Agilent Technologies G2570A GC/MSD Owner's manual

Installation and
Operation Differences
G2570A GC/MSD
System

© Copyright 2000, Agilent
Technologies Company
All Rights Reserved.
Reproduction, adaptation, or
translation without prior
written permission is
prohibited, except as allowed
under the copyright laws.
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are registered trademarks of
Microsoft Corporation.
Document History
Publication number
G2589-90008
First edition, 1/00
Printed in USA
Warranty
The information contained in
this document is subject to
change without notice.
Agilent Technologies makes no
warranty of any kind with
regard to this material,
including, but not limited to,
the implied warranties of
merchantability and fitness for
a particular purpose.
Agilent Technologies shall not
be liable for errors contained
herein or for incidental or
consequential damages in
connection with the
furnishing, performance, or
use of this material.
Agilent Technologies assumes
no responsibility for the use or
reliability of its software on
equipment that is not
furnished by Agilent
Technologies.
Noise Declaration
Deutsch
LpA << 70 dB am Arbeitsplatz
normaler Betrieb nach EN
27779:1991
English
LpA << 70 dB operator
position normal operation per
ISO 7779:1988
System Identification
Each of the following main
components in the G2570A
GC/MSD system is identified
by a unique 10-character serial
number:
MSD-Ready 6850A GC
Right side of the unit, lower
left corner
G2629A Control Module
Back side of the unit, near
center
G2577A Diffusion Pump MSD
Left side of the unit, lower
right corner
Computer
Varies per model
Computer Monitor
Back side of the unit, near
center
G1701CA MSD Productivity
software
Registration number in
Software Certificate and
Registration Packet
Manual Conventions
Cautions
Cautions call attention to
procedures which, if not
correctly performed or
adhered to, could result in
damage to the instrument.
Warnings
Warnings call attention to
procedures which, if not
correctly performed or
adhered to, could result in
personal injury.
Part Numbers
In this manual, Agilent
Technologies part numbers
are generally listed in
parentheses after the name of
the part. Most part numbers
are either four-digit-by-four-
digit (1234-1234) numbers or
five-digit-by-five-digit (12345-
12345) numbers.
Safety Information
Safety Symbols
(on equipment)
Safety class
The 5973N Mass Selective
Detector (MSD) is a Safety
Class I instrument and has
been designed and tested in
accordance with IEC
Publication 1010-1 Safety
Requirements for Electrical
Equipment for Measurement,
Control, and Laboratory Use.
WA R N IN G
Connecting the system to a
power source which is not
equipped with a protective
earth contact creates a shock
hazard for the operator and
can damage the instruments.
Likewise, interrupting the
protective conductor inside or
outside the system or
disconnecting the protective
earth terminal creates a shock
hazard for the operator and
can damage the instruments.
WARNING
Make sure that only fuses with
the required current rating
and of the specified type are
used for replacement. The use
of incorrect or makeshift fuses
or the short-circuiting of fuse
holders creates a shock hazard
for the operator and can
damage the instrument.
WARNING
Any adjustment, maintenance
or repair of the opened
instrument while it is
connected to a power source
should be avoided if possible
and, if required, should be
carried out only by trained
persons who are aware of the
hazards involved.
Safety Information is
continued on the inside of the
back cover.
;Refer to operating
instructions
=Indicates hazardous
voltage
+Indicates hot surface
3Indicates earth
(ground) terminal

3
Table of Contents
Chapter 1 Introduction, 5
About this Manual, 6
Description of G2570A GC/MSD System, 7
Installation and Operation Implications for the G2570A GC/MSD System, 10
Chapter 2 Hardware Installation (Differences), 11
Purpose of Installation, 12
Customer Responsibilities, 13
Installing the GC, 15
Reconfiguring the Column Outlet, 20
Installing the Column Inlet, 25
Preparing to Condition the Column, 27
Conditioning the Column and Inlet System, 30
Preparing the MSD for Installation, 31
Connecting the MSD and the GC, 32
Installing the Column in the GC/MSD Interface, 34
Installing the ChemStation Hardware, 38
Installing the MSD Productivity Software, 39
Verifying EI Scan System Performance, 40
Installation Checklist, 45
Customer Familiarization Checklist, 54
Chapter 3 Operational Differences, 59
Introduction, 60
Installing GC columns, 62
Reconfiguring the Column Outlet, 63
Installing the Column Inlet, 68
Conditioning the column, 71
Venting/pumping down the MSD, 72
Installing the Column in the GC/MS Interface, 73
Creating GC/MSD Methods, 76
Manual injection, 78
Automatic injection, 80

4
Contents
Appendix A Summary of Navigation on 6850A GC Control Module, 85
Appendix B Naming Methods, 89
Appendix C GC Parameters for the PREP_RUN Method, 91
Setup Parameters, 92
Settings Parameters, 93
Automation Parameters, 94
Saving the Method, 95
Appendix D GC Parameters for the OFN_SN Method, 97
Setup Parameters, 98
Settings Parameters, 99
Automation Parameters, 100
Saving the Method, 101

1
Introduction

6
1 Introduction
About this Manual
About this Manual
This manual describes the installation and operation procedures for the G2570A
GC/MSD System that are different than the same activities for the individual
6850A GC and the 5973N MSD components. Successful installation and operation
of the G2570A GC/MSD critically depends upon becoming familiar with
information from the following sources which are included with the G2570A
shipping kits:
• 6850A GC User Information (CD-ROM, Part No. G2630-90220 or newer version)
• 6850A Control Module User Information (CD-ROM, Part No. G2629-90220 or
newer version) and online help
• 6850A GC Multimedia Maintenance (CD-ROM, Part No. G2630-90240 or newer
version)
• 5973Network MSD Hardware Installation Manual (paper, Part No. G2589-
90006)
• G1701CA MSD Productivity ChemStation Software Installation Manual (paper,
Part No. G1701-90039)
• G1701CA MSD Software (CD-ROM, Part No. G1030-60101)
• 5973Network MSD Hardware Manual (Part No. G2589-90001) and online help
• 5973Network MSD Local Control Panel Quick Reference (paper, Part No.
G2589-90011) and online help
• 5973Network MSD Maintenance (CD-ROM, Part No. G1030-60108)
• MSD Reference Collection (CD-ROM, Part No. G1030-60104)
• Relevant 6850A GC accessory (autosampler, valves) manuals/CD-ROM
materials
For updated information, see the Agilent Technologies’ Chemical Analysis Group
website at www.agilent.com/chem.

1 Introduction
Description of G2570A GC/MSD System
7
Description of G2570A GC/MSD System
This section summarizes changes to the sub-systems that make up the G2570A
GC/MSD System.
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8
1 Introduction
Description of G2570A GC/MSD System
6850A GC/ MSD-Ready
This special configuration of the 6850A GC (firmware version A.02.04 or later) is
only available as part of the G2570A GC/MSD System. The gas chromatograph has
been modified as follows:
• The on/off power switch moved to the right side in the lower front corner.
• A hole pre-drilled in the left outer panel, insulation and oven wall to
accommodate the GC- MS interface heater.
• The GC-MS interface heater uses the detector heated zone.
• The Injector Mounting Bracket support relocated on the right side panel.
• The GC is configured only with a split/splitless inlet containing an unpacked,
single taper deactivated liner (Part No. 5181-3316).
• The use of a JetDirect card is NOT supported.
• The GC communicates with the MS only via the APG Start/Stop remote cable
(Part No. G1530-60930).
6850A GC Control Module
The firmware (version E.02.10 or later) of the GC Control Module has been
modified to recognize that the MSD is the only supported detector for the MSD-
Ready 6850A GC.
5973Network MSD
The G2577A diffusion pump EI MSD is the only MSD used in the G2570A system.
ChemStation Hardware and Software
The computer hardware sub-system (applicable PC, monitor, printer, hub, and
LAN cables) supports the use of one MSD. The G1701CA MSD Productivity
software is the same software as is used with other 5973N MSDs.

1 Introduction
Description of G2570A GC/MSD System
9
Supported Accessories
The G2570A GC/MSD system will support the following accessories:
• 7683 ALS Injector (G2613A) controlled by the GC Control Module
• Valving compatible with the standard 6850A GC controlled by the GC Control
Module
• High-Pressure Merlin Microseal (Part No. 5182-3442)
• Ion Gauge Controller (59864B)
Other detectors and other means for introducing samples into the split/splitless
inlet are NOT supported.
Special Parts
The following parts are unique to the G2570A GC/MSD system:
• GC Instrument Base, G2630-00152
• MS Detector Plate (counterweight used in place of GC detector), G2630-20980
• GC Ship Kit, G2630-60201
• GC/MSD Interstitial Panel, G2589-00031
With frequent GC column changes, it is recommended that additional column clips
(G2630-20890) be purchased.

10
1 Introduction
Installation and Operation Implications for the G2570A GC/MSD System
Installation and Operation Implications for the G2570A
GC/MSD System
The following table summarizes how the differences described above translate into
installation and operation differences between the G2570A GC/MSD system and
6890 Plus/5973N GC/MSD systems:
Differences Implications
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2
Hardware Installation (Differences)

12
2 Hardware Installation (Differences)
Purpose of Installation
Purpose of Installation
The purpose of installation is to ensure that instruments and systems are correctly
installed and functioning as designed, in the customer’s facility. Correct
installation is the first step in ensuring that instruments and systems operate
reliably over their expected lifetimes. An Agilent Technologies service
representative must perform the installation. This chapter details the
installation differences for the sub-systems. The following documents contain
the basic installation procedures:
•Setting up your 6850 Quick Reference Guide (Part No. G2630-90230)
• 5973Network MSD Hardware Installation Manual (Part No. G2589-90006)
• Relevant 6850A GC accessory (autosampler, valves) manuals

2 Hardware Installation (Differences)
Customer Responsibilities
13
Customer Responsibilities
The customer should ensure that the installation site is prepared in accordance
with the specifications contained in the following documents:
• 5973Network MSD Site Preparation Manual (Part No. G2589-90010)
•Site Prep Summary as part of the 6850A User Information Manual
(Part No. G2630-90220)
• G2570A GC/MSD System Site Preparation Addendum (Part No. G2589-90040)
A customer representative should be present at all times during the installation.
The G2570A GC/MSD System is shipped in the following boxes:
• 6850A GC - MSD-Ready
• 6850A Control Module
• 5973Network MSD
• Rough pump for MSD
• PC hardware.
Unpack and verify the contents of each container in the presence of an Agilent
Technologies representative.
Check serial numbers and fill in installation documentation S/N fields if necessary.
• Check voltage settings of the instruments and computer systems.
• Verify that power cables are correct (must mate with power receptacles).
• Verify line voltage is correct and the correct line voltage is delivered.
Description Serial Number
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14
2 Hardware Installation (Differences)
Customer Responsibilities
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2 Hardware Installation (Differences)
Installing the GC
15
Installing the GC
1 Place the GC on the bench
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16
2 Hardware Installation (Differences)
Installing the GC
2After connecting and purging the copper tubing sections and helium gas purifier
with the UPC/Zero Grade Helium carrier gas (see 5973N Hardware Installation
Manual for details), attach the carrier gas line to the fitting marked "carrier gas"
at the rear of the GC.
If space permits, it is suggested that the Helium gas purifier be attached with the
purifier clamp to the rear portion of the right side panel.
3 Set the pressure to approximately 50 psi (345 KPa)
Make sure all connections are tight, including the septum retainer nut, liner insert
weldment nut and the inlet column nut containing the ferrule plug
Note The 6850 GC does not ship with a column attached to the inlet.

2 Hardware Installation (Differences)
Installing the GC
17
4 Connect the Control Module to the connector below the GC Display and
Keypad.
5 Connect the APG start/stop cable to the "Remote" connector on the back
of the GC.

18
2 Hardware Installation (Differences)
Installing the GC
6 Connect the power cord to the GC and to the appropriate wall socket.
7 Turn on the power switch to the GC (located on the lower front corner of
the right panel).
8 Using the Control Module, run the Inlet and Keyboard Tests.
You must become comfortable using the G2629A GC control module, especially
entering values in screen fields and navigating through and between screens. See
Appendix Afor a summary of control module screens.

2 Hardware Installation (Differences)
Installing the GC
19
9 Display the Diagnostics screen via the Status/Service/Diagnostics path.
Detector Test key is inactive when the MSD is the detector.
10 Choose the Inlet Test key (F3 key).
The 6850A GC is shipped from the factory with an inlet nut containing a blank
ferrule; the Leak Test and Split Vent Test is based on having a blank ferrule
installed in the inlet. If you are running these tests after using the system,
remember to re-install the blank ferrule before proceeding.
11 From the Inlet Test screen, perform the Leak Test (F8 key) and then
perform the Split Vent Test diagnostics (F7 key), following the
instructions for both tests.
Correct any inlet problems resulting from these tests before continuing.
12 Run the Keyboard Test (F5 key in the Diagnostics screen) after successful
completion of the Inlet Test diagnostics pass.
13 Turn off the power to the GC.

20
2 Hardware Installation (Differences)
Reconfiguring the Column Outlet
Reconfiguring the Column Outlet
The following suggested column installation procedure is based on the column
label facing the user and positioned approximately at the top (12 o’clock position)
of the column cage holder. With this configuration the inlet and outlet ends of the
column remain the same as when a GC detector is used and the column outlet is
positioned at the back (closer to the fan) of the column cage holder.
1 Lay the column (19091S-433E found in the GC ship kit) on a clean surface
with the column label facing the user in the 12 o’clock position.
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