Agilent Technologies G7166A User manual

Agilent Technologies
Agilent 1260 Infinity II
Preparative Valve-Based
Fraction Collector
User Manual

Preparative Valve-Based Fraction Collector
Notices
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Manual Part Number
G7166-90000 Rev. B
Edition
03/2018
Printed in Germany
Agilent Technologies
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Preparative Valve-Based Fraction Collector 3
In This Guide
In This Guide
This manual contains technical reference information about the Agilent 1260
Infinity II Preparative Valve-Based Fraction Collector.
1 Introduction to the Valve-Based Fraction Collector
This chapter gives an introduction to the module, instrument overview and
internal connectors.
2 Site Requirements and Specifications
This chapter provides information on environmental requirements, physical
and performance specifications.
3 Installing the Preparative Valve-based Fraction Collector
This chapter gives information about the installation of the module.
4 Using the Preparative Valve-Based Fraction Collector
This chapter explains the essential operational parameters of the module.
5 Preparing the Preparative Valve-Based Fraction Collector
This chapter explains the operational parameters of the module.
6 Troubleshooting and Diagnostics
This chapter gives an overview about the troubleshooting and diagnostic
features and the different user interfaces.
7 Error Information
This chapter describes the meaning of error messages, and provides
information on probable causes and suggested actions how to recover from
error conditions.

4 Preparative Valve-Based Fraction Collector
In This Guide
8 Maintenance
This chapter gives you an overview and instructions about the possible
maintenance and repair procedures that can be performed by the user.
9 Parts and Materials
This chapter provides information on parts and materials.
10 Identifying Cables
This chapter provides information on cables used with the module.
11 Hardware Information
This chapter describes the module in more detail on hardware and electronics.
12 Appendix
This chapter provides additional information on safety, legal, and web.

Preparative Valve-Based Fraction Collector 5
Contents
Contents
1 Introduction to the Valve-Based Fraction Collector 9
Product Description 10
Features 11
Typical Applications 12
Mounting Examples 13
2 Site Requirements and Specifications 15
Site Requirements 16
Physical Specifications 19
Performance Specifications 20
3 Installing the Preparative Valve-based Fraction Collector 21
Unpacking the module 22
Installing the Preparative Valve-Based Fraction Collector 24
Flow connections with the Preparative Valve-Based Fraction Collector 31
4 Using the Preparative Valve-Based Fraction Collector 33
Configuration and Operation of the Fraction Collector 34
Solvent Information 36
Status Indicators 42
5 Preparing the Preparative Valve-Based Fraction Collector 43
Leak and Waste Concept 44
Best Practices 45
Setting up the Preparative Valve-Based Fraction Collector with the Instrument
Control Interface 46
Method Parameter Settings 52
Pooling 62

6 Preparative Valve-Based Fraction Collector
Contents
6 Troubleshooting and Diagnostics 63
User Interfaces 64
Agilent Lab Advisor Software 65
Hardware Symptoms 66
7 Error Information 69
What Are Error Messages 70
General Error Messages 71
Module Specific Error Messages 76
8 Maintenance 79
Introduction to Maintenance 80
Cautions and Warnings 81
Overview of Maintenance 83
Cleaning the Module 84
Replacing the Fuses of the Preparative Valve-Based Fraction Collector 85
Replacing the Module Firmware 87
9 Parts and Materials 89
Valve Drive Parts 90
Accessory Kit 91
10 Identifying Cables 93
Cable Overview 94
Analog Cables 96
Remote Cables 98
CAN/LAN Cables 102
RS-232 Cables 103
USB 104

Preparative Valve-Based Fraction Collector 7
Contents
11 Hardware Information 105
Electrical Connections 106
Interfaces 109
Configuration Switch Settings of the Preparative Valve-Based Fraction
Collector 116
12 Appendix 119
General Safety Information 120
Waste Electrical and Electronic Equipment Directive 127
Radio Interference 128
Sound Emission 129
Agilent Technologies on Internet 130

8 Preparative Valve-Based Fraction Collector
Contents

9
Preparative Valve-Based Fraction Collector
Agilent Technologies
1
Introduction to the Valve-Based
Fraction Collector
Product Description 10
Features 11
Typical Applications 12
Mounting Examples 13
This chapter gives an introduction to the module, instrument overview and
internal connectors.

10 Preparative Valve-Based Fraction Collector
1 Introduction to the Valve-Based Fraction Collector
Product Description
Product Description
The Agilent 1260 Infinity II Preparative Valve-Based Fraction Collector
(G7166A) comprises 11 collection valves, one waste valve and one solvent inlet
port. Solvent coming from a preparative HPLC system can be diverted into
11 different fractions depending on the software/firmware settings. The valves
can then be blown clean by allowing compressed air or nitrogen to be passed
through the same valves.
No fraction racks are required, as collection takes place into larger collection
bottles that can be placed anywhere within reach of the tubing outlets. The
Preparative Valve-Based Fraction Collector can be used in addition to a
fraction collector.
Figure 1 Overview of front
Valve
Clamps (attachable to both sides)
Leak sensor
Leak plane (attachable)