Agilent Technologies 1100 Series User manual

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Agilent 1100 Series
Thermostatted Column
Compartment
Reference Manual
Agilent G1316A COLCOM
Asset # 304025

ii 1100 Series TCC Reference Manual
Notices
© Agilent Technologies, Inc. 2002
No part of this manual may be reproduced in
any form or by any means (including elec-
tronic storage and retrieval or translation
into a foreign language) without prior agree-
ment and written consent from Agilent
Technologies, Inc. as governed by United
States and international copyright laws.
Manual Part Number
G1316-90003
Edition
Edition 07/02
Printed in Germany
Agilent Technologies
Hewlett-Packard-Strasse 8
76337 Waldbronn, Germany
Software Revision
This guide is valid for A.01.xx revisions of
the Agilent 1100 Series Thermostatted Col-
umn Compartment software, where xx
refers to minor revisions of the software
that do not affect the technical accuracy of
this guide.
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CAUTION
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ard. It calls attention to an operat-
ing procedure, practice, or the like
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adhered to, could result in damage
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conditions are fully understood and
met.
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A WARNING notice denotes a
hazard. It calls attention to an
operating procedure, practice, or
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notice until the indicated condi-
tions are fully understood and
met.

1100 Series TCC Reference Manual iii
In This Guide…
1 Installing the Column Compartment
How to install the thermostatted column compartment
2 How to optimize the Column Compartment
An introduction to the column compartment’s optimization
3 Troubleshooting and Test Functions
This chapter describes the instrument’s built in troubleshooting
and test functions.
4 Repairing the Column Compartment
Instructions on how to repair the column compartment
5 Identifying Parts and Materials
Detailed illustrations and listings for parts and materials
identification
6 Introduction to the Column Compartment
An introduction to the column compartment, instrument
overview, theory of operation, external communication and
internal connectors
7 Control Module Sceens for the Agilent 1100 Column Compartment
This chapter is intended to introduce an operator to the screens
available for operation of the Agilent 1100 thermostatted
column compartment (TCC) with the Agilent 1100 control
module.
Please use the manual of control module for further detailed
reference.
8 Specifications
Performance specifications of the thermostatted column
compartment

iv 1100 Series TCC Reference Manual

1100 Series TCC Reference Manual v
Contents
1 Installing the Column Compartment
Site Requirements 2
Physical Specifications 4
Unpacking the Column Compartment 5
Optimizing the Stack Configuration 7
Installing the Column Compartment 9
Flow Connections of the Column Compartment 11
2 How to optimize the Column Compartment
Optimizing the Column Compartment 16
3 Troubleshooting and Test Functions
Overview of the Column Department’s Indicators and Test
Functions 18
Status indicators 19
Power Supply Indicator 20
Instrument Status Indicator 20
Error Messages 21
Timeout 22
Shutdown 23
Remote Timeout 24
Synchronization Lost 25
Leak 26
Leak Sensor Open 27
Leak Sensor Short 28

vi 1100 Series TCC Reference Manual
Compensation Sensor Open 29
Compensation Sensor Short 30
Left Fan Failed 31
Right Fan Failed 32
Open Cover 33
Cover Violation 34
Left Temperature Timeout 35
Right Temperature Timeout 36
Defective Temperature Sensor 37
Heater Profile 38
Valve Failed 39
Column Temperature 40
Heatsink Temperature 41
Defective Heater Circuit 42
Thermostat Function Test 43
Temperature Calibration 45
Temperature Calibration Procedure 46
Calibration Problems 47
Installing the Temperature Sensor 48
4 Repairing the Column Compartment
Introduction into Repairing the Column Compartment 52
Overview of the Repairing the Column Compartment 55
Simple Repairs 56
Changing Column Identification Tags 57
Replacing Head Parts of Column Switching Valve 60
Correcting Leaks 62
Exchanging Internal Parts 63
Removing the Top Cover and Foam 65
Removing the Column Switching Valve 68
Installing the Column Switching Valve 71

1100 Series TCC Reference Manual vii
Exchanging the Column Compartment Main (CCM) Board 74
Replacing the Column Identification Module (CID) Board 78
Exchanging the Fan 79
Removing the Heat Exchanger Assemblies 81
Installing the Heat Exchanger Assemblies 84
Exchanging the Power Supply 87
Replacing the Leak Sensor or Leak Base 90
Replacing Status Light Pipe 95
Installing the Foam and the Top Cover 96
Assembling the Main Cover 99
Replacing the Column Compartment’s Firmware 100
5 Identifying Parts and Materials
Overview of Main Assemblies 102
Control Module 104
Column Switching Valve 105
Sheet Metal Kit 107
Plastic Parts 108
Foam Parts 109
Power and Status Light Pipes 110
Leak Parts 111
Accessory Kit 112
Cable Overview 113
Analog Cables 115
Remote Cables 118
BCD Cables 124
Auxiliary Cable 127
CAN Cable 128
External Contact Cable 129

viii 1100 Series TCC Reference Manual
RS-232C Cable Kit 130
LAN Cables 131
6 Introduction to the Column Compartment
Introduction to the Column Compartment 134
System Overview 135
Column-Identification System 137
Column-Identification Tag 138
Column Clip 139
Column Switching Valve (Optional) 140
Electrical Connections 142
Instrument Layout 144
The Electronics 145
Column Compartment Main Board (CCM) 146
Firmware Description 151
Firmware Updates 151
Agilent 1100 Series Interfaces 153
GPIB Interface 154
CAN Interface 154
Remote Interface 154
RS-232C 155
Setting the 8-bit Configuration Switch 157
GPIB Default Addresses 158
Communication Settings for RS-232C Communication 158
Forced Cold-Start Settings 160
Stay Resident Settings 160
The Main Power Supply Assembly 162

1100 Series TCC Reference Manual ix
7 Control Module Screens for the Agilent 1100 Column Compartment
Major keys on the Agilent 1100 Control Module 166
Screens available from the Analysis screen 167
Screens available from the System screen 176
Screens available from the Records screen 178
Diagnostics and Tests 183
8 Specifications
Performance Specifications 186
ASafetyInformations
General Safety Information 190
Lithium Batteries Information 193
Radio Interference 194
Sound Emission 195
Solvent Information 196
Agilent Technologies on Internet 197
Index

x 1100 Series TCC Reference Manual