Agilent Technologies 1290 infinity User manual

Agilent Technologies
Agilent 1290 Infinity
Thermostatted Column
Compartment
User Manual

1290 Infinity TCC User Manual
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Manual Part Number
G1316-90030
Edition
07/10
Printed in Germany
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1290 Infinity TCC User Manual 3
In This Guide...
In This Guide...
This manual covers the Agilent 1290 Infinity Thermostatted Column
Compartment (TCC) (G1316C).
1 Introduction to the Column Compartment
This chapter gives an introduction to the TCC, instrument overview and
internal connectors.
2 Site Requirements and Specifications
This chapter provides information on environmental requirements, physical
and performance specifications.
3 Installing the Module
This chapter provides information on unpacking, checking on completeness,
stack considerations and installation of the module.
4 How to optimize the Column Compartment
This chapter provides information on how to optimize the Thermostatted
Column Compartment.
5 Troubleshooting and Diagnostics
Overview about the troubleshooting and diagnostic features.
6 Error Information
This chapter describes the meaning of error messages, and provides
information on probable causes and suggested actions how to recover from
error conditions.
7 Test Functions and Calibrations
This chapter describes the TCC’s built in test functions.

4 1290 Infinity TCC User Manual
In This Guide...
8 Maintenance
This chapter describes the maintenance tasks for the TCC. If the instrument
needs repair please contact your Agilent service representative.
9 Parts and Materials for Maintenance
This chapter provides information on parts for maintenance.
10 Identifying Cables
This chapter summarizes information on all cables.
11 Appendix
This chapter provides addition information on safety, legal and web.

1290 Infinity TCC User Manual 5
Contents
Contents
1 Introduction to the Column Compartment 9
Overview of the Module 10
System Overview 11
Column-Identification System 13
Column Switching Valve (Optional) 15
Early Maintenance Feedback 24
Instrument Layout 25
Electrical Connections 26
Interfaces 29
Setting the 8-bit Configuration Switch 34
2 Site Requirements and Specifications 41
Site Requirements 42
Physical Specifications 45
Performance Specifications 46
Extended Specifications on G1316C 47
3 Installing the Module 49
Unpacking the module 50
Optimizing the Stack Configuration 51
Installing the Column Compartment 56
Installing Valve Heads 61
Installation of Heater Devices 64
Flow Connections of the Column Compartment 66
Placing Columns 74
4 How to optimize the Column Compartment 77
Optimizing the Column Compartment 78
Using Additional Heater Devices 79
Delay Volume and Extra-Column Volume 80
How to Configure the Optimum Delay Volume 82
How to Achieve Higher Injection Volumes 83
How to Achieve High Throughput 84

6 1290 Infinity TCC User Manual
Contents
5 Troubleshooting and Diagnostics 87
Overview of the Module’s Indicators and Test Functions 88
Status indicators 89
Available Tests vs User Interfaces 91
Agilent Lab Advisor Software 92
6 Error Information 93
What Are Error Messages 94
General Error Messages 95
TCC Error Messages 100
7 Test Functions and Calibrations 111
Thermostat Function Test 112
Pressure Test 114
Temperature Calibration 115
8 Maintenance 119
Introduction to Maintenance and Repair 120
Cautions and Warnings 121
Overview of Maintenance 123
Cleaning the Column Compartment 124
Changing Column Identification Tags 125
Adding Heater Devices 127
Installing the capillaries 131
Correcting Leaks 141
Replacing Valve Heads 142
Preparing the Thermostatted Column Compartment for Transportation 145
Replacing the Module Firmware 147
9 Parts and Materials for Maintenance 149
Valve Options Overview 150
Heater and Cooling Devices 152
Column Switching Valve 8 Position-9 Port 155
2 pos/6 Port Ultra High Pressure Valve Head 156
2Pos/10Port Ultra High Pressure Valve Head 157
8Pos/9Port Ultra High Pressure Valve Head 158

1290 Infinity TCC User Manual 7
Contents
2pos/6 port valve head 600 bar 159
2pos/10 port valve head 600 bar 160
8pos/9 port valve head 600 bar 161
Accessory Kits 162
10 Identifying Cables 167
Cable Overview 168
Analog cables 170
Remote Cables 172
BCD Cables 175
CAN Cable 177
RS-232 Cable Kit 178
Agilent Module to Printer 179
11 Appendix 181
General Safety Information 182
The Waste Electrical and Electronic Equipment (WEEE) Directive
(2002-96-EC) 185
Lithium Batteries Information 186
Radio Interference 187
Sound Emission 188
Solvent Information 189
Agilent Technologies on Internet 190

8 1290 Infinity TCC User Manual
Contents

9
1290 Infinity TCC User Manual
Agilent Technologies
1
Introduction to the Column
Compartment
Overview of the Module 10
System Overview 11
Column-Identification System 13
Column Switching Valve (Optional) 15
Typical Applications 18
Early Maintenance Feedback 24
Instrument Layout 25
Electrical Connections 26
Serial Number Information 27
Rear view of the module 28
Interfaces 29
Overview Interfaces 30
Setting the 8-bit Configuration Switch 34
Communication Settings for RS-232C 37
Special Settings 39
This chapter gives an introduction to the TCC, instrument overview and internal
connectors.

10 1290 Infinity TCC User Manual
1Introduction to the Column Compartment
Overview of the Module
Overview of the Module
The Agilent 1290 Infinity thermostatted column compartments is a stackable
temperature-controlled column compartment for LC. It is available as
standalone module or as a component of an Agilent 1290 Infinity system. It is
used for heating and cooling to meet extreme requirements of retention time
reproducibility.
The main features of the 1290 Infinity thermostatted column compartment
are:
•Peltier heating and cooling from 10 degrees below ambient up to 100 °C
with high heating and cooling speeds for maximum application flexibility
and stability,
•holds up to three 30 cm columns and optimized design gives minimum dead
volumes and maximum efficiency,
•two independently programmable heat exchangers contribute volumes of
only 3 and 6 µl,
•additional heating devices for low flow rates, which reduce the risk of
additional dispersion,
•it can be supplemented by a kit to install a small heat-exchanger with 1.6 µl
delay volume to reduce the delay volume.
•electronic column-identification module as standard for GLP
documentation of column type, and major column parameters,
•optional high-quality Rheodyne®column switching valves with ceramic
stator-face assemblies for prolonged lifetime.
For specifications, see “Performance Specifications” on page 46.