Endress+Hauser Liquistation CSF48 User manual

Products Solutions Services
Operating Instructions
Liquistation CSF48
Automatic sampler for liquid media
BA00443C/07/EN/20.16
71317183
Valid as of version
01.06.00

Table of contents
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Table of contents
1 Document information .............. 5
1.1 Warnings ............................ 5
1.2 Symbols .............................. 5
1.3 Symbols at the device .................... 5
1.4 Documentation ........................ 6
2 Basic safety instructions ............ 7
2.1 Requirements for the personnel ............ 7
2.2 Designated use ........................ 7
2.3 Occupational safety ..................... 7
2.4 Operational safety ...................... 8
2.5 Product safety ......................... 9
3 Device description ................. 10
3.1 Device design ......................... 10
3.2 Equipment architecture ................. 12
3.3 Terminal diagram ..................... 13
4 Incoming acceptance and product
identification ..................... 14
4.1 Incoming acceptance ................... 14
4.2 Product identification ................... 14
4.3 Scope of delivery ...................... 15
4.4 Certificates and approvals ............... 15
5 Installation ....................... 16
5.1 Installation conditions .................. 16
5.2 Installation .......................... 22
5.3 Sampling with a flow assembly ............ 24
5.4 Post-installation check .................. 25
6 Electrical connection .............. 26
6.1 Connecting the sampler ................. 26
6.2 Connecting modules and sensors .......... 30
6.3 Terminal assignment for input/output
signals .............................. 37
6.4 Connection conditions .................. 37
6.5 Connecting additional inputs, outputs or
relays .............................. 39
6.6 Connecting digital communication ......... 42
6.7 Hardware settings ..................... 45
6.8 Ensuring the degree of protection .......... 46
6.9 Post-connection check .................. 47
7 System integration ................ 48
7.1 Web server .......................... 48
7.2 Service interface ...................... 49
7.3 Fieldbuses ........................... 50
8 Operation options ................. 52
8.1 Overview ............................ 52
8.2 Access to the operating menu via the local
display ............................. 53
8.3 Configuration options .................. 54
9 Commissioning .................... 57
9.1 Function check ....................... 57
9.2 Power up ............................ 57
9.3 Basic setup .......................... 59
9.4 Sampling programs .................... 60
10 Operation ......................... 63
10.1 Display ............................. 63
10.2 General settings ....................... 64
10.3 Programming ........................ 82
10.4 Inputs ............................. 123
10.5 Outputs ............................ 130
10.6 Additional functions .................. 138
11 Diagnostics and troubleshooting .. 155
11.1 General troubleshooting ................ 155
11.2 Diagnostic information on local display ..... 156
11.3 Diagnostic information via web browser .... 156
11.4 Diagnostic information via fieldbus ........ 156
11.5 Adapting the diagnostic information ...... 157
11.6 Overview of diagnostic information ....... 158
11.7 Pending diagnostic messages ............ 167
11.8 Diagnosis list ........................ 167
11.9 Logbooks ........................... 168
11.10 Device information ................... 173
11.11 Simulation .......................... 175
11.12 Device test .......................... 177
11.13 Resetting the measuring device .......... 180
11.14 Information on transit times ............ 180
11.15 Status of inputs/outputs ................ 181
11.16 Firmware history ..................... 182
12 Maintenance .................... 186
12.1 Recommended maintenance ............ 186
12.2 Calibration ......................... 187
12.3 Replacing the pump tube ............... 190
12.4 Cleaning ........................... 192
12.5 Replacing the rechargeable batteries ...... 197
12.6 Technical support .................... 198
13 Repairs .......................... 199
13.1 Spare parts ......................... 199
13.2 Return ............................. 203
13.3 Disposal ........................... 203

Table of contents
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14 Accessories ...................... 204
14.1 Measuring cable ..................... 207
14.2 Sensors ............................ 207
15 Technical data ................... 212
Index ................................. 222

Liquistation CSF48 Document information
Endress+Hauser 5
1 Document information
1.1 Warnings
Structure of information Meaning
LDANGER
Causes (/consequences)
Consequences of non-compliance
(if applicable)
‣Corrective action
This symbol alerts you to a dangerous situation.
Failure to avoid the dangerous situation will result in a fatal or serious
injury.
LWARNING
Causes (/consequences)
Consequences of non-compliance
(if applicable)
‣Corrective action
This symbol alerts you to a dangerous situation.
Failure to avoid the dangerous situation can result in a fatal or serious
injury.
LCAUTION
Causes (/consequences)
Consequences of non-compliance
(if applicable)
‣Corrective action
This symbol alerts you to a dangerous situation.
Failure to avoid this situation can result in minor or more serious injuries.
NOTICE
Cause/situation
Consequences of non-compliance
(if applicable)
‣Action/note
This symbol alerts you to situations which may result in damage to
property.
1.2 Symbols
Symbol Meaning
Additional information, tips
Permitted or recommended
Not permitted or not recommended
Reference to device documentation
Reference to page
Reference to graphic
 Result of a step
1.3 Symbols at the device
Symbol Meaning
Reference to device documentation

Document information Liquistation CSF48
6 Endress+Hauser
1.4 Documentation
The following manuals which are available on the complement these Brief Operating
Instructions Operating Instructions:
• Brief Operating Instructions for Liquistation CSF48, BA00443C
• Operating Instructions for Memosens, BA01245C
– Software description for Memosens inputs
– Calibration of Memosens sensors
– Sensor-specific diagnostics and troubleshooting
• Operating Instructions for HART communication, BA00486C
– Onsite settings and installation instructions for HART
– Description of HART driver
• Guidelines for communication via fieldbus and web server
– HART, SD01187C
– PROFIBUS, SD01188C
– Modbus, SD01189C
– Web server, SD01190C
– Web server (optional), SD01190C
– EtherNet/IP, SD01293C
• Special Documentation: Sampler application manual SD01068C
• Documentation on other devices in the Liquiline platform:
– Liquiline CM44xR (DIN rail device)
– Liquiline System CA80 (analyzer)
– Liquiline System CAT8x0 (sample preparation)
– Liquistation CSFxx (sampler)
– Liquiport CSP44 (sampler)

Liquistation CSF48 Basic safety instructions
Endress+Hauser 7
2 Basic safety instructions
2.1 Requirements for the personnel
• Installation, commissioning, operation and maintenance of the measuring system may
be carried out only by specially trained technical personnel.
• The technical personnel must be authorized by the plant operator to carry out the
specified activities.
• The electrical connection may be performed only by an electrical technician.
• The technical personnel must have read and understood these Operating Instructions
and must follow the instructions contained therein.
• Measuring point faults may be repaired only by authorized and specially trained
personnel.
Repairs not described in the Operating Instructions provided may only be carried out
directly by the manufacturer or by the service organization.
2.2 Designated use
Liquistation CSF48 is a stationary sampler for liquid media. The samples are taken
discontinuously using a vacuum pump or peristaltic pump or sampling assembly and are
then distributed into sampling containers and refrigerated.
The sampler is designed for use in the following applications:
• Communal and industrial wastewater treatment plants
• Laboratories and water management offices
• Monitoring of liquid media in industrial processes
Use of the device for any purpose other than that described, poses a threat to the safety of
people and of the entire measuring system and is therefore not permitted. The
manufacturer is not liable for damage caused by improper or non-designated use.
2.3 Occupational safety
As the user, you are responsible for complying with the following safety conditions:
• Installation guidelines
• Local standards and regulations
• Regulations for explosion protection
Electromagnetic compatibility
• The product has been tested for electromagnetic compatibility in accordance with the
applicable European standards for industrial applications.
• The electromagnetic compatibility indicated applies only to a product that has been
connected in accordance with these Operating Instructions.

Basic safety instructions Liquistation CSF48
8 Endress+Hauser
2.4 Operational safety
1. Before commissioning the entire measuring point, verify that all connections are
correct. Ensure that electrical cables and hose connections are undamaged.
2. Do not operate damaged products, and safeguard them to ensure that they are not
operated inadvertently. Label the damaged product as defective.
3. If faults cannot be rectified:
Take the products out of operation and safeguard them to ensure that they are not
operated inadvertently.
LCAUTION
Cleaning not switched off during calibration or maintenance activities
Risk of injury due to medium or cleaning agent
‣If a cleaning system is connected, switch if off before removing a sensor from the
medium.
‣If you wish to check the cleaning function and have therefore not switched off the
cleaning system, please wear protective clothing, goggles and gloves or take other
appropriate measures.

Liquistation CSF48 Basic safety instructions
Endress+Hauser 9
2.5 Product safety
2.5.1 State of the art
The product is designed to meet state-of-the-art safety requirements, has been tested, and
left the factory in a condition in which it is safe to operate. The relevant regulations and
European standards have been observed.
Devices connected to the sampler must comply with the applicable safety standards.
2.5.2 IT security
We only provide a warranty if the device is installed and used as described in the
Operating Instructions. The device is equipped with security mechanisms to protect it
against any inadvertent changes to the device settings.
IT security measures in line with operators' security standards and designed to provide
additional protection for the device and device data transfer must be implemented by the
operators themselves.

Device description Liquistation CSF48
10 Endress+Hauser
3 Device description
3.1 Device design
Depending on the version, a complete sampling unit for open channels comprises:
• Controller with display, soft keys and navigator
• Vacuum or peristaltic pump for sampling
• PE or glass sample bottles for sample preservation
• Sampling chamber temperature regulator (optional) for safe sample storage
• Suction line with suction head
12
3
4
5
6
7
9
8
10
A0029715
 1 Example of a Liquistation, version with vacuum pump
1 Controller
2 Window (optional)
3 Dosing chamber door
4 Suction line connection
5 Sampling chamber door
6 Sample bottles, e.g. 2 x 12
bottles, PE, 1 liter
7 Bottle trays (depending on
sample bottles selected)
8 Distribution plate (depending
on sample bottles selected)
9 Distribution arm
10 Vacuum system, e.g. Dosing
system with conductive
sample sensor
12
3
4
5
6
7
9
8
10
A0024291
 2 Example of a Liquistation, version with peristaltic pump
1 Controller
2 Window (optional)
3 Dosing chamber door
4 Suction line connection
5 Sampling chamber door
6 Sample bottles, e.g. 2 x 12
bottles, PE, 1 liter
7 Bottle trays (depending on
sample bottles selected)
8 Distribution plate (depending
on sample bottles selected)
9 Distribution arm
10 Peristaltic pump
LWARNING
Risk of injury
Danger of injury due to rotating parts
‣Secure the sampler against unintentional start-up whilst you work on the opened hose
pump.

Liquistation CSF48 Device description
Endress+Hauser 11
A complete sampling unit for pressurized pipes comprises a Liquistation and a Samplefit
CSA420 sampling assembly with:
• Controller with display, soft keys and navigator
• Samplefit CSA420 sampling assembly for 10 ml, 30 ml or 50 ml sample volume,
depending on version
• PE or glass sample bottles for sample preservation
• Sampling chamber temperature regulator (optional) for safe sample storage
1
2
3
4
5
6
7
8
A0024319
 3 Example of a Liquistation CSF48 with CSA420 sampling assembly
1 Controller
2 Samplefit CSA420 sampling
assembly
3 Gland for sample line
4 Sample bottles, e.g. 2 x 12
bottles, PE, 1 liter
5 Bottle trays (depending on
sample bottles selected)
6 Distribution plate (depending
on sample bottles selected)
7 Distribution arm
8 Distribution plate (depending
on sample bottles selected)
9 Distribution arm
10 Direct supply line for sample
Example of Samplefit CSA420 sampling assembly with flange connection
A0024320
 4 Samplefit CSA420 sampling assembly with flange connection DN50, PP
Example of Samplefit CSA420 sampling assembly with Triclamp connection
A0024321
 5 Samplefit CSA420 sampling assembly with triclamp connection DN50, DIN 32676

Device description Liquistation CSF48
12 Endress+Hauser
3.2 Equipment architecture
3.2.1 Slot and port assignment
E
85
85 86
86
41
43 42
87
88
97
98
31
31 32
32
SD
Display
1
2
Sensor
0/4 ... 20 mA
Sensor supply
+
+
–
+
+
–
1
2
Service
PK
GY
PK
GYGY
1
2
–
BN
WH
GN
YE
BN
WH
GN
YE
87
88
97
98
+
–AB
+
–
A
B
–
Alarm
HART
Power
(internal)
24VDC
24V
12,5V
3,3V
A0016633-EN
 6 Slot and port assignment of hardware and presentation on the display
The electronics configuration follows a modular concept:
• There are several slots for electronics modules. These are referred to as "slots".
• These slots are numbered consecutively in the housing. Slots 0 and 1 are always reserved
for the basic module.
• In addition there are also inputs and outputs for the control module. These slots are
labeled "S".
• Each electronics module has one or more inputs and outputs or relays. Here they are all
collectively known as "ports".
• Ports are consecutively numbered per electronics module and are recognized
automatically by the software.
• Outputs and relays are named according to their function, e.g. "current output", and are
displayed in ascending order with the slot and port numbers.
Example:
"Current output 2:1" shown on the display means: slot 2 (e.g. AOR module) : port 1
(current output 1 of the AOR module)
• Inputs are assigned to measuring channels in the ascending order of "slot:port number"
Example:
"CH1: 1:1" shown on the display means:
Slot 1 (base module) : port 1 (input 1) is channel 1 (CH1) and a conductivity sensor is
connected here.

Liquistation CSF48 Device description
Endress+Hauser 13
3.3 Terminal diagram
The unique terminal name is derived from:
Slot no. : Port no. : Terminal
Example, NO contact of a relay
Device with inputs for digital sensors, 4 current outputs and 4 relays
• Base module BASE-E (contains 2 sensor inputs, 2 current outputs)
• Module 2AO (2 current outputs)
• Module 4R (4 relays)
1 2 34
43 42 41 43 42 41 43 42 41 43 42 41
Relay 1
Relay 2
Relay 3
Relay 4
Slot
Slot 4 Port 1 Pin 41
A0025105
 7 Creating a terminal diagram using the example of the NO contact (terminal 41) of a relay

Incoming acceptance and product identification Liquistation CSF48
14 Endress+Hauser
4 Incoming acceptance and product
identification
4.1 Incoming acceptance
1. Verify that the packaging is undamaged.
 Notify your supplier of any damage to the packaging.
Keep the damaged packaging until the matter has been settled.
2. Verify that the contents are undamaged.
 Notify your supplier of any damage to the delivery contents.
Keep the damaged products until the matter has been settled.
3. Check the delivery for completeness.
 Check it against the delivery papers and your order.
4. Pack the product for storage and transportation in such a way that it is protected
against impact and moisture.
 The original packaging offers the best protection.
The permitted ambient conditions must be observed (see "Technical data").
If you have any questions, please contact your supplier or your local sales center.
NOTICE
Damage to the sampler
If transported incorrectly, the roof may become damaged or tear off.
‣Transport the sampler using a forklift truck. Never lift the sampler by the top. Lift it in
the middle between the upper and lower sections.
4.2 Product identification
Nameplates can be found:
• On the inside of the door
• On the packaging (adhesive label, portrait format)
4.2.1 Nameplate
The nameplate provides you with the following information on your device:
• Manufacturer identification
• Order code
• Extended order code
• Serial number
• Firmware version
• Ambient and process conditions
• Input and output values
• Activation codes
• Safety information and warnings
‣Compare the data on the nameplate with your order.

Liquistation CSF48 Incoming acceptance and product identification
Endress+Hauser 15
4.3 Scope of delivery
The scope of delivery comprises:
• 1 Liquistation CSF48 with:
– The ordered bottle configuration
– Optional hardware
• Accessories kit
– For peristaltic or vacuum pump:
Connection nipple for suction line with various angles (straight, 90°), Allen key (for
version with vacuum pump only)
– For sampling assembly:
2 or 3 compressed air lines 5 m each, 1 sample line EPDM 13 mm ID 5 m
• 1 print version of Brief Operating Instructions in the language ordered
• Optional accessories
If you have any questions, please contact your supplier or your local sales center.
4.4 Certificates and approvals
4.4.1  mark
Declaration of Conformity
The product meets the requirements of the harmonized European standards. As such, it
complies with the legal specifications of the EC directives. The manufacturer confirms
successful testing of the product by affixing to it the  mark.
MCERTS
The device has been assessed by Sira Certification Service and complies with "MCERTS
Performance Standards for Water Monitoring Equipment Part 1, Version 2.1 dated
November 2009"; certificate no.: Sira MC100176/02.
cCSAus General purpose
The product meets the requirements in accordance with "Class 8721 05, laboratory
equipment, electrical; Class 8721 85, laboratory equipment, electrical, certified to US
standards" for indoor use. Certificate no.: 2318018

Installation Liquistation CSF48
16 Endress+Hauser
5 Installation
5.1 Installation conditions
5.1.1 Dimensions
355 (14.0)
125 (4.9)
903 (35.6)
1258 (49.5)
625 (24.6)
471 (18.5)
816 (32.1)
753 (29.7)
355 (14.0)
125 (4.9)
530 (20.9)
1403 (55.2)
1758 (69.2)
625 (24.6)
471 (18.5)
816 (32.1)
753 (29.7)
AA
A
A
A0025857
 8 Dimensions of Liquistation CSF48 plastic version, without/with stand, dimensions in mm (in)
A Suction line connection

Liquistation CSF48 Installation
Endress+Hauser 17
355 (14.0)
125 (4.9)
903 (35.6)
1297 (51.1)
624 (24.6)
467 (18.4)
816 (32.1)
743 (29.3)
355 (14.0)
125 (4.9)
530 (20.9)
1403 (55.2)
1797 (70.8)
624 (24.6)
467 (18.4)
816 (32.1)
743 (29.3)
A
A
AA
A0024423
 9 Dimensions of Liquistation CSF48 CSF34 stainless steel version, without/with stand, dimensions in mm
(in)
A Suction line connection

Installation Liquistation CSF48
18 Endress+Hauser
5.1.2 Installation site
For version with sample pump
1 2 3
4
A0024411
 10 Installation conditions for the Liquistation
1. Correct
 The suction line must be routed with a downward slope to the sampling point.
2. Incorrect
 The sampler should never be mounted in a place where it is exposed to
aggressive gases.
3. Incorrect
 Avoid siphoning effects in the suction line.
4. Incorrect
 The suction pipe should never be routed with an upward gradient to the sampling
point.
Note the following when erecting the device:
• Erect the device on a level surface.
• Protect the device against additional heating (e.g. from a heating system).
• Protect the device against mechanical vibrations.
• Protect the device against strong magnetic fields.
• Make sure air can circulate freely at the side panels of the cabinet. Do not mount the
device directly against a wall. Allow at least 150 mm (5.9") from the wall to the left and
right.
• Do not erect the device directly above the inlet channel of a wastewater treatment plant.

Liquistation CSF48 Installation
Endress+Hauser 19
For version with sampling assembly
1
2
3
4
A0024412
 11 Installation conditions for Liquistation CSF48 with Samplefit CSA420 sampling assembly
Note the following when installing the sampling assembly in a pipe:
• The best installation location is in the ascending pipe (pos. 2). Installation is also
possible in the horizontal pipe (pos. 1).
• Avoid installation in the down pipe (pos. 4).
• Avoid siphoning effects in the sample line.
• The minimum vertical distance between the assembly and the inlet of the sampler
should be at least 0.5 m (1.65 ft).
Note the following when erecting the sampler:
• Erect the device on a level surface.
• Protect the device against additional heating (e.g. from a heating system).
• Protect the device against mechanical vibrations.
• Protect the device against strong magnetic fields.
• Make sure air can circulate freely at the side panels of the cabinet. Do not mount the
device directly against a wall. Allow at least 150 mm (5.9") from the wall to the left and
right.
• Do not erect the device directly above the inlet channel of a wastewater treatment plant.

Installation Liquistation CSF48
20 Endress+Hauser
5.1.3 Mechanical connection
Foundation plan
302 (11.9)
195.4 (7.69)
C
C
D
B
AA
AA
137.4 (5.41) 355 (14.0) 61 (2.4)
605 (23.8)
730 (28.7)
786 (30.9)
214 (8.43)
255 (10.0)
311 (12.2) 305 (12.0)
33.6 (1.32)
A0024406
 12 Foundation plan
A Fasteners (4 x M10)
B Cable inlet
C Outlet for condensate and overflow > DN 50
D Sample supply from below > DN 80
--- Dimensions of Liquistation
5.1.4 Connection for suctioning samples
• Maximum suction height:
– Vacuum pump: Standard 6 m (20 ft) Optional 8 m (26 ft)
– Peristaltic pump: standard 8 m (26 ft)
• Maximum hose length: 30 m (98 ft)
• Hose connection diameter
– Vacuum pump: 10 mm (3/8") 13 mm (1/2") , 16 mm (5/8") or 19 mm (3/4") internal
diameter
– Peristaltic pump: internal diameter of 10 mm (3/8")
• Intake speed:
> 0.6 m/s (> 1.9 ft/s) for 10 mm (3/8") ID, as per Ö 5893, US EPA
> 0.5 m/s (> 1.6 ft/s) for ≤ 13 mm (1/2") ID, in accordance with EN 25667, ISO 5667
Note the following when erecting the device:
• Always route the suction line so that it slopes upwards from the sampling point to the
sampler.
• The sampler must be located above the sampling point.
• Avoid siphoning effects in the suction line.