Shimadzu MOC63u User manual

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Moisture Analyzer
Instruction Manual
MOC63u
321-78013A
MAR.2013
Checking Package Contents P.24
Names and
Functions of Parts P.25
Installation P.32
Preparing for Measurement P.38
Menu P.42
Measuring Moisture Content P.44
Aborting Measurement P.48
After Measurement P.49
Turning Power Off P.50
Setting Measuring Conditions P.52
Changing Moisture Analyzer
Settings P.63
Calibrating Moisture Analyzer P.73
When Connecting MOC63u
to Peripheral Devices P.78
Using Windows
Direct Function P.79
Control Moisture Analyzer
from PC P.85
Printer Output (Option) P.91
Maintenance of
Moisture Analyzer P.98
Replacing Heater P.102
Replacing Fuses P.104
Clearing Measurement
Data from Memory P.105
Initializing Moisture Analyzer
Settings P.106
Inspection P.107
Troubleshooting Guide P.110
When Required P.113
BEFORE MEASUREMENT MEASURE DETAILED
MEASUREMENT
CONNECTION TO
PERIPHERALS
MAINTENANCE
TROUBLESHOOTING GUIDE
AND OTHER INFORMATION

2
Requests
If you lend or transfer this product to others, attach this instruction manual to the product.
If you lose or damage this instruction manual, contact your Shimadzu sales representative immediately.
Remarks
The information in this instruction manual is subject to change without notice for the purpose of
improvement.
All information in this instruction manual has been carefully veried to ensure its accuracy. Any errors
or missing information, should any be found, may not be corrected immediately.
Shimadzu Corporation (the Company) owns the copyright to this instruction manual. Neither part nor the
entirety of this document may be transferred or reproduced without the prior written permission of the
Company.
© 2010-2013 Shimadzu Corporation. All rights reserved.
Microsoft, Windows, and Excel are the registered trademarks of Microsoft Corporation. All other
company names and product names in this document are the trademarks and registered trademarks of
their respective owners. The symbol that represents the trademark or ® is not used in this document.
Company names, organization names, product names, etc. in this document are the trademarks or
registered trademarks of their respective owners.
The Company does not guarantee that Windows Direct Function can run normally on all personal
computers. The Company is not responsible for any problems caused by this function.
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Introduction
Thank you for choosing the MOC63u, Shimadzu Moisture Analyzer.
Shimadzu Corporation, with more than 90 years experience in manufacturing high
precision balances, is condent in the high quality of the MOC63u moisture analyzer.
The MOC63u provides prompt and accurate measurement of moisture contents. With
the full adoption of UniBloc
®
cell, which we started to use for electronic balances
in 1989, the MOC63u also features improved reliability. The cross key dedicated to
menu manipulation has improved the operability of the MOC63u, making it easier to
use.
The MOC63u is also equipped with the Windows Direct Function that can transmit
measurement results to a PC without requiring any software to be installed, as well
as other various functions that users can use conveniently according to their aims.
To make full use of the performance and functions of the MOC63u moisture
analyzer, please read this instruction manual carefully, and follow the usage
instructions. Please keep this instruction manual with the product, so that you can
refer to the manual at anytime necessary.
You can download the instruction manual (PDF format) from our web site
(http://www.shimadzu.com/an/balance/index.html).
For information on the following points, please contact your Shimadzu Balance
representative.
Product warranty
After service
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4
What You Can Do
You can search the usage instructions for information about functions you want to try or learn about by aim.
nI want to measure moisture content!
Measuring Moisture Content page 44
nI want to set measuring conditions in detail!
Setting Measuring Conditions page 52
nI want to measure data easily!
Standard Drying Automatic Ending Mode page 53
nI want to measure data by setting the time!
Standard Drying Timed Ending Mode page 55
nI want to measure samples that change largely with
heat!
Slow Drying Mode page 58
nI want to measure liquid samples!
Rapid Drying Mode page 56
nI want to measure the amount of change in moisture
content at different temperatures!
Stepped Drying Mode page 60
Various
measuring
methods
nI want to measure data accurately with the moisture
analyzer!
Calibrating Moisture Analyzer page 73
nI want to span calibration of the moisture analyzer!
Span calibration page 73
nI want to calibrate the temperature of the moisture
analyzer!
Calibrating the Temperature (*1) page 73
For accurate
measurements
(*1) The temperature calibration kit (option) is required.

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nI want to transfer the measured data to PC
(Excel, etc.)!
Using Windows Direct Function page 79
nI want to set the ID for each moisture analyzer unit to
control several units!
Setting the Moisture Analyzer ID page 72
nI want to set sample codes for the moisture analyzer
to control samples!
Setting Sample Codes page 67
nI want to set the date and time for the moisture
analyzer to control the measurement date and time!
Setting the Date and Time page 68
nI want to print out measurement results!
Printing Stored Measurement Data page 93
nI want to print out the settings!
Outputting the Moisture Analyzer Settings from a Printer page 94
Outputting
measurement
results and
settings
nI want to switch types of values to be referenced for
measurement!
Setting the Measurement Standard page 63
nI want to restrict menu items to be displayed!
Restricting the Menu Display page 69
nI want to set the password!
Setting the Password page 70
nI want to clear measurement data from memory!
Clearing Measurement Data from Memory page 105
nI want restore the default settings of the moisture
analyzer!
Initializing Moisture Analyzer Settings page 106
Others

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Safety Notes Be sure to follow the safety guidelines
To use the moisture analyzer safely and properly, carefully read and observe the following safety guidelines.
The levels of danger and damage that will arise if the moisture analyzer is used incorrectly are
classied and indicated as shown below.
! WARNING
Indicates a potentially hazardous
situation which, if not avoided,
could result in serious injury or
possibly death.
! CAUTION
Indicates a potentially hazardous
situation which, if not avoided,
may result in minor to moderate
injury or equipment damage.
Precautions are classied and explained by using one of the symbols below, depending on the nature
of the precaution.
Instructions
Indicates an action that must be
performed.
Prohibitions
Indicates an action that must
NOT be performed
!WARNING
Prohibitions
Do not use the moisture
analyzer and peripherals
(Connected PC or Printer)
outdoors or in a location where
it can be splashed with water.
Doing so may result in an electric
shock or lead to abnormal operation.
Prohibitions
Never disassemble, remodel, or repair this
product and accessories.
Doing so may result in an electric shock or lead to
abnormal operation.
If you believe the moisture analyzer may be
malfunctioning, contact an authorized Shimadzu
representative.
Instructions
Use the moisture analyzer with the specified power source and in the specified
voltage environment.
Using the moisture analyzer with an inappropriate power source or voltage level may result in re or malfunction.
Also note that the optimal performance may not be achieved when power source or voltage is unstable, or power
capacity is insufcient.
Instructions
Ground the product.
To prevent electric shock and to maintain stability in operation of the product, be sure to ground the product.
The product will be grounded when its power plug is inserted into a 3-wired power socket equipped with a ground
terminal.

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!WARNING
Prohibitions
Do not attempt to measure samples
that may undergo dangerous chemical
reactions when heated.
Doing so may result in an explosion or release of toxic gas.
Prohibitions
Do not place anything on
top of the heater cover.
Doing so may result in re.
Prohibitions
Do not place flammable
materials near the moisture
analyzer.
Some parts of the moisture analyzer
become extremely hot during
operation and could cause a re
if ammable materials are placed
nearby.
!CAUTION
Prohibitions
Do not place any non-heat
resistant objects near the
moisture analyzer.
Some parts of the moisture analyzer
become extremely hot during
operation and could lead to damage
or deformation of non-heat resistant
objects.
Prohibitions
Do not touch the heat-dispersing
component of the heater cover or sample
pan with your bare hands during and
immediately after measurement.
Doing so may result in burn injury.
This moisture analyzer is extremely hot during and
immediately after measurement.
When touching the moisture analyzer, only use the
specied control knobs and accessories.

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!CAUTION
Prohibitions
Do not use the moisture analyzer in
the following locations:
Doing so may result in a malfunction.
Where there is an air ow (near an air-
conditioner, air vent, door, window, etc.)
Where temperatures change markedly
Where vibrations occur
In an area exposed to direct sunlight
Where corrosive or inammable gases are
present
Where dust, electromagnetic waves, or
magnetic elds are present
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Instructions
Handle the moisture analyzer carefully.
The moisture analyzer is a precision device. Subjecting
it to impact may result in a malfunction.
When moving the moisture analyzer main unit, securely
hold it with both your hands.
If long-term storage is required, use the original
package box to pack the product.
Instructions
Place the moisture analyzer
on a rigid, stable, and flat
table, or on the floor in the
room.
Placing the moisture analyzer on an
unstable surface may cause personal
injury or a malfunction.
Secure a sufcient space for your
measurement work in consideration
of the total weight of measuring
objects and the moisture analyzer
loaded on the installation location.
Instructions
After a power failure, turn
the power switch on.
If a power failure occurs, the power is
automatically turned off. See "Turning
the Power On" (^ Page 38) to
restore operation.
Prohibitions
Do not use the moisture
analyzer as a proof of
transaction.
The law does not allow the moisture
analyzer to be used for proof
of transaction such as medical
preparation.
Instructions
If an abnormal situation occurs (for
example, a burning odor is smelt), remove
the power cable immediately.
If you continue operating the device in an abnormal
situation, re or electric shock may result.
Prohibitions
Only connect peripherals that have been
specified by us to the connector of the
moisture analyzer.
Connecting other peripherals may cause abnormal
operation.
To prevent problems, be sure to connect peripherals
using the procedure specied in this instruction
manual.

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Precautions
The moisture analyzer includes a heater that heats samples to dry them off during measurement. The heater
becomes hotter than the preset heating temperature. Incorrect handling may cause re, explosion, burn
injury, or other injury. To ensure your safety during measurements, carefully read this section along with
"Safety Notes", (^page 6) and follow the guidelines outlining correct operation procedures.
Samples
The samples measured with the MOC63u moisture analyzer are heated during the measurement. Measuring
hazardous samples may lead to burn injuries or re.
!CAUTION
Prohibitions
Do not measure the following hazardous samples.
Samples in which the characteristics are unknown.
Measuring hazardous samples may lead to burn injuries or re.
Any sample whose surface hardens or solidies by heating, causing high inner pressure.
Such a sample may burst.
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Prohibitions
Do not use the moisture analyzer only to dry a sample.
The moisture analyzer is for measuring the moisture level of a sample, and should not be used
for any other purposes.
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Instructions
Measure samples within the safety range.
Use the moisture analyzer only for measurements that vaporize moisture by heating.
Set the drying temperature within the safe temperature range of each sample.
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Environment for Measurements
!CAUTION
Prohibitions
Do not place flammable objects near the moisture analyzer.
Instructions
If lightning is expected to strike, turn the power off and disconnect
power cable.
^ "Turning Power Off", page 50
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Handling the Moisture Analyzer During and Immediately after
Measurement
!CAUTION
Instructions
Install the parts correctly
Install the sample pan and pan supporter correctly.
^"Installing Parts", page 35
Prohibitions
Do not touch the sample pan and surrounding parts with bare hands
during or immediately after measurement.
The sample pan and surrounding parts become extremely hot immediately after measurement.
Be sufciently careful so as not to suffer a burn injury.
Be sure to use the Sample pan handler when removing the sample pan.
Never touch any metal parts of the heater or surrounding parts when removing the sample
pan. Otherwise, burn injuries may result.
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Parts that Become Hot During and Immediately after Measurement
!CAUTION
Prohibitions
Do not touch the shaded areas during and immediately after
measurement.
The shaded areas in the following gure become extremely hot. Only touch the round marks
when operating.
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Additional Notes
!CAUTION
Instructions
When the device will not be used for a long period of time, turn the
power off and disconnect the power cable.
^"Turning Power Off", page 50
Instructions
After a power failure, turn the power switch on.
If a power failure occurs, the power is automatically turned off. Turn the power switch off once,
then turn it on again.
^"Turning Power Off", page 50
^"Turning the Power On", page 38
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Warning labels on device
! WARNING
Caution. Hot
Do not touch the black grill or the observation window on the upper part of the heater cover. Doing so may result in
a burn injury.
Warning labels
! WARNING
Caution. Hot
Start your operation only after heated parts have completely cooled down. Doing so may result in a burn injury.
Preventing measurement of flammable materials
Do not measure ammable materials.
Warning labels

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! WARNING
Caution. High voltage
Pull out the power cable from a receptacle when changing the heater. Otherwise, you may receive an electric shock.
Warning labels
* When the glass case is removed

14
Indication on the display panel
The instruction manual describes the indication on the display panel corresponding to each
operating procedure.
The operations of the display panel (ashing, lighting up, and conrmation) are indicated as
follows:
Flashing•Lighting up•Confirmation•
! ! !0.0!0!0
/
/
/
/
/
/
/
/
/
/
/
/
/
/
! ! !0.0!0!0 ! ! !0.0!0!0
u
How to Search for Desired Items
There are various methods you can use to search for the function or operation you want to learn about in this
instruction manual.
"Cover Page Index" You can search for the item on the cover page of the instruction manual.
"What You Can Do", page 4 You can search for the item based on what you want to do.
"Menu Map", page 115 You can quickly search the menu item for the function or procedure you
want to use.
"Table of Contents", page 20 You can search for the item in the instruction manual’s table of contents.
"Index", page 118 You can search for the item using a previously-known name or keyword.
Notation for menu manipulations
In the instruction manual, some menu manipulations are indicated using simplied symbols.
Example:
Press in the standby state to
select the menu item
Information shown
on the display
Press to move to the
next item in the menu
Menu manipulation
flow
Select the numeric
value or setting
User's operation or
supplement
Press to accept the
setting or selected item
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Sample page (The following is a sample page to show the layout of this document. The content does
not provide actual operations.)
u
Continued on next page
The following appears on the top of the
next page.
Linked to the cover page index (right pages only) Index
Depiction of the display
The title of the previous page
is shown.
Notes
The following information
will help you to use the
device correctly.
Explanation of terms
Describe terms used for
MOC63u.
Menu operation
Reference

16
After-Sales Service
If this product does not operate normally, follow the guidelines in "Troubleshooting Guide" (^ P. 110) to
analyze and manage the problem.
If the problem still persists, or a symptom occurs presumably caused by another failure, contact our service
representative (details on back cover).
Supply of Parts
Repair parts for this product shall be kept for a period of seven years after this product is discontinued.
Please note that, after the above-mentioned period, a requested spare part may not be able to be supplied.
As exceptions, non-genuine repair parts shall be supplied during the period determined by the relevant
manufacturer.

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Action for Environment (WEEE)
To all user of Shimadzu equipment in the European Union:
Equipment marked with this symbol indicates that it was sold on or after 13th August 2005,
which means it should not be disposed of with general household waste. Note that our equipment
is for industrial/professional use only.
Contact Shimadzu service representative when the equipment has reached the
end of its life.
They will advise you regarding the equipment take-back.
With your co-operation we are aiming to reduce contamination
from waste electronic and electrical equipment and preserve natural
resource through re-use and recycling.
Do not hesitate to ask Shimadzu service representative, if you require
further information.
WEEE Mark

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