Agilent Technologies 1200 series User manual

Agilent Technologies
Agilent 1200 Series
Thermostatted Column
Compartment
G1316A/G1316B/G1316C
User Manual
1200 Series TCC User Manual

1200 Series TCC User Manual
Notices
© Agilent Technologies, Inc. 1995,
1996-2008
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Manual Part Number
G1316-90011
Edition
09/2008
Printed in Germany
Agilent Technologies
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76337 Waldbronn
Research Use Only
Not for use in Diagnostic Procedures.
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Manual Structure
The User Manual G1316-90011 (English)
and its localized versions contain a subset
of the Service Manual and is shipped with
the Thermostatted Column Compartment in
printed matter.
Latest versions of the manuals can be
obtained from the Agilent web.

1200 Series TCC User Manual 3
In This Guide…
In This Guide…
This manual covers the Agilent 1200 Series Thermostatted Column
Compartments (TCC)
•G1316A Agilent 1200 Series TCC
•G1316B Agilent 1200 Series TCC SL
•G1316C Agilent 1200 Series TCC SL Plus
1 Introduction to the Column Compartment
This chapter gives an introduction to the TCC, instrument overview and
internal connectors.
3 Installing the Column Compartment
This chapter describes the installation of the Thermostatted Column
Compartment.
4 How to optimize the Column Compartment
This chapter provides information on how to optimize the Thermostatted
Column Compartement.
5 Troubleshooting and Diagnostics
Overview about the troubleshooting and diagnostic features.
6TestFunctions
This chapter describes the TCC’s built in test functions.

4 1200 Series TCC User Manual
In This Guide…
7 Maintenance
This chapter describes the maintenance of the TCC.
8 Parts and Materials for Maintenance
This chapter provides information on parts for maintenance.
9 Appendix
This chapter provides addition information on safety, legal and web.

1200 Series TCC User Manual 5
Contents
Contents
1 Introduction to the Column Compartment 9
Main Features 10
System Overview 11
Column-Identification System 13
Column Switching Valve (Optional for G1316A/G1316B SL) 15
Electrical Connections 18
Instrument Layout 21
Agilent Diagnostic Software 22
2 Site Requirements and Specifications 23
Site Requirements and Specifications 24
Physical Specifications 27
Performance Specifications 28
Extended Specifications on G1316B SL/G1316C SL Plus 30
3 Installing the Column Compartment 33
Unpacking the Column Compartment 34
Optimizing the Stack Configuration 35
Installing the Column Compartment 38
Installing Valve Heads (G1316C SL Plus) 42
Flow Connections of the Column Compartment 44
Installation of Heater and Cooling Devices 47
Placing Columns 49
4 How to optimize the Column Compartment 51
Optimizing the Performance of your Column Compartment 52
Using Additional Heater and Cooling Devices 53

6 1200 Series TCC User Manual
Contents
5 Troubleshooting and Diagnostics 55
Overview of the Column Department’s Indicators and Test Functions 56
Status Indicators 57
Available Tests depending on User Interfaces 59
Agilent Diagnostic Software 60
6TestFunctions 61
Thermostat Function Test 62
Pressure Test 65
Column Thermostat Temperature Calibration 66
7 Maintenance 71
Introduction to Maintenance and Repair 72
Warnings and Cautions 73
Overview of Maintenance 75
Cleaning the Column Compartment 76
Changing Column Identification Tags 77
Replacing Head Parts of Column Switching Valve (G1316A/G1316B SL) 79
Adding Heater and Cooling Devices (G1316B SL/G1316C SL Plus) 82
Correcting Leaks 84
Replacing the Column Compartment’s Firmware 85
Replacing Valve Heads (G1316C SL Plus) 86
Preparing the G1316C SL Plus for Transportation 89
8 Parts and Materials for Maintenance 91
Valve Options Overview 92
Heater and Cooling Devices for G1316B SL/G1316C SL Plus 93
Column Switching Valve 2 Position/6 Port (G1316A/G1316B SL) 95
Column Switching Valve 8 Position-9 Port (G1316C SL Plus) 97
Micro Column Switching Valve 2 Postion/6 Port (G1316A/G1316B SL) 99
Micro Column Switching Valve 2 Position/10 Port (G1316A/G1316B SL) 100
Accessory Kits 102
Plastic Parts 109
Leak Parts 110

1200 Series TCC User Manual 7
Contents
9 Appendix 113
Safety Symbols 114
The Waste Electrical and Electronic Equipment Directive 117
Lithium Batteries Information 118
Radio Interference 119
Sound Emission 120
Solvent Information 121
Agilent Technologies on Internet 123

8 1200 Series TCC User Manual
Contents

9
1200 Series TCC User Manual
Agilent Technologies
1
Introduction to the Column
Compartment
Main Features 10
System Overview 11
Column-Identification System 13
Column Switching Valve (Optional for G1316A/G1316B SL) 15
Electrical Connections 18
Serial Number Information 20
Instrument Layout 21
Agilent Diagnostic Software 22
This chapter gives an introduction to the TCC, instrument overview and
internal connectors.

10 1200 Series TCC User Manual
1Introduction to the Column Compartment
Main Features
Main Features
The Agilent 1200 Series thermostatted column compartments are stackable
temperature-controlled column compartments for LC. They are available as
standalone modules or as a component of a Agilent 1200 Series system. They
are used for heating and cooling to meet extreme requirements of retention
time reproducibility.
The main features are:
•Peltier heating and cooling from 10 degrees below ambient up to
80 °C(G1316A) or 100 °C (G1316B SL/G1316C SL Plus) with high heating
and cooling speeds for maximum application flexibility and stability,
•holds up to three 30-cm columns and optimized design gives minimum dead
volumes and maximum efficiency,
•two independently programmable heat exchangers contribute volumes of
only 3 and 6 µl,
•G1316B SL features additional heating and cooling devices for low flow
rates, which reduce the risk of additional dispersion,
•G1316B SL and G1316C SL Plus can be supplemented by a kit to install a
small heat-exchanger with 1.6 µl delay volume to reduce the delay volume.
In additon a cooling device with 1.5 µl is available,
•electronic column-identification module as standard for GLP
documentation of column type, and major column parameters,
•optional high-quality Rheodyne®column switching valves with ceramic
stator-face assemblies for prolonged lifetime.
For specifications, see “Performance Specifications” on page 28.