Fritsch PULVERISETTE 0 User manual

VIBRATORY MICRO MILL
PULVERISETTE 0
Operating instructions
Valid starting with: 00.6020/215
Read the instructions prior to performing any task!
Translation of the original operating instructions

Version 12/2014 Index 006
Fritsch GmbH
Milling and Sizing
Industriestraße 8
D - 55743 Idar-Oberstein
Telephone: [phone]
Fax: [phone]
email: [email protected]
Internet: www.fritsch.de

Certifications and CE conformity
Fritsch GmbH has been certified by the TÜV-Zertifizierungsgemeinschaft
e.V.
An audit certified that Fritsch GmbH conforms to the requirements of
the DIN EN ISO 9001:2008.
The enclosed Conformity Declaration lists the guidelines the FRITSCH
instrument conforms to, to be able to bear the CE mark.
Certification
CE Conformity
Certifications and CE conformity
- 3 -

Table of contents
1Basic structure............................................................................... 7
2 Safety information and use........................................................... 8
2.1 Requirements for the user..................................................... 8
2.2 Scope of application............................................................... 8
2.2.1 Operating principle............................................................. 9
2.2.2 Amplitude control............................................................... 9
2.3 Obligations of the operator................................................... 9
2.4 Information on hazards and symbols used in this manual.. 10
2.5 Device safety information.................................................... 13
2.6 Protective equipment.......................................................... 14
2.7 Hazardous points................................................................. 14
2.8 Electrical safety.................................................................... 14
2.8.1 General information......................................................... 14
2.8.2 Protection against restart................................................. 14
2.8.3 Overload protection.......................................................... 15
3 Technical data.............................................................................. 16
3.1 Dimensions.......................................................................... 16
3.2 Weight.................................................................................. 16
3.3 Operating noise.................................................................... 16
3.4 Voltage................................................................................. 16
3.5 Current consumption........................................................... 16
3.6 Power consumption............................................................. 16
3.7 Electrical fuses..................................................................... 17
3.8 Load..................................................................................... 17
3.9 Material................................................................................ 17
3.10 Final fineness of a grinding process with the PULVERI-
SETTE 0............................................................................... 17
4 Installation................................................................................... 18
4.1 Transport............................................................................. 18
4.2 Unpacking............................................................................ 18
4.3 Setting up............................................................................. 18
4.4 Ambient conditions.............................................................. 19
4.5 Electrical connection............................................................ 19
4.5.1 Adjusting the mains voltage.............................................. 20
5 Initial start-up.............................................................................. 21
5.1 Switching on......................................................................... 21
5.2 Function check..................................................................... 21
5.3 Switching off........................................................................ 21
6 Using the device........................................................................... 22
6.1 Conducting a grinding operation......................................... 22
Table of contents
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6.1.1 Parameters........................................................................ 22
6.1.2 Fitting and clamping the mortar....................................... 22
6.1.3 Grinding with liquid nitrogen............................................ 23
6.2 Setting the grinding duration............................................... 24
6.3 Setting the amplitude.......................................................... 25
6.3.1 Displaying the amplitude.................................................. 25
7 Accessories................................................................................... 26
7.1 Sound absorption hood....................................................... 26
7.2 Conversion to Vibratory Sieve Shaker ANALYSETTE 3
SPARTAN.............................................................................. 26
7.2.1 Conducting a sieve analysis............................................... 26
7.2.1.1 Sieve mesh widths that can be used.............................. 26
7.2.1.2 Fitting and clamping the sieves...................................... 26
7.2.1.3 Multiple sieving.............................................................. 28
7.2.1.4 Feed quantity for dry or wet sieving.............................. 28
7.2.2 Dry sieving......................................................................... 29
7.2.2.1 Sieving parameters........................................................ 29
7.2.2.2 Sieving aids..................................................................... 29
7.2.3 Wet sieving....................................................................... 30
7.2.3.1 Sieving parameters........................................................ 30
7.2.3.2 Wetting agents............................................................... 30
7.2.3.3 Feeding the rinsing liquid............................................... 31
7.2.3.4 Extracting the passing particles..................................... 31
7.2.3.5 Tips for wet sieving of difficult sieving stock................. 32
7.2.4 Cleaning the test sieves (mesh wire sieves)...................... 32
7.2.5 Setting the sieving time.................................................... 33
7.2.6 Einstellung und Anzeige der Amplitude............................ 33
7.2.7 TorqueMaster for easy clamping of the sieve set............. 34
7.2.7.1 Fitting the TorqueMaster clamping device.................... 34
7.2.7.2 Clamping the TorqueMaster.......................................... 35
7.2.7.3 Releasing the TorqueMaster.......................................... 37
7.2.7.4 TorqueMaster malfunctions.......................................... 37
7.2.7.5 Compatibility.................................................................. 37
7.2.7.6 Maintenance of the TorqueMaster clamping device..... 38
8 Cleaning........................................................................................ 39
8.1 Cleaning the device.............................................................. 39
8.2 Cleaning grinding elements................................................. 39
9 Maintenance................................................................................ 41
10 Repairs......................................................................................... 42
10.1 Checklist for troubleshooting............................................. 42
11 Disposal........................................................................................ 43
12 Guarantee terms.......................................................................... 44
Table of contents
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13 Exclusion of liability..................................................................... 46
14 Safety logbook............................................................................. 48
15 Index............................................................................................. 50
Table of contents
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1 Basic structure
The PULVERISETTE 0 is equivalent in design to the ANALY‐
SETTE 3 SPARTAN, except that the ANALYSETTE 3 SPARTAN,
like the PRO version, also uses a sieve set.
1 Lid (also used in the ANALYSETTE 3 as a clamping lid
for the 100 mm test sieves)
2 Mortar with grinding ball
3 Vibratory plate
4 Knurled knob
5 Toothed belt
6 Belt clamping device
7 Control panel
Basic structure
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2 Safety information and use
2.1 Requirements for the user
This operating manual is intended for persons assigned with operating
and monitoring the Fritsch of the PULVERISETTE 0. The operating manual
and especially its safety instructions are to be observed by all persons
working on or with this device. In addition, the applicable rules and regu-
lations for accident prevention at the installation site are to be observed.
Always keep the operating manual at the installation site of the of the
PULVERISETTE 0.
People with health problems or under the influence of medication,
drugs, alcohol or exhaustion must not operate this device.
The of the PULVERISETTE 0 may only be operated by authorised persons
and serviced or repaired by trained specialists. All commissioning, main-
tenance and repair work may only be carried out by technically qualified
personnel. Qualified personnel are persons who, because of their educa-
tion, experience and training as well as their knowledge of relevant
standards, regulations, accident prevention guidelines and operating
conditions, are authorised by those responsible for the safety of the
machine to carry out the required work and are able to recognize and
avoid possible hazards as defined for skilled workers in IEC 364.
In order to prevent hazards to users, follow the instructions in this
manual.
Malfunctions that impair the safety of persons, the of the PULVERISETTE
0 or other material property must be rectified immediately. The fol-
lowing information serves both the personal safety of operating per-
sonnel as well as the safety of the products described and any devices
connected to them: All maintenance and repair work may only be per-
formed by technically qualified personnel.
This operating manual is not a complete technical description. Only the
details required for operation and maintaining usability are described.
Fritsch has prepared and reviewed this operating manual with the
greatest care. However, no guarantee is made for its completeness or
accuracy.
Subject to technical modifications.
2.2 Scope of application
The "Vibratory Micro Mill PULVERISETTE 0" is used for the fine comminu-
tion of dry laboratory sample material or suspensions. It is used for
homogenising emulsions or pastes.
Safety information and use
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2.2.1 Operating principle
The plastic housing contains a solid cast structure with an electronically
controlled electromagnet. Three permanently flexible flat springs carry
the pole plate of this magnet together with the vibratory plate, which is
fastened to it. When the magnet is switched on, the pole plate and vibra-
tory plate are attracted and spring back when it is switched off. The cast
structure and magnet on one side and the pole plate, vibratory plate and
sieves on the other side form a vibratory system.
The different weights of the mortar material or grinding balls change the
natural frequency of the vibratory system. For this reason, it is not
always possible to set the amplitude of the micro mill optimally e.g. with
a constant 50 Hz mains frequency present. The processor-controlled
electronics of the PULVERISETTE 0 micro mill ensure a precisely adjust-
able, reproducible oscillation amplitude. This is achieved by bringing the
frequency to stimulate oscillation closer to the natural frequency of the
system or farther away from it. The desired oscillation amplitude of the
grinding set between 0.1 mm and 3.0 mm can always be achieved - and
with relatively low energy input. Therefore, continuous operation is pos-
sible without heating the sample material and the overall mill system.
The mortar bowl with 50 mm diameter grinding ball (or 70 mm for agate
only) and grinding stock oscillates vertically. This causes the grinding ball
in the mortar bowl to vibrate and comminute the grinding stock by
impact and friction.
2.2.2 Amplitude control
An electronic control circuit guides the oscillation frequency of the PUL-
VERISETTE 0 from a high to a low frequency range. In the meantime, a
measuring system records the amplitude and reports it to the control cir-
cuit until the preselected amplitude is reached.
This amplitude control takes place at regular intervals during the entire
operation. This makes it possible to react to changes in the vibratory
system.
The amplitude of the PULVERISETTE 0 is set manually with the Plus and
Minus key on the control panel and viewed on the lid.
2.3 Obligations of the operator
Before using the of the PULVERISETTE 0, this manual is to be carefully
read and understood. The use of the of the PULVERISETTE 0 requires
technical knowledge; only commercial use is permitted.
The operating personnel must be familiar with the content of the oper-
ating manual. For this reason, it is very important that these persons
actually receive the present operating manual. Ensure that the operating
manual is always near the device.
Safety information and use
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The of the PULVERISETTE 0 may exclusively be used within the scope of
applications set down in this manual and within the framework of guide-
lines put forth in this manual. In case of non-compliance or improper
use, the customer assumes full liability for the functional capability of
the PULVERISETTE 0 and for any damage or injury arising from failure to
fulfil this obligation.
By using the of the PULVERISETTE 0 the customer agrees with this and
recognizes that defects, malfunctions or errors cannot be completely
excluded. To prevent risk of damage to persons or property or of other
direct or indirect damage, resulting from this or other causes, the cus-
tomer must implement sufficient and comprehensive safety measures
for working with the of the PULVERISETTE 0.
Neither compliance with this manual nor the conditions and methods
used during installation, operation, use and maintenance of the of the
PULVERISETTE 0 can be monitored by Fritsch GmbH. Improper execution
of the installation can result in property damage and thus endanger per-
sons. Therefore, we assume absolutely no responsibility or liability for
loss, damage or costs that result from errors at installation, improper
operation or improper use or improper maintenance or are in any way
connected to these.
The applicable accident prevention guidelines must be complied with.
Generally applicable legal and other obligatory regulations regarding
environmental protection must be observed.
2.4 Information on hazards and symbols used in this manual
Safety information in this manual is designated by symbols. Safety infor-
mation is introduced by keywords that express the extent of the hazard.
DANGER!
This symbol and keyword combination points out a directly
hazardous situation that can result in death or serious
injury if not avoided.
WARNING!
This symbol and keyword combination points out a possibly
hazardous situation that can result in death or serious
injury if not avoided.
CAUTION!
This symbol and keyword combination points out a possibly
hazardous situation that can result in slight or minor injury
if not avoided.
Safety information
Safety information and use
- 10 -

NOTICE!
This symbol and keyword combination points out a possibly
hazardous situation that can result in property damage if
not avoided.
ENVIRONMENT!
This symbol and keyword combination points out a possibly
hazardous situation that can result in environmental
damage if not avoided.
To call attention to specific hazards, the following symbols are used in
the safety information:
DANGER!
This symbol and keyword combination points out a directly
hazardous situation due to electrical current. Ignoring infor-
mation with this designation will result in serious or fatal
injury.
DANGER!
This symbol and keyword combination designates contents
and instructions for proper use of the machine in explosive
areas or with explosive substances. Ignoring information
with this designation will result in serious or fatal injury.
DANGER!
This symbol and keyword combination designates contents
and instructions for proper use of the machine with com-
bustible substances. Ignoring information with this designa-
tion will result in serious or fatal injury.
WARNING!
This symbol and keyword combination points out a directly
hazardous situation due to movable parts. Ignoring infor-
mation with this designation can result in hand injuries.
Special safety information
Safety information and use
- 11 -

WARNING!
This symbol and keyword combination points out a directly
hazardous situation due to hot surfaces. Ignoring informa-
tion with this designation can result in serious burn injuries
due to skin contact with hot surfaces.
Safety information can refer to specific, individual procedure instruc-
tions. Such safety information is embedded in the procedure instructions
so that the text can be read without interruption as the procedure is
being carried out. The keywords described above are used.
Example:
1. Loosen screw.
2.
CAUTION!
Risk of entrapment at the lid.
Close the lid carefully.
3. Tighten screw.
This symbol emphasises useful tips and recommendations
as wells as information for efficient operation without mal‐
function.
To emphasise procedure instructions, results, lists, references and other
elements, the following designations are used in this manual:
Designation Explanation
1., 2., 3. ...
Step-by-step procedure instructions
ðResults of steps in the procedure
References to sections in this manual and rele-
vant documentation
Lists without a specific order
Safety information in the procedure
instructions
Tips and recommendations
Further designations
Safety information and use
- 12 -

Designation Explanation
[Button] Operating elements (e.g. push button, switch),
display elements (e.g. signal lamps)
‘Display’ Screen elements (e.g. buttons, function key
assignment)
2.5 Device safety information
nOnly use original accessories and original spare parts. Failure to
observe this instruction can compromise the safety of the machine.
nAccident-proof conduct is to be strictly followed during all work.
nComply with all currently applicable national and international acci-
dent prevention guidelines.
CAUTION!
Wear hearing protection!
If a noise level of 85 dB(A) is reached or exceeded, ear pro-
tection should be worn to prevent hearing damage.
WARNING!
The maximum accepted concentration (MAC) levels of the
relevant safety guidelines must be observed; if necessary,
ventilation must be provided or the machine must be oper-
ated under an extractor hood.
DANGER!
Explosion hazard!
– When grinding oxidizable substances, e.g. metals or
coal, there is a risk of spontaneous combustion (dust
explosion) if the share of fine particles exceeds a cer-
tain percentage. When grinding these kinds of sub-
stances, special safety measures must be taken and the
work must be supervised from a specialist.
–The high-speed rotor mill is not explosion protected
and is not designed to grind explosive materials.
nDo not remove the information signs.
NOTICE!
Immediately replace damaged or illegible information signs.
Please observe!
Safety information and use
- 13 -

nUnauthorised alteration of the of the PULVERISETTE 0 will void Frit-
sch's declaration of conformity to European directives and void the
guarantee.
nOnly use the of the PULVERISETTE 0 when it is in proper working
order, as intended and in a safety- and hazard-conscious manner
adhering to the operating manual. In particular, immediately rectify
any malfunctions that could pose a safety hazard.
nIf, after reading the operating manual, there are still questions or
problems, please do not hesitate to contact our specialised per-
sonnel.
2.6 Protective equipment
Protective equipment is to be used as intended and may not
be disabled or removed.
All protective equipment is to be regularly checked for
integrity and proper functioning.
NOTICE!
– The toothed belts must only be released or clamped in
the switched off state.
– Before switching on again, ensure that the two toothed
belts are evenly, tightly clamped using the knurled
knobs.
2.7 Hazardous points
nCrushing hazard at the mortar clamping device
nCrushing hazard between vibratory plate and housing
2.8 Electrical safety
2.8.1 General information
The main switch separates the device from the mains on two poles.
2.8.2 Protection against restart
After switching off at the main switch and switching on again, the START
key must be pressed for start-up.
Safety information and use
- 14 -

2.8.3 Overload protection
The mains fuse provides overload protection.
Safety information and use
- 15 -

3 Technical data
3.1 Dimensions
Without grinding set:
350 x 200 x 400 mm (width x height x depth)
3.2 Weight
Net: 21 kg
Gross: approx. 27 kg
3.3 Operating noise
Emissions value of workplace according to DIN EN ISO 3746:2005 is up to
76.6 dB (A) for grinding gravel. The value fluctuates depending on fre-
quency, grinding stock and the material of the grinding set.
When grinding with the PULVERISETTE 0, the operating noise is greatly
reduced by using the sound absorption hood made of plexiglas (order
no.: 00.0130.17).
3.4 Voltage
The device can be operated in two voltage ranges:
nSingle phase alternating current 115V ± 10% and
nSingle phase alternating current 230 V ± 10%.
(See also
Ä Chapter 4.5 ‘Electrical connection’ on page 19)
It is not necessary to change the voltage range manually.
3.5 Current consumption
Depending on the mains voltage, the maximum current consumption is
in the ranges:
n115 V ® 0.44 A
n230 V ® 0.22 A
3.6 Power consumption
Depending on the voltage range, the maximum power consumption is
approx. 50 W.
Technical data
- 16 -

3.7 Electrical fuses
nFuse under mains switch (on the back of the device)
Replacement: 4 A M micro fuse, 5 x 20 mm
3.8 Load
The maximum load of the PULVERISETTE 0 is up to 6 kg!
3.9 Material
nMaximum feed size 5 mm
nMaximum feed quantity 10 ml
3.10 Final fineness of a grinding process with the PULVERISETTE 0
The achievable final fineness (PULVERISETTE 0) of the grinding stock is
approx. 10 µm. (Depending on the grindability of the sample and the
grinding duration)
Technical data
- 17 -

4 Installation
4.1 Transport
The device is delivered in a cardboard box. In the case of delivery with
several accessories, the device is delivered in a transport crate.
WARNING!
Improper lifting can lead to personal injury or property
damage. The machine must only be lifted with suitable
equipment by qualified personnel.
The guarantee excludes all claims for damage due to improper transport.
4.2 Unpacking
nIn the case of delivery in a crate, pull out the nails that fasten the lid
to the surrounding packaging.
nRemove the lid.
nTake out the accessories.
nTo remove the device, three hexagon screws under the wooden
plate must be unscrewed.
nCompare the contents of the delivery with your order.
Keep the wooden plate, screws and washers, as this trans‐
port securing device must be reattached in the case of fur‐
ther transport or return.
4.3 Setting up
nPlace the device on a flat, stable surface. It does not have to be fas-
tened to the surface. Leave sufficient space beside the device for
placing the accessories used.
nThe space behind the device must be freely accessible so that the
main switch on the mains connection can be accessed quickly in case
of emergency.
nThe device rests on three flat coil spring assemblies. Level the micro
mill:
–PULVERISETTE 0:
Level the micro mill by screwing these feet in or out so that
during grinding, the grinding stock is evenly distributed on the
walls of the mortar bowl.
Installation
- 18 -

4.4 Ambient conditions
WARNING!
Mains voltage!
– The device may only be operated indoors.
–The surrounding air may not carry any electrically con-
ductive dust.
– Maximum relative humidity 80% for temperatures up
to 31°C, linearly decreasing down to 50% relative
humidity at 40°C.
nThe room temperature has to stay between 5 - 40°C.
nAltitudes up to 2000 m
nDegree of pollution 2 according to IEC 664.
4.5 Electrical connection
Before establishing the connection, compare the voltage and current
values stated on the type plate with the values of the mains system to be
used.
CAUTION!
Ignoring the values on the type plate may result in damage
to the electrical and mechanical components.
Installation
- 19 -

4.5.1 Adjusting the mains voltage
CAUTION!
Only qualified personnel may change the voltage range on
the device!
CAUTION!
The voltage range may only be adjusted after the mains has
been disconnected.
CAUTION!
If the values 06 or 07 are set at a voltage of 230V~, it will
result in a defect in the sieve shaker during operation.
Failure to observe this will render void the guarantee, and
releases us from liability for any resulting damage to the
device.
1. Switch main switch to "0".
2. Switch the device on at the main switch while holding down the
Stop key.
The device is now in "Setup" mode.
3. The "Sieving Time" display now shows the default setting "04" for
230 V, "06" for 115 V. The value "07" is preset for a mains voltage
of 100 V (in Japan).
4. These values can be changed with the "Sieving Time" +/- key and
adapted to the mains voltage.
n230 V - 04
n115 V - 06
n100 V - 07
The set value is automatically saved.
5. After making adjustments, switch on the main switch again.
Installation
- 20 -