Analytik Jena PlasmaQuant PQ 9000 User manual

PlasmaQuant PQ 9000
High-Resolution Array ICP OES
Operating manual

Service:
Analytik Jena AG
Customer Service
Konrad
-Zuse-Str. 1
07745 Jena
Germany
Phone:
Hotline: + 49 (0) 3641 / 77-7407
Fax: + 49 (0) 3641 / 77-7449
E
-mail: [e-mail]
General information about Analytik Jena AG
on the internet: http://www.analytik-jena.de
Copyrights and trademarks
PlasmaQuant is a registered trademark of Analytik Jena AG.
Microsoft, Windows 7, MS Excel are registered trademarks of Microsoft Corp.
The identification with ® or TM is omitted in this manual.
Documentation number: 13-5850-002-23
Edition – May 2014
Implementation of the Technical Documentation:
Analytik Jena AG
© Copyright 2014, Analytik Jena AG

Contents
PlasmaQuant PQ 9000 Edition 05/2014 1
Contents
1Basic information 7
1.1 User manual notes ..................................................................................................7
1.2 Intended use ...........................................................................................................7
1.3 Warranty and liability...............................................................................................8
2Safety instructions 9
2.1 General notes..........................................................................................................9
2.2 Symbols and signal words used .............................................................................9
2.3 Safety markings on the PlasmaQuant PQ 9000 .....................................................9
2.4 Requirements for the operating personnel ...........................................................10
2.5 Safety instructions, transport and commissioning ................................................11
2.6 Safety instructions - operation ..............................................................................11
2.6.1 General .................................................................................................................11
2.6.2 Safety instructions relating to ambient conditions.................................................11
2.6.3 Safety instructions - electrical equipment .............................................................11
2.6.4 Hazards caused by plasma operation ..................................................................12
2.6.5 Behavior in case of ring plasmas ..........................................................................13
2.6.6 Safety instructions relating to the formation of ozone and toxic vapors ...............13
2.6.7 Safety instructions relating to compressed gas containers and systems .............13
2.6.8 Handling of samples, auxiliary and operating materials .......................................14
2.6.9 Safety instructions relating to cleaning and decontamination measures in
case of biological contamination ...........................................................................14
2.6.10 Safety instructions - maintenance and repair .......................................................15
2.7 Behavior during emergencies ...............................................................................15
3Specification 16
3.1 Technical data.......................................................................................................16
3.1.1 PlasmaQuant PQ 9000 data .................................................................................16
3.1.2 Control computer data ..........................................................................................18
3.1.3 Cooling system data .............................................................................................18
3.1.4 Automatic sampler data ........................................................................................18
3.2 Guidelines and standards .....................................................................................19
4Installation conditions 20
4.1 Environmental conditions......................................................................................20
4.2 Energy supply .......................................................................................................20
4.3 Gas supply ............................................................................................................21
4.4 Exhaust unit ..........................................................................................................22
4.5 Recirculating chiller...............................................................................................22
4.6 Device layout and space requirements.................................................................23

Contents
2 Edition 05/2014 PlasmaQuant PQ 9000
5Function and setup of the PlasmaQuant PQ 9000 25
5.1 Physical functional principle of ICP-OES ..............................................................25
5.2 Setup of the PlasmaQuant PQ 9000 ....................................................................25
5.3 Automatic sampler ................................................................................................29
6Installation and commissioning 30
6.1 Supply and control connections ............................................................................30
6.2 Connections in the plasma compartment and in the sampling compartment.......33
6.3 Installing the PlasmaQuant PQ 9000....................................................................34
6.4 Connecting the PlasmaQuant PQ 9000................................................................34
6.4.1 Installation of the torch, nebulizer with spray chamber and sample supply .........34
6.4.2 Initial operation of the automatic sampler .............................................................37
7Operation 40
7.1 Switching on the PlasmaQuant PQ 9000 and igniting the plasma .......................40
7.2 Switching off the PlasmaQuant PQ 9000 .............................................................41
7.3 Using the plasma deactivation switch in the event of faults .................................42
7.4 Starting a measurement routine............................................................................42
8Maintenance and care 44
8.1 Maintenance intervals ...........................................................................................45
8.2 Base device maintenance.....................................................................................46
8.2.1 Cleaning the demountable torch ...........................................................................46
8.2.2 Replacing the torch body ......................................................................................48
8.2.3 Cleaning the one-piece torch ................................................................................50
8.2.4 Cleaning the nebulizer ..........................................................................................52
8.2.5 Cleaning the sampling compartment and the plasma compartment ....................53
8.2.6 Replacing pump hoses .........................................................................................53
8.2.7 Changing the plasma compartment windows .......................................................53
8.2.8 Checking the gas system for leaks .......................................................................56
8.2.9 Changing fuses .....................................................................................................57
8.2.10 Replacing the air filter of the PQ 9000 ..................................................................58
8.3 Maintenance of the automatic sampler.................................................................59
8.3.1 Replacing the cannula and the sample hose........................................................59
8.3.2 Replacing the pump hose .....................................................................................59
8.3.3 Clean-up after cup overflow ..................................................................................60
8.3.4 Replacing the fuses ..............................................................................................60
8.4 Maintenance of the recirculating chiller ................................................................61
8.4.1 Cleaning the dust filter ..........................................................................................61
8.4.2 Cleaning the foam sieve .......................................................................................61
8.4.3 Changing the cooling water ..................................................................................61

Contents
PlasmaQuant PQ 9000 Edition 05/2014 3
9Fault removal 63
9.1 Fault removal ........................................................................................................63
9.2 Equipment faults and analytical problems ............................................................66
10 Transport and storage 70
10.1 Preparing the PlasmaQuant PQ 9000 for transport..............................................70
10.2 Ambient conditions for transport and storage .......................................................71
10.3 Recommissioning after transport or storage.........................................................71
10.4 Installing the recirculating chiller ...........................................................................72
11 Index 73

Figures
4 Edition 05/2014 PlasmaQuant PQ 9000
Figures
Figure 1 Dimensions of the PlasmaQuant PQ 9000 - front view..................................... 24
Figure 2 Dimensions of the PlasmaQuant PQ 9000 - top view ....................................... 24
Figure 3 Sampling compartment and plasma compartment in the
PlasmaQuant PQ 9000 ...................................................................................... 26
Figure 4 Concentric nebulizer and spray chamber ......................................................... 27
Figure 5 Schematic structure of the torch with gas flows .............................................. 27
Figure 6 Demountable torch ........................................................................................... 28
Figure 7 One-piece torch................................................................................................. 28
Figure 8 Automatic sampler............................................................................................ 29
Figure 9 Overview of connections on the left side of the device.................................... 30
Figure 10 Interfaces and fuses on the PlasmaQuant PQ 9000.......................................... 31
Figure 11 Connections for cooling water and gases ......................................................... 31
Figure 12 Plug-in connectors for gas connections ............................................................ 31
Figure 13 Ventilation openings and air filter on the rear of the PlasmaQuant PQ 9000.. 32
Figure 14 Data on the type plate ...................................................................................... 32
Figure 15 Serial number of the device in the plasma compartment ................................ 32
Figure 16 Plasma compartment ........................................................................................ 33
Figure 17 Sampling compartment with torch holder, spray chamber, nebulizer and
hose pump......................................................................................................... 33
Figure 18 Automatic sampler - overview .......................................................................... 37
Figure 19 Connections on the right side of the automatic sampler ................................. 37
Figure 20 Nebulizer cleaning tool with installed nebulizer............................................... 52
Figure 21 Plug-in connectors for gas connections ............................................................ 56
Figure 22 Gas distribution during pure argon operation .................................................. 57
Figure 23 Automatic sampler cannula and sample hose dismantled ............................... 59
Figure24 Automatic sampler pump.................................................................................. 60

Summaries
PlasmaQuant PQ 9000 Edition 05/2014 5
Summaries
Summary 1 Environmental conditions for operation........................................................... 20
Summary 2 Power supply..................................................................................................... 21
Summary 3 Gas supply ......................................................................................................... 21
Summary 4 Exhaust unit requirements................................................................................ 22
Summary 5 Cooling circuit requirements............................................................................. 22

Summaries
6 Edition 05/2014 PlasmaQuant PQ 9000

Basic information
PlasmaQuant PQ 9000 Edition 05/2014 7
1 Basic information
1.1 User manual notes
The PlasmaQuant PQ 9000 is intended for operation by qualified specialist personnel observing
this user manual.
The user manual informs about the design and function of the PlasmaQuant PQ 9000 and
provides the necessary know-how for the safe handling of the device and its components to
personnel familiar with analysis. The user manual further includes notes on the maintenance
and service of the equipment and potential causes and remedies of any faults.
Conventions
Instructions for actions which occur in chronological order are numbered and combined in
action units.
Lists which are not in chronological order are shown as itemized lists, sub-listings as bullet
points.
Safety notes are indicated by pictogaphs and signal words. The type and source of the danger
are stated together with notes on preventing the danger. The meaning of the pictographs and
signal words used is explained in the chapter "Safety notes".
The elements of the control and analysis program are indicated as follows:
Program terms are identified with SMALL CAPS (e.g., Menu FILE).
Buttons are shown by square brackets (e.g., [OK] button)
Menu items are separated by arrows (e.g., FILE OPEN).
1.2 Intended use
The ICP Emission Spectrometer (ICP-OES) PlasmaQuant PQ 9000 is used in a chemical
analysis laboratory for the analysis of liquid - mainly aqueous - samples to determine the
concentrations of up to 75 elements up to the trace range.
The PlasmaQuant PQ 9000 may only be used for the measurement solutions described in this
user manual. Additional modules also allow for the analysis of gaseous substances or solids
(e.g., laser ablation). Any other use is not as intended! The operator is exclusively liable for any
damages as a result.
The PlasmaQuant PQ is not suitable for solutions containing hydrofluoric acid if the nebulizer or
spray chamber are made of glass or quartz. Use hydrofluoric acid-resistant components for this
purpose. Special provisions must be made for operations involving organic solvents. In addition
to apparatus-related and methodical aspects, fire and health protection for the particular organic
solvent must be observed here.

Basic information
8 Edition 05/2014 PlasmaQuant PQ 9000
1.3 Warranty and liability
The warranty and liability periods comply with the legal requirements and the provisions in the
General Terms and Conditions of Analytik Jena AG.
Deviations from the intended use described in this user manual will result in limitations of
warranty and liability in the event of damage. Damage to wearing parts or breakage of glass are
not included in the warranty.
Warranty and liability claims are excluded for personal injury and property damage if resulting
from one or several of the following causes:
use of the PlasmaQuant PQ 9000 other than intended
improper commissioning, operation and servicing of the device
modifications to the equipment without prior consultation with Analytik Jena AG
operation of the device with faulty safety equipment or improperly fitted safety and
protection equipment
inadequate monitoring of the equipment components subject to wear
use of other than original spare parts, wearing parts or consumables
improper repairs
faults due to the non-observance of this user manual

Safety instructions
PlasmaQuant PQ 9000 Edition 05/2014 9
2 Safety instructions
2.1 General notes
For your own safety and to ensure error-free and safe operation of the PlasmaQuant PQ 9000,
please read this chapter carefully before using the appliance.
Observe all safety notes listed in this user manual and all messages and notes displayed by the
control and analysis program on the monitor.
Besides the safety instructions in this user manual and the local safety regulations that apply to
the operation of the device, the general applicable regulations regarding accident prevention,
occupational health and safety and environmental protection have to be observed and complied
with.
References to potential dangers do not replace the work protection regulations which must be
observed.
2.2 Symbols and signal words used
The user manual uses the following symbols and signal words to indicate hazards or
instructions. The safety instructions are always placed before an action.
WARNING
Indicates a potentially hazardous situation which might cause fatal or very serious injuries
(deformities).
CAUTION
Indicates a potentially hazardous situation which might cause light or minor injuries.
ATTENTION
Indicates a potentially hazardous situation which might cause damage to property.
IMPORTANT
Indicates application hints and other especially useful information without any resulting
hazardous or damaging situations.
2.3 Safety markings on the PlasmaQuant PQ 9000
Warnings and notice symbols have been attached to the PlasmaQuant PQ 9000 which must
always be observed.
Damaged or missing warning and notice symbols can cause incorrect actions leading to
personal injury or material damage! The symbol labels must not be removed! Damaged symbol
labels must be replaced without delay!

Safety instructions
10 Edition 05/2014 PlasmaQuant PQ 9000
Warning
symbol
Meaning Remark
Warning of a hazard
location
−At the extractor device:
Warning of optical radiation. If no exhaust
air hose is connected, it is possible to look
indirectly (by mirror) into the radiation of
the plasma.
−At the sampling compartment:
Warning of moving parts; warning of hot
torch
−At the plasma compartment:
Warning of hot surfaces.
−At the power inlet:
Caution when connecting the media
(gases, cooling water and power)
Warning of a hot surface −At the plasma compartment:
Warning of hot surfaces. Immediately after
extinguishing the plasma, the surface of
the plasma compartment and in particular
the torch and the plasma chamber window
components and the induction coil are hot.
There is a risk of getting burnt!
Notice symbol Meaning Remark
Observe the operating
manual
−At the power switch:
Before starting work, read the operating
manual.
Before opening the
device, always
disconnect the mains
plug
−On the side wall at the power inlet:
Before opening the device cover, switch
off the device and disconnect the mains
plug from the mains socket.
The following notice sign is attached to the rear of the PlasmaQuant PQ 9000:
2.4 Requirements for the operating personnel
The PlasmaQuant PQ 9000 must only be operated by qualified specialist personnel instructed
in the use of the device. The instruction must also include conveying the content of this user
manual and the user manuals of other system components.
In addition to the safety at work instructions in this user manual, the generally applicable safety
and accident prevention regulations of the respective country of operation must be observed
and adhered to. The operator must ascertain the latest version of these regulations.

Safety instructions
PlasmaQuant PQ 9000 Edition 05/2014 11
The user manual must be accessible to the operating and service personnel at all times!
2.5 Safety instructions, transport and commissioning
Observe the following notes:
The PlasmaQuant PQ 9000 is always installed by the service engineers of Analytik Jena
AG or its authorized and trained specialist personnel. Independent assembly and
installation are not permitted. Incorrect installation can create serious hazards.
The device weighs 170 kg. Use a lift truck to transport the device.
Four people are required to move the device in the laboratory by holding the device on four
firmly screwed-in carrying handles.
2.6 Safety instructions - operation
2.6.1 General
Observe the following notes:
The operator of the PlasmaQuant PQ 9000 must make sure before each commissioning
that the condition of the device including its safety equipment is sound. This applies in
particular after each modification to or extension of the device or its repair.
The device may only be operated if all protective equipment (e.g., covers and doors) are in
place, properly installed and fully operational. The sound condition of the protection and
safety equipment must be checked regularly. Any defects must be corrected as soon as
they occur. Protective and safety equipment must never be removed, modified or
decommissioned during operation.
During operation, free access to the connections, the power switch and the manual plasma
deactivation switch on the left housing wall must always be ensured.
The ventilation equipment on the device must be in good working condition. Covered vents
or ventilation slits etc. may cause the device to break down or may cause damage to it.
Caution when handing quartz glass and glass parts. Risk of broken glass and therefore risk
of injury!
2.6.2 Safety instructions relating to ambient conditions
Explosion protection
The PlasmaQuant PQ 9000 must not be operated in explosion-hazard areas. Smoking or
open flames in the operating room of the PlasmaQuant PQ 9000 are prohibited! Keep all
combustible materials away from the device.
2.6.3 Safety instructions - electrical equipment
Work on the electrical components of the PlasmaQuant PQ 9000 may only be performed by a
qualified electrical technician according to applicable electro-technical regulations. Lethal
voltages may occur in the device! Contact with live components may cause death, serious injury
or painful electrical shock.
Observe the following notes:

Safety instructions
12 Edition 05/2014 PlasmaQuant PQ 9000
The mains plug must be connected to a proper CEE power socket to ensure that the
device meets protection class I (ground connector). It may only be connected to power
sources whose nominal voltage is the same as that on the type plate of the equipment. The
protective effect must not be invalidated by the use of an extension line which does not
have a protective conductor (→section "Energy supply" p.20).
The PlasmaQuant PQ 9000 and its system components must always be switched off
before being connected to the mains.
Before opening the device, it must be switched off at the device switch and the mains
connector must be disconnected from the mains outlet! Any work on the electronics
(behind the device enclosure) may only be carried out by the service engineers of Analytik
Jena AG and specially authorized technicians.
2.6.4 Hazards caused by plasma operation
Plasma is extremely hot (up to 10,000 K) and it emits electromagnetic and UV radiation. The
induction coil is operated with 1500 V RMS and 40.68 MHz. High-frequency radiation and UV
radiation can cause serious injuries to skin and eyes. Contact with the torch (plasma torch)
shortly after operation will cause skin burns. An electrical discharge may also occur across
larger distances and cause fatal injuries, electrical shock and skin injuries.
Observe the following notes:
To ensure safe torch operation, you must not ignite the plasma unless the following
conditions are met:
−The plasma compartment door is closed.
−The torch is in working position.
−Sufficient cooling is supplied.
−The extractor device is connected and switched on.
−Argon supply is ensured.
Note: The above mentioned components are backed up by hardware safety circuits.
Unless the reliable functioning of these components is guaranteed, the plasma will not be
ignited or it will be extinguished automatically if a component reports a malfunction.
The safety circuits must not be bridged.
Before opening the plasma compartment door, extinguish the plasma in the ASpect PQ
program. To do this, click on the button in the program toolbar.
Wait for the compartment to cool down for at least 5 min and avoid touching any hot parts
of the torch and its environment immediately after extinguishing the plasma.

Safety instructions
PlasmaQuant PQ 9000 Edition 05/2014 13
2.6.5 Behavior in case of ring plasmas
The manual plasma deactivation switch is located on the left-hand side of the device (red).
In the following situations, press the deactivation switch without delay to prevent the torch
from melting:
−The plasma produces loud noises (rattles).
−The shape of the plasma changes considerably and a shining ring is visible on the
inside of the coil.
−Torch parts begin to glow.
2.6.6 Safety instructions relating to the formation of ozone and toxic vapors
The interaction between the UV radiation from the torch and the surrounding air results in the
formation of a high concentration of toxic gases such as ozone and nitrogen oxides.
Additionally, toxic byproducts may escape from the samples and during sample processing.
Observe the following notes:
The PlasmaQuant PQ 9000 may only be operated with an active exhaust unit.
The exhaust unit must be switched on before igniting the plasma.
2.6.7 Safety instructions relating to compressed gas containers and systems
Observe the following notes:
Argon is taken from compressed gas containers or local liquid gas systems. The required
purity of the gases must be ensured.
Work on compressed gas containers and systems must only be carried out by individuals
with specialist knowledge and experience in compressed gas systems.
For compressed gas container or gas plant operation, the safety instructions and
guidelines which are valid at the operating location must be strictly complied with.
High pressure hoses and pressure reducers may only be used for the assigned gases.
All pipes, hoses and screw connections must be checked weekly for leaks and externally
visible damage. Possible pressure losses from closed systems and lines under pressure
must be determined. Leaks and damaged must be repaired without delay.
The gas supply must be closed prior to servicing and repairs!
After successful repair and servicing of the components of the compressed air containers
or system, the device must be checked for sound operation prior to recommissioning!
Independent assembly and installation are not permitted!

Safety instructions
14 Edition 05/2014 PlasmaQuant PQ 9000
2.6.8 Handling of samples, auxiliary and operating materials
Observe the following notes:
The operator is responsible for the selection of substances used in the process as well as
for their safe handling. This is particularly important for radioactive, infectious, poisonous,
corrosive, combustible, explosive and otherwise dangerous substances.
When handling dangerous substances, local safety codes and guidelines must be
observed.
Warnings on the labels must always be observed. Only use clearly marked containers as
well as protective goggles and rubber gloves. Use suitable body protection (coat, safety
glasses and rubber gloves) when handling samples. Ensure sufficient ventilation.
Cleaning with hydrofluoric acid must be carried out in an exhaust chamber. When
handling hydrofluoric acid, rubber aprons, gloves and face masks must be worn.
Biological samples must be handled according to local guidelines regarding the handling
of infectious material.
When measuring material containing cyanide, you have to make sure that prussic acid
cannot be generated in the waste bottle, i.e., the waste solution must not be acidic.
Ensure that all residue liquid from the nebulizer and the automatic sampler is directed into
the waste bottle supplied.
The operator is responsible for ensuring that waste materials such as drained coolant and
residue liquid from the waste bottle are disposed of in an environmentally responsible
manner and according to local regulations.
Examples of dangerous organic solvents
Methyl isobutyl ketone (MIBK)
Flammable, highly volatile, noxious-smelling
Toluene
Flammable, hazardous to health
Kerosene
Flammable, hazardous to the aquatic environment,
hazardous to health
Methanol, ethanol, propanol
Flammable, partly acutely toxic
Tetrahydrofuran (THF)
Flammable, hazardous to health, extremely volatile,
dissolves polyethylene and polystyrene
This list is in so far incomplete that other solvents could also come into consideration for use in
the PlasmaQuant PQ 9000. In cases of uncertainty about an unnamed fluid, this may only be
used when the manufacturer has confirmed that there is no danger to safety.
2.6.9 Safety instructions relating to cleaning and decontamination measures in
case of biological contamination
Observe the following notes:
The operator is responsible for carrying out suitable decontamination should the device be
contaminated externally or internally with dangerous substances.
Spots, drops or larger spillages should be removed and cleaned using an absorbent
material such as cotton wool, laboratory wipes or cellulose. The affected areas must then
be wiped with an Incidin Plus solution.
Before using a cleaning or decontamination procedure other than that prescribed by the
manufacturer, the user is required to check with the manufacturer that the intended
procedure will not damage the device. Safety labels attached to the PlasmaQuant PQ 9000
must not be wetted by methanol.

Safety instructions
PlasmaQuant PQ 9000 Edition 05/2014 15
2.6.10 Safety instructions - maintenance and repair
Observe the following notes:
The PlasmaQuant PQ 9000 is always serviced by the service engineers of Analytik Jena
AG or its authorized and trained specialist personnel. Independent servicing can maladjust
or damage the device. Therefore, the operator may only carry out the tasks listed in the
chapter "Service and care".
The exterior of the PlasmaQuant PQ 9000 may only be cleaned with a damp, not dripping,
cloth. Use only water and, if required, commercial surfactants.
For cleaning the sampling compartment and transport channels (hose system) of the
PlasmaQuant PQ 9000 the operator is responsible for establishing appropriate safety
precautions – particularly in terms of contaminated and infectious materials.
2.7 Behavior during emergencies
Observe the following notes:
If there is no immediate danger of injury, you must extinguish the plasma immediately by
using the deactivation switch in case of danger or accidents.
If possible, switch off the device at the power switch after allowing a cooling down period of
30 s. Then disconnect the mains plugs of the device and the system components from their
power sockets!
Close the gas supply as soon as possible after switching off the devices.

Specification
16 Edition 05/2014 PlasmaQuant PQ 9000
3 Specification
3.1 Technical data
3.1.1 PlasmaQuant PQ 9000 data
Optical system
Monochromator Echelle grating double-monochromator with a focal length of F=380 mm and variable
gap; pre-monochromator with quartz prism, wavelength selection via additional
reflected neon radiator
Wavelength range 160 – 900 nm
Wavelength accuracy < 0.4 pm
Spectral resolution 0.002 nm at 2 nm
Grating Mechanically ruled grating, 79 grooves/mm, blaze angle of 74°r
Optical bank
encapsulation
photometer
Optics in modular construction on compact cast base plate for stability and
endurance;
protection against moisture, exhaust fumes and chemical environmental impacts
Detector Two-dimensional FFT backside illuminated CCD with high quantum efficiency and
increased UV sensitivity
Display modes
Emission Counts (ct)
Intensity Counts/seconds (ct/s)
Concentration Value range: 5 characters (0.0001 to 99999), unit freely selectable
Signal evaluation
Spectrally resolved Specters of 20 pixels to a maximum of 200 pixels in width
Power supply
Supply voltage
Frequency
230 V ±10%
50/60 Hz
Mains fuse installation in the
building
35 A
Typical average power
consumption
Base device: 4500 VA
Overvoltage category II according to DIN EN 61010-1
Degree of contamination 2 according to DIN EN 61010-1
Protection class I
Protection type IP 20

Specification
PlasmaQuant PQ 9000 Edition 05/2014 17
Instrument fuses
Fuse number Type Protected circuit
S1 10 A NFC 10x38 gG AC 400 V Spectrometer
S2 6 A NFC 10x38 gG AC 400 V Tubular heating generator
S3 25 A NFC 10x38 gG AC 400 V Power supply unit generator
Safety circuits
Monitoring of Plasma compartment door closure
Torch working position
Cooling
Waste air
Argon supply
Plasma (optical monitoring)
Gas supply
Recommended gas Inlet pressure Consumption
Argon 4.8 or superior
Permitted components:
Oxygen ≤ 3 ppm
Nitrogen ≤ 10 ppm
Hydrocarbons ≤ 0.5 ppm
Humidity ≤ 5 ppm
6 bar (5 – 7 bar) 13 L/min
Additive gas (optional)
Oxygen 4.5 or superior
6 bar (5 – 7 bar) 0.02 L/min
Environmental conditions
According to DIN ISO 9022-2:2003/01
Corrosion protection The device is corrosion-proof against the samples used in the analysis
Operating temperature +15°C to +35°C, at best +20°C to +25°C
as constant as possible during measuring
Humidity 20 to 90% at 20°C
Storage Temperature: -40°C to +70°C
Use desiccant
Dimensions and weights
Mass 170 kg
Dimensions (WxDxH) 987 mm x 853 mm x 937 mm
Analytic data
Type of sample Liquid
Type of nebulizer Concentric nebulizer
Spray chamber Cyclone chamber

Specification
18 Edition 05/2014 PlasmaQuant PQ 9000
3.1.2 Control computer data
Computer
(minimum requirements)
PC Pentium 1 GHz with 512 MB RAM
Hard disk with 40 GB,
43 cm color monitor (17")
VGA graphic card
Resolution 800x600 pixels or higher
CD-ROM drive
Ports:
2 x USB port (USB 2.0 Highspeed)
USB cable length shorter than 3 m
Mouse
Operating system Windows 7 Professional or later
3.1.3 Cooling system data
Tank capacity 4.2 L
Dimensions (height x width x depth) 576 mm x 368 mm x 702 mm
Supply voltage
Frequency
100 - 240 V AC
50/60 Hz
Cooling performance 3 000 W
Mass (empty) 89 kg
3.1.4 Automatic sampler data
Dimensions H x W x D 510 mm x 285 mm x 490 mm
Mass 15 kg
Supply voltage
Frequency
100 - 240 V AC
50/60 Hz
Fuse 5 A
Typical average power consumption 75 VA
Racks
Sample cups
3 for sample cups
2 for special cups
Wash bottle 2 L