EYELA FDS-1000 User manual

取扱説明書
Freeze dryer
Model FDS-1000
R00
Instruction Manual
This instruction manual is designed to use the product safely with keeping its best
performance.
Please keep this manual in a place easily accessible to every users.
IMPORTANT Be sure to read “Safety precautions” before use.
Tokyo Rikakikai Co., Ltd.
（230V）

IMPORTANT SAFETY INFORMATION
1. Warning signal word
Attempting to carelessly operate the product or to
touch the portion not-specified may result in
unexpected injury.
Most of such accidents can be prevented if such
danger is known beforehand.
To ensure the safety, this manual defines the
information on such matters as requiring particular
care in the safety as follows in terms of the
importance and risk and attaches the alert mark and
signal word.
It is recommended to follow the instruction to ensure
the safe use of the product.
We have undertaken thorough verification concerning the possible occurrence of risk in the
course of use of the product, but prediction of all and every kind of risk is extremely difficult.
Namely, cautions contained in this manual are not necessarily all of possible risks.
However, if the product is operated according to the procedure described in this manual, the
safe operation and work is ensured. Be sure to pay utmost care during handling of the product
to prevent accident or failure of the product.
Alert mark
Signal word Definition
Wrong handling is assumed to cause the possibility of the death
or heavy injury of the user.
Wrong handling is assumed to cause the risk of injury of the
operator or physical damages.
Warning
Caution

Leak filter
No. Nomenclature Quantity
1 Main body 1
2 Trap barrier 1
3 Leak filter 1
4 Tube 1
5Tube（spare）1
6 Connector 1
7Operation manual 1
8Guarantee 1
Tube
Tube (spare)
Trap barrier
1 For safe operations
2. Product Outline
2 - 1 Application
2 - 2 Specification
2 - 3 Sublimation rate data（reference）
2 - 4 Optional parts
2 - 5 Name of parts
3. Name and Functions of Parts
3 - 1 Control panel
3 - 2 Safety Functions
4. Installation
4 - 1 Installation environment
4 - 2 Installation conditions
4 - 3 Connecting the utilities
1
2
2
3
4
7
8
11
13
13
14
5. Operation
5 - 1 Preparation
5 - 2 Operation method
6. Troubleshooting Guide
7. Maintenance and Inspection
7 - 1 Replacing the consumables
7 - 2 Operation test of the leak breaker
7 - 3 Oil control of vacuum pump
Replacing the cartridge
7 - 4 Cleaning and care of the product
8. Disposal of Product
9. After-sale Services
10. Optional Products
15
20
29
32
33
33
34
35
36
37
Thank you for purchasing our product.
Introduction
This instruction manual explains
installation, operation, troubleshooting,
maintenance and inspection, and discarding
procedures for the Freeze dryer FDS-1000.
Always read this manual before use to
ensure familiarization of the product.
Contents
Be sure to confirm the kinds and quantities of parts before starting installation.
Package Contents
Connector

Be very careful when drying flammable substances, such organic
solvent, etc.
Solvent that cannot be trapped may be drawn by the vacuum pump,
possibly causing ignition and explosion
Take utmost care when drying the sample containing
flammable substances, such as organic solvent, etc.
Warning
- 1 -
●Carry out prior freezing of sample container.
●Change oil of the vacuum pump periodically.
1For safe operations
This product is not explosion-proof. Be sure to take extreme care for safety during
operation.
Caution Do not touch the cooling fin with bare hand during maintenance work. The
cooling fan is keen and may cut your hand.
Do not touch the cooling fin with bare hands.
Cooling fin

- 2 -
※1.The performance shown is at the ambient temperature of 20℃and at no load.
※2.The power input shown is the value not including the capacity of service outlet.
This product is applicable to drying of the
diluted aqueous solution of protein, enzyme, etc.
or drying of the extracted solution of biologic
sample or biotic sample (urine, blood serum, etc.).
Product name Freeze dryer
Model FDS-1000
Cooling method Can body cooling
Perfor-
mance
Trap cooling temperature ※1 -80℃
Dehumidification rate 150mL/one batch
Function
Setting and display function Sheet key input and digital display
Safety function Leak/overcurrent breaker, circuit protector for socket outlet, refrigerator self-diagnosis
function, control board self-diagnosis function
Vacuum releasing function Automatic vacuum leak valve
Trap deicing function Deicing by the can body heater
Other functions Automatic vacuum pump operation, display of automatic vacuum pump operation time, stopwatch function, freeze-drying ready display, selection of power recovery,
monitoring of vacuum abnormality, monitoring of trap temperature
Compo-
sition
Temperature sensor Ｔtype thermocouple sensor
Refrigerator, refrigerant Stirling refrigerator, helium（non-CFC)
Defrosting heater Silicon rubber heater, 60W
Standard
Vacuum pump (required
displacement) Option: 50L/min or more
Vacuum gauge
Pirani vacuum indicator：Digital display（0.0～533Pa）
Display accuracy at 0.4～4.0Pa ±2.0 Pa
at 4.1～10.0Pa ±3.0 Pa
at 10.1～15.0Pa ±4.0 Pa
at 15.1～40.0Pa ±7.0 Pa
Trap size (mm)・material Φ90×145（about 0.85L)・SUS304
Vacuum pump connection port
(mm) Outside diameter 17 （Rear side of main body）
Service socket Max.5A for both vacuum pump and driver chamber
Operating ambient temperature range 5～35℃
Outside dimensions (mm)（excluding
projection)）455W×220D×497H
Weight About 19kg
Power input/rated power ※20.9A 200VA・AC230V 50Hz
2Product Outline
2-1 Application
Never attempt to modify the product.
Operate the unit for the specified
purpose only.
An electric shock or a malfunction may result if the
product is modified or used for any purposes other
than that specified.
Warning
2-2 Specification

2-3 Sublimation rate data（reference）
・After prior freezing of four 100 mL sample (egg-plant shaped) flasks, each filled with 38g of water (a total
of 152g), they were installed to the trap. The sublimation rate was calculated back from the residue of flasks
after the time had passed.
Conditions ・AC230V,50Hz
・Ambient temperature 20℃
Sublimation
rate（ｇ）
■Model FDS-1000
・The sublimation rate differs depending on the use conditions, such as the room temperature, capacity
and shape of sample containers (egg-plant shaped flask, freeze-drying bottle), type and amount of
samples, the degree of prior-freezing of samples.
・When the ambient temperature is 35℃, install one 100mL sample (egg-plant shaped) flask filled
with 40 g (max) of water (after prior freezing).
As the time passes, the trap time and the degree of vacuum decrease. When they decrease below the
set value, install the similarly-prepared container to he remaining adaptor.
0
10
20
30
40
50
60
70
80
90
100
110
120
130
140
150
160
0 1 2 3 4 5 6 7 8 9 10
Evaporation (g)
Time（h）
- 3 -

2-4 Optional parts
■Cock Ｃ,test tube, ampoule, etc.
①22
④
⑤
⑥③
② ⑦
⑧
⑨
⑩ ⑮
⑪⑫
⑬
⑭
⑯
⑰
⑱
⑲
⑳
22
※① The cock C belongs to the manifold. Prepare other adapters separately according to the intended use.
- 4 -

No. Name Standard Quantity Code No.
1 Cock C FD-1000,PMS-4S/4A（manifold for FDS-1000）1 191140
2 Adapter for ampoule For φ8 1 120520
For 6 1 120530
3 Ampoule Egg-plant shaped（1ml）20 120210
Pencil shaped with round bottom（1ml）20 120220
Pencil shaped with flat bottom（1ml）20 120221
Flat bottom（2ml）20 120230
Flat bottom（5ml）20 120240
Flat bottom（10ml）20 120250
Round bottom （2ml）20 120260
Round bottom （5ml）20 120270
Round bottom （10ml）20 120280
4 Type B adapter for test tube 1 120510
5 Sealing 1 145610
6 Rimmed test tube φ10×75（3ml）100 143970
φ12×75（4ml）100 143980
φ12×90（5ml）100 143990
φ12×105（6ml）100 144000
φ12×120（7ml）100 144010
φ13×75（5ml）100 144020
φ13×90（6ml）100 144030
φ13×100（7ml）100 144040
φ15×85（8ml）100 144050
φ15×105（10ml）100 144060
φ15×150（15ml）50 144070
φ16.5×105（12ml）100 144080
φ16.5×165（20ml）50 144090
φ18×165（24ml）50 144100
φ18×180（27ml）50 144110
φ21×200（42ml）50 144120
7 Type C adapter for flask Taper size 29 1 191120
8 Sample flask For 50ml, taper size 29 1 116040
For 100ml, taper size 29 1 116150
9 Type C adapter for freezing bottle 1 191130
10 Cap (for freeze-drying Φ45, （for 40ml and 80ml）1 120020
11 Filter holder 1 120100
12 Filter 100 pieces/box 1 120110
13 Freeze-drying bottle 40ml （φ45）1 120050
80ml （φ45）1 120060
14 Freeze-drying bottle set 40ml 1 119940
80ml 1 119950
- 5 -

No. Name Standard Quantity Code No.
15 Cap （for freeze-drying bottle）φ70、（for 120ml, 150ml, 300ml）1 120030
16 Micro-tube holder 1.5ml×12 micro-tubes installed 1 191110
17 Freeze-drying bottle 150ml、φ70 1 120130
18 Freeze-drying bottle set Bottle：150ml、φ70 / cap：φ70 1 119970
19 Micro-tube holder 1.5ml×24 micro-tubes installed 1 191150
20 Freeze-drying bottle 300ml、φ70 1 120140
21 Freeze-drying bottle set Bottle：300ml、φ70 / cap：φ70 1 119980
22 Air filter 1 187450
■Drip box for egg-plant shaped flask Code No. 263490
The drip box receives drips of thawed frost adhering to the container outside when 50ml and 100ml flaks are used.
This is made from stainless steel and can be cleaned with ease.
- 6 -