at the desired setting pro-
ceed to operate in any one of the following vac-
uum environments
Operation in a Static
Environment
Static environment refers to operation at atmospheric
pressure and with air, as it is present. n this case the
operator would simply place the sample in the oven
chamber and set the desired temperature.
Operation in a Controlled
Environment
Controlled environment refers to operation with the sam-
ples in an inert gas. To accomplish this, perform the fol-
lowing:
1. Place samples in the oven chamber then close
the oven door.
2. Close the purge control valve.
3. Open the vacuum control valve then turn on the
vacuum pumping system to remove any air
remaining in the oven.
6
OPERATION
Note
When the oven is new and is first
heated, the insulation will become
scorched and some smoke and
burning odor will occur. t is normal
for this condition to last 2 to 3 hours
at high heat.

4. Close the vacuum control valve and open the
purge control valve to bleed in an inert gas.
5. Close the purge control valve.
Operation in a Vacuum
Environment
To operate in a vacuum environment, perform the follow-
ing:
1. Place samples in the oven then close the oven
door.
2. Close both the purge control and vacuum con-
trol valves
3. Turn on the vacuum pumping system then open
the vacuum control valve (fully counterclock-
wise)
4. The vacuum, in inches of mercury, can be
obtained from the vacuum gauge on the top of
the oven.
Vacuum Sealing Agents
• High temperature vacuum grease is often nec-
essary to provide a proper seal at tubing con-
nections, valve connections, door seals, etc.
This is especially important at high vacuums.
Using silicone vacuum grease will damage the
door seal and has restrictions for some types of
materials placed in the oven.
Out Gassing
• The operation of the oven at high temperature
while evacuating the chamber will help drive off
absorbed gasses on the walls and three sur-
faces and facilitate attainment of high vacuums.
7
OPERATION

Safety Precautions
• Before operation, always observe the following
Safety precautions. This unit is not explosion
proof. Do not use in the presence of flammable
or combustible materials; fire or explosion may
result. Unit contains components that may ignite
such materials. Do not place volatile items in the
chamber. Fumes and spillage from acidic solu-
tions cause corrosion of the stainless steel
chamber. Care should be taken to maintain neu-
tral pH at all times.
• Do not operate oven at temperatures above
200° C.
• Do not permit materials of any kind to rest on
top of unit when operating at elevated tempera-
tures.
• Do not touch the oven door particularly the glass
portion, with unprotected hands when operating
at elevated temperatures.
• To prevent overheating unit is equipped with a
safety thermostat that will open at approximately
230°C.
• The oven is equipped with silicone door gas-
kets. Do not use silicone door gaskets or vacu-
um grease when evaporating solvents in the
oven or when using high aniline point oils.
BUNA-N gaskets should be used in applications
when evaporating solvents or when using high
aniline point oils. The interior finish or silicone
gaskets may be damaged by the following:
• BUNA-N gaskets should not be used above 125°C.
8
OPERATION
Diesel oil JP-4 oil
M L-0-5606 Hydraulic Fluids
Butyl Acetate Carbon Tetrachloride
Ethylene Chloride Gasoline
Kerosene Zylene
Methyl Chloride Stoddard Solvent
Toluene Aromatic Chlorinated Solvent

Cleaning Suggestions
• Use the mildest cleaning procedure that will do
the job effectively.
• Rinse thoroughly with water after every cleaning
operation.
• Wipe dry to avoid watermarks.
• A stainless steel wool pad, sponge or fibrous
brush is recommended. Avoid use of ordinary
steel wool or steel brushes for scouring stain-
less steel.
Periodic Maintenance
• Secured access panels, covers, etc., should
never be removed from this equipment by any-
one other then experienced service personnel,
• f the oven fails to maintain set temperature, it
may indicate a problem with the Temp. Control,
or possibly a heating element failure. Contact
your local Fisher Scientific service representa-
tive (1-800-395-5442).
• Gaskets should be checked periodically for
hardening, shrinking, deterioration or other signs
of wear. t is advisable to keep several gaskets
available for use as replacements.
Seal Replacement
To replace the oven seal, remove the old seal and
perform the following:
1. Clean edge of chamber with Xylene, (Cat. No.
LLX5-500).
2. Apply a thin bead of Dow Corning RTV-736 red
silicone rubber adhesive to edge of the cham-
ber. Place gasket on chamber and close the
door.
3. Keep door closed for a minimum of 16 hours
with 1 to 2 inches of vacuum before using.
9
Maintenance and Servicing

Accessory tems
Detailed information on accessory items is located in the
Fisher Scientific catalog.
Item No. Description
01-257-2C Vacuum Pump
01-257-4A Vacuum Pump Oil
01-257-12 Clear Vacuum Tubing
14-635-5D Vacuum Grease
Replacement Parts
Part No. Description
SPN83373 Power Switch
SPN102219 Temp. Control (Thermostat)
SPN20845 Temp. Control Knob
SPN102222 Thermal Cut-Out
SPN98991 Pilot Light
SPN102256 Thermometer
SPN98998 Rubber Feet
SPN102161 Control Valve
SPN102220 Vacuum Gauge
SPN30790 Heating Element (120V)
SPN50430 Door Gasket - Silicone
SPN50430B Door Gasket - BUNA-N
SPN50430V Door Gasket - Viton
SPN02336 Window
When ordering replacement parts, please specify the
model number and serial number of your unit, and date
the unit was purchased. The model and serial numbers
can be found on the nameplate, which is located near the
service cord.
10
Accessories and Replacement Parts

11
Schematics

Laboratory instruments and equipment manufactured by Fisher Scientific Company L.L.C. – Laboratory
Equipment Division (hereinafter called “the Company”) are warranted only as stated below.
Subject to the exceptions and upon the conditions specified below, the Company agrees, at its election, to
correct by repair, by replacement, or by credit to the purchaser, any defect of materials or workmanship which
develops within one year (13 months for refrigerator and freezer products) from the date of purchase by the
original purchaser by the Company or by an authorized dealer of the Company provided that investigation or
factory inspection by the Company discloses that such defect developed under normal and proper use
The exceptions an con itions mentione above are the following:
a. The Company makes no warranty concerning components or accessories not manufactured by it,
such as tubes, batteries, etc. However, in the event of the failure of any component or accessory not
manufactured by the Company, the Company will give reasonable assistance to the purchaser in
obtaining from the respective manufacturer whatever adjustment is reasonable in the light of the
manufacturer’s own warranty.
b. The Company shall be released from all obligations under its warranty in the event repairs or
modifications are made by persons other than its own service personnel or authorized dealer
personnel unless such repairs by others are made with the written consent of the Company.
c. THE COMPANY MAKES NO WARRANTY OF MERCHANTABILITY, FITNESS FOR ANY
PARTICULAR PURPOSE, OR ANY OTHER WARRANTY, EXPRESS OR IMPLIED, EITHER IN
FACT OF BY OPERATION OF LAW,…STATUTORY OR OTHERWISE.
. The above warranty and the above obligations to repair, replace, or credit are complete and
exclusive and the Company expressly disclaims liability for lost profits or for special, indirect,
incidental, consequential, or exemplary damages of any nature whether attributable to contract,
warranty, negligence, strict liability, or otherwise even if the Company has been advised of the
possibility of such damages.
e. Representations and warranties made by any person, including dealers and representatives of the
Company, which are inconsistent or in conflict with the foregoing warranty shall not be binding upon
the Company unless reduced to writing and signed by an officer of the Company.
Warranty